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294results about How to "Evenly distributed ingredients" patented technology

Preparation method of iron oxide cathode material for lithium ion battery

The invention discloses a preparation method of an iron oxide cathode material for lithium ion battery, which belongs to the fields of new material and electrochemistry. The invention employs a sol-gel method and normal pressure drying technology for preparing an iron oxide precursor with xerogel or aerogel structure, and after a heat treatment technology, the iron oxide cathode material is parpared. The invention also employs a carbon cladding technology for preparing iron oxide / carbon composite material. The invention has the advantages that the prepared material is fine and uniform particle powder, and the preparation technology process is simple with mild condition and low cost, and is convenient for large scale preparation. The iron oxide cathode material and iron oxide / carbon composite cathode material has higher circulating ratio capacity and good circulating stability, and is used as an ideal lithium ion battery cathode material, and has latent application prospects in the fields of portable electronic equipment, electric automobile and aviation spaceflight, etc.
Owner:UNIV OF SCI & TECH BEIJING

Spherical copper coating tungsten composite powder, preparation method and application thereof

The invention relates to a spherical copper coating tungsten composite powder, a preparation method and an application thereof. The copper coating tungsten composite powder is in a core-shell structure, the shell is a copper plating layer, the core is tungsten powder, and the weight ratio of the tungsten elements and copper elements of the copper coating tungsten composite powder ranges from 5 to 95 : 95 to 5; the spherical copper coating tungsten composite powder has the advantages of fine dispersion performance, high liquidity, even ingredients and high purity. The preparation method includes processing ordinary tungsten powder by a plasma spheroidizing technology, allowing the copper to deposit on the surface of the tungsten powder evenly by the intermittent copper electroplating process, and cleaning and drying the composite powder coated with copper. The spherical copper coating tungsten composite powder is prepared by combining the plasma spheroidizing and intermittent copper electroplating, the method is simple, reliable and easy to operate, the electroplating speed, the electroplated layer thickness and copper content range can be adjusted effectively, the copper-tungsten composite material comprehensive performances can be improved effectively, the expanded application prospect is provided, and the method can be applied to industrialized mass production.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Lithium-rich manganese-based cathode material precursor, cathode material and preparation method thereof

ActiveCN106564967AAccelerates and intensifies the mass transfer processWell mixedMaterial nanotechnologyCell electrodesNickel saltManganese
The invention belongs to the field of electrode material preparation and relates to a lithium-rich manganese-based cathode material precursor, a cathode material and a preparation method thereof. The preparation method comprises the following steps: mixing metal salts (manganese salt, cobalt salt and nickel salt) and a surfactant and water, and dissolving to obtain a metal salt solution; putting a precipitant in water, stirring and dissolving to obtain a precipitant solution; carrying out liquid-liquid coprecipitation reaction on the metal salt solution and the precipitant solution in a hypergravity field reactor, filtering, cleaning, and carrying out vacuum drying so as to obtain a precursor; mixing the precursor and lithium salt and then calcining so as to obtain the lithium-rich manganese-based cathode material. By the coprecipitation method based on the hypergravity technology, the lithium-rich manganese-based cathode material precursor with primary particle being below 100 nm and secondary particle being 1-10 microns is rapidly prepared, and furthermore the prepared cathode material has advantages of uniform component distribution and particle size distribution, small granularity and high activity. Initial irreversible capacity can be reduced, and cycle performance of a lithium ion secondary battery can be enhanced.
Owner:ADVANCED TECHNOLOGY & MATERIALS CO LTD

Preparation method of lithium ion battery silicon-carbon composite cathode material

The invention discloses a preparation method of a lithium ion battery silicon-carbon composite cathode material. The preparation method is characterized by comprising the following steps: 1), dissolving ethyl orthosilicate in a mixed solution of absolute ethyl alcohol and deionized water, adding organic acid in the solution, regulating the pH value of the solution to 3-5, and marking the solution as a solution A; 2), adding graphite particles in the solution A, stirring the mixture, and marking the mixture as a mixture B; 3), slowly adding ammonia water in the mixture B while stirring by high speed magnetic force, wherein the concentration of the ammonia water is 10-20%, adding a basic catalyst until forming gel; 4), drying gel prepared in the step 3 at 90-110 DEG C; 5), introducing hydrocarbon gas and nitrogen or the mixed gas of nitrogen and argon to the gel material prepared in the step 4 at 600-800 DEG C for 2-6 h, and then introducing high-pure nitrogen or high-pure argon, raising the temperature to 900-1200 DEG C, keeping the temperature for 1-6 h, cooling the mixture, and at last obtaining the silicon-carbon composite cathode material.
Owner:CHINA NAT OFFSHORE OIL CORP +2

Gamma-type high-entropy rare earth disilicate with ultrahigh-temperature stability and preparation method thereof

ActiveCN111056826AIncrease configuration entropyHas ultra-high temperature stabilityRare-earth elementHigh density
The invention relates to the field of ceramic materials for thermal barrier/environmental barrier integrated coating layers of advanced aero-engines, and in particular, relates to gamma-type high-entropy rare earth disilicate with ultrahigh-temperature stability and a preparation method thereof. The chemical formula of the gamma-type high-entropy rare earth disilicate ceramic material is defined in the specification, wherein n is more than or equal to 5, and REn is one of rare earth elements Y, Sc, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb and Lu respectively. The preparation method specifically comprises the preparation processes: by taking corresponding rare earth oxide powder and silicon oxide powder as raw materials, performing wet mixing, and performing pressureless sintering synthesis in an air atmosphere, and thus obtaining the gamma-type high-entropy rare earth disilicate ceramic powder material; and further hot-pressing and sintering in a hot-pressing furnace witha protective atmosphere to obtain the gamma-type high-entropy rare earth disilicate ceramic block material with excellent high-temperature phase stability. According to the invention, the gamma-typehigh-entropy ceramic material with high purity, high density and excellent high-temperature phase stability can be prepared.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

High-conductivity hard aluminum wire and preparing technology thereof

The invention discloses a high-conductivity (63 percent IACS) hard aluminum wire and a preparing technology thereof. The preparing technology of the high-conductivity hard aluminum wire comprises the following steps that firstly, a high-conductivity aluminum rod is prepared in a continuous casting and rolling mode; secondly, the high-conductivity aluminum rod is drawn into high-conductivity aluminum wires which are drawn through various dies, wherein the coefficient of elongation of the last die is controlled within 1.35-1.50, and the coefficients of elongation of the other dies are controlled within 1.30-1.40; thirdly, a plurality of high-conductivity aluminum wires are twisted, the pay-off tension is controlled in the twisting process, the control air pressure is smaller than or equal to 3 kilograms, the tensile strength of the manufactured single hard aluminum wire is larger than or equal to 160 MPa, and the conductor resistance is smaller than or equal to 0.027366 Omega*mm<2> / m when the temperature is 20 DEG C. The tensile strength of the manufactured single hard aluminum wire in an overhead conductor is larger than or equal to 160 MPa, the conductor resistance is smaller than or equal to 0.027366 Omega*mm<2> / m when the temperature is 20 DEG C, the tensile strength of the hard aluminum wire is kept, the conductivity of the hard aluminum wire is increased to 63 percent IACS, and the conductivity is increased by 3.28 percent compared with the stipulated conductivity of a hard aluminum wire in common GB / T17937-2009. The high-conductivity hard aluminum wire is used in the overhead conductor, the loss of the circuit electric energy can be greatly reduced, the circuit operation cost is reduced, and the carrying capacity of the wire can be obviously improved.
Owner:FAR EAST CABLE +2

Casting equipment and method using solid-liquid two-phase region temperature as casting mold temperature

ActiveCN101817072AHigh surface finishSpecial organizational structureSurface finishCrucible
The invention discloses casting equipment and a casting method using solid-liquid two-phase region temperature as casting mold temperature, and belongs to the technical field of metal casting. The casting equipment is characterized by consisting of a crucible, two-phase region casting molds, a heater, a cooler and a traction mechanism, wherein one or more two phase region casting molds are arranged below, above or beside the crucible; the casting mold is insulated and heated through the heater or heated by using the heat which is conducted by the cast metal melt before entering the casting mold so as to keep the casting mold temperature between the solidus temperature and the liquidus temperature of the cast metal; the cast metal is forcibly cooled through the cooler which is arranged close to the outlet of the casting mold or a cooling device which is arranged at the outlet of the casting mold and can move along the casting direction; and the traction mechanism is used for drawing a metal casting blank. The equipment of the invention has the advantages of simple structure, convenient operation and repair, high production efficiency and wide application range and can industrially produce the high-quality metal casting blank with high strength, high plasticity, high surface finish, high dimensional accuracy, high compactness and low or no segregation in batches.
Owner:UNIV OF SCI & TECH BEIJING

Preparing method for aluminum base silicon carbide

A preparing method for an aluminum base silicon carbide comprises the steps that firstly, SiC/Al slurry is prepared, SiC slurry is obtained through preparing of SiC micro powder, and aluminum powder and magnesium powder are added in proportion and are evenly mixed; secondly, tape casting is carried out, the SiC/Al slurry is subjected to defoaming, an initiating agent with the weight accounting for 1% to 3% of the total weight of the SiC/Al slurry and monomer with the weight accounting for 2% to 4% of the total weight of the SiC/Al slurry are added and are evenly mixed, and tape casting is carried out to obtain an SiC/Al cast film; thirdly, biscuiting is carried out on the cast film, wherein biscuiting is carried out on the casting film obtained in the second step, and an SiC/Al biscuit is obtained; and fourthly, vacuum sintering is carried out, and the SiC/Al biscuit is sintered in the vacuum state to obtain the aluminum base silicon carbide. The aluminum base silicon carbide is prepared through a gel tape casting method, obtained product components are evenly distributed, the porosity is low, the heat conduction rate is high, the magnesium powder is introduced, the sintering performance is improved, and the sintering temperature is reduced. The technology is simple, and energy consumption is low.
Owner:李大海

Iron-based composite powder high in chromium content for laser cladding

The invention discloses iron-based composite powder high in chromium content for laser cladding. The iron-based composite powder high in chromium content for laser cladding is composed of the chemical compound of Cr3C2, Cr and Fe, Ni, Mo, Si and B. The iron-based composite powder high in chromium content for laser cladding comprises, by mass, 38%-40% of Cr, 4.2%-4.5% of C, 3%-5% of Ni, 0.05%-0.08% of Mo, 0.8%-1.02% of Si, 1.2%-1.78% of B and the balance Fe. The particle size of the iron-based composite powder is between +140 meshes and -325 meshes. The iron-based composite powder is high in carbon content and chromium content, the hardness of a coating can be effectively improved, requirements of the laser cladding technology of iron-based base materials such as carbon steel and stainless steel can be met, a cladding layer of a sample of the iron-based composite powder is free of cracks and macroscopic pores, all the components are distributed evenly, the hardness of the iron-based composite powder can reach HV0.21000 and is five times that of a base body, the corrosion resistance of the iron-based composite powder cladding layer is improved due to the high chromium content, and the iron-based composite powder is suitable for normal temperature, high temperature, abrasion resistance and corrosion resistance working conditions.
Owner:INST OF SEMICONDUCTORS - CHINESE ACAD OF SCI

Flat plate solar energy heat absorption coating

The invention discloses a flat plate solar energy heat absorption coating. A light absorption agent, a film forming agent, a solvent and an addition agent are evenly scattered in a ball milling mode, then a film forming addition agent is added into the mixture to be mixed to be uniform, and therefore the flat plate solar energy heat absorption coating is obtained. The flat plate solar energy heat absorption coating is prepared from, by weight, 50-100 parts of the film forming agent, 10-30 parts of the film forming addition agent, 35-55 parts of the light absorption agent, 20-50 parts of the solvent and 10-30 part of the addition agent. The film forming addition agent is ethylene glycol monobutyl ether, triethylene glycol monomethyl and the like. A preparation method of the film forming agent comprises the steps that casein and gelatin are mixed according to the weight ratio of 5-10:2-3, water is added into the mixture, the mixture is soaked at the temperature of 15-22 DEG C and then transferred to a plate under the normal temperature, a mixture solution with methyl methacrylate and polysiloxane quaternary ammonium sodium with the ratio of parts by weight of 1-2:1-3, the mixture is stirred and then irradiated by ultraviolet light for 10-15 min, and then modified casein-gelatin is obtained. The film forming agent is modified and then used as the important raw material of the coating, so that the prepared coating has the good weather resistance and water resistance under the outdoor conditions, the preparation technology is simple and easy to understand, and the heat absorption efficiency of the heat absorption coating is ensured.
Owner:GUANGXI CHAOXING SOLAR ENERGY TECH
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