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697results about How to "Reduce hydrophilicity" patented technology

Preparation method of wear-resistant super-hydrophobic nanometer titania coating

The invention discloses a preparation method of a wear-resistant super-hydrophobic nanometer titania coating. The preparation method includes firstly, dissolving silane coupling agent in ethyl alcohol and then heating and stirring to react to obtain a solution; secondly, adding nanometer titania into the solution and then stirring and drying to obtain hydrophobic nanometer titania powder; thirdly, mixing a certain quantity of epoxy resin with hardener while adding in diluting agent to dilute the resin completely to obtain a diluted liquid, adding the hydrophobic nanometer titania powder into the diluted liquid, then subjecting the mixture to ultrasonic dispersion with complete stirring to allow the nanometer titania to contact with the resin completely so as to obtain a suspension liquid; and finally, coating the suspension liquid on a base material and drying completely so as to obtain the wear-resistant super-hydrophobic nanometer titania coating. Compared with the pure hydrophobic nanometer coating, the wear-resistant super-hydrophobic nanometer titania coating prepared by the method has the advantages that coating hardness is improved greatly, and super-hydrophobic property of the coating is guaranteed while interlayer adhesion and inner binding force of the nanometer coating are improved greatly.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Preparation method and application of basalt fiber surface modified coating

The invention belongs to the technical field of inorganic fiber modification, and relates to basalt fiber surface modification, in particular to a preparation method of a basalt fiber surface modifiedcoating. The method includes the steps: firstly, adding silane coupling agents, surface active agent solution, polyacrylamide solution and 1/3 water-borne epoxy resins into an appropriate amount of nano-silicon dioxide dispersion liquid, and performing reflux reaction; secondly, dropping residual water-borne epoxy resins and initiating agent solution when heating, and performing continuous reaction of an alkaline system to obtain the basalt fiber surface modified coating. The invention further discloses an application of the prepared basalt fiber surface modified coating. Basalt fiber surfacegroups are activated by strong H2SO4/H2O2 mixed solution, etched by hydrochloric acid, soaked into the coating to graft and dried to constant weight. Prepared coating emulsion does not contain any organic solvents and is green, environmentally friendly, convenient and simple in operation technique, high in applicability and stable in performance and can be applied to the field of microbial film carrier materials, basalt fibers can be rapidly and effectively modified, and the surface roughness of the basalt fibers is obviously increased.
Owner:JIANGSU UNIV

Bottom surface-integrated wear-resistant fluorosilicone-based super-amphiphobic coating, and preparation method and application thereof

The invention discloses a bottom surface-integrated wear-resistant fluorosilicone-based super-amphiphobic coating, and a preparation method and application thereof. The preparation method comprises the following steps: 1) performing synergistic modification treatment on two or more nanoparticles to obtain modified blended particles; 2) adding the blended modified particles into a dispersing solvent, performing ultrasonic dispersion for 1 to 2 hours and then mechanically stirring; 3) adding a certain amount of tert-butyl acetate into fluoro-siloxane resin and performing shearing dispersion to obtain substrate material emulsion; 4) mixing the blended modified particle turbid liquid in the step 2 and the substrate material emulsion in the step 3, adding a coupling agent, heating, stirring anddispersing, and performing dispersion by a high-speed shearing dispersing machine to obtain super-amphiphobic coating; and 5) stirring the super-amphiphobic coating uniformly, spray-coating the surface of an object with the super-amphiphobic coating and drying at room temperature for 10 to 30 minutes to successfully prepare the wear-resistant integrated super-amphiphobic coating. The wear-resistant super-amphiphobic organic-inorganic hybrid coating is obtained by connecting a fluorine-silicon substrate and the blended modified particles through chemical grafting copolymerization reaction.
Owner:ELECTRIC POWER RESEARCH INSTITUTE OF STATE GRID SHANDONG ELECTRIC POWER COMPANY +1

Durable cellulose fiber and application thereof

The invention relates to the technical field of macromolecular composite materials, in particular to durable cellulose fiber and application thereof. A preparation method for the durable cellulose fiber comprises the following steps of: dispersing cellulose fiber in solvent in an amount which is 1 to 10 times the total amount of the cellulose fiber; adding diisocyanate monomer which accounts for 10 to 60 percent of the total weight of the cellulose fiber, and metal catalyst or amine catalyst, which accounts for 0 to 5 percent of the total weight of the cellulose fiber, for polyurethane synthesis into the dispersed solution to perform reaction, and then adding siloxane monomer or siloxane polymer which accounts for 5 to 50 percent of total weight of the cellulose fiber into the reaction solution to perform reaction; and finally, cooling the obtained reaction product to room temperature, washing and separating filtrate, and drying the filtrate to obtain the durable cellulose fiber of the invention. The obtained durable cellulose fiber has the advantages of obviously improved hydrophobic property, good thermal stability, ultraviolet ageing resistance and antibacterial performance, and meanwhile has good durability when the durable cellulose fiber is applied in a wood-plastic composite material.
Owner:HUANGSHAN HUASU NEW MATERIAL SCI & TECH CO LTD

Silane/graphene oxide composite passivation liquid and preparing method and application thereof

The invention relates to silane / graphene oxide composite passivation liquid and a preparing method and application thereof. The preparing method comprises the following steps that a water-based silanecoupling agent, water and alcohol are mixed according to the volume ratio being 1:(7-9):(0.8-1.2) to obtain mixing liquid; graphene oxide is added into the mixing liquid, and ultrasonic treatment iscarried out to obtain dispersion liquid; the pH value of the dispersion liquid is adjusted to be 2-4, and hydrolysis is carried out to obtain the silane / graphene oxide composite passivation liquid. The silane / graphene oxide composite passivation liquid and the preparing method of the silane / graphene oxide composite passivation liquid combine advantages of the graphene oxide and silane, the graphene oxide and the water-based silane coupling agent are used for joint hydrolysis, and the silane functionalization of the graphene oxide is achieved; and the silane coupling agent and a metal substrateform covalent bonds, the bonding force between a film layer and the metal substrate is improved, and the lamellar graphene oxide can strengthen the physic shielding property of the film layer on a corrosion medium.
Owner:GUANGZHOU SPECIAL PRESSURE EQUIP INSPECTION & RES INST

Adhesive for veneering of artificial board and preparation method of adhesive

The invention relates to an adhesive for a veneering of an artificial board and a preparation method of the adhesive. The adhesive comprises the components in parts by weight: 200 parts of formaldehyde, 20-50 parts of a modifier, 110-140 parts of urea, 5-15 parts of tripolycyanamide, and 1-10 parts of a tackifier. By addition of appropriate parts of modifier, on the one hand, the high solid content adhesive can be prepared without dehydration, moisture brought to a base material during coating is reduced, permeation of the adhesive is reduced, and glue penetration is reduced. In addition, through addition of the modifier, the molar ratio of formaldehyde and urea in the polycondensation phase in the urea resin synthetic process can be greatly reduced, so that hydrophilic radicals in the resin structure are greatly decreased. Meanwhile, tripolycyanamide in appropriate parts is added to modify, so that the water-solubility of the adhesive is reduced, the hydrophobicity of the adhesive is enhanced, and glue penetration is beneficially reduced. The tackifier in appropriate parts is added to improve the initial adhesion of the adhesive and reduce malposition of a veneer on the base material, so that the product quality is improved.
Owner:EVERFIRST WISEFUND TECH BEIJING

Preparation method of hydrophobic modified cationic polyacrylamide flocculant

A preparation method of hydrophobic modified cationic polyacrylamide flocculant comprises the following steps: weighing and mixing acrylamide, acryloyloxyethyl trimethyl ammonium chloride, butyl acrylate, perfluorinated octyl ethyl acrylate and a surfactant, obtaining polymer monomer aqueous solution by adding deionized water and mixing well by stirring, and then adding a plurality of additives; adding a compound initiator for polymerization and then adding a photoinitiator for polymerization; after the polymerization reaction, taking out colloidal particles for prilling, drying, crushing, and sifting, so that the hydrophobic modified cationic polyacrylamide flocculant is obtained. The flocculant provided by the present invention is able to improve the adsorption capacity of polymers to suspended particles, especially organic matters in water, by introducing lyophobic group into the macromolecule of the flocculant. Meanwhile, the flocculant possesses the properties of hydrophobic associating polymer, which is beneficial to the interaction between macromolecules, reducing the hydrophilic performance of the floc body, increasing the settling velocity of the floc body, and improving intensity of the flocs and water separation capability of the filter cake.
Owner:格润化学(东营)有限公司

Preparation method for metal organic framework structure wrapped ammonium polyphosphate fire retardant and application

The invention discloses a preparation method for a metal organic framework structure wrapped ammonium polyphosphate fire retardant and application. The preparation method comprises the following steps: dispersing ammonium polyphosphate in a methanol solution, adding the methanol solution containing dimethylimidazole in the mixed solution, uniformly stirring and mixing, dropwise adding the methanolsolution containing metal nitrate, uniformly stirring, performing a heating reflux reaction, centrifuging, washing and drying after completing the reaction, thereby obtaining the fire retardant. Thepreparation method has the advantages of simple processing step, high operability and low preparation cost; the active site of ammonium polyphosphate is sealed by adopting a metal organic framework structure to form an organic isolation layer with certain thickness to block the invasion of water, so that the polarity and the hydrophily of the material can be effectively reduced, the compatibilityand the dispersibility of the material and an organic high-molecular polymer are improved, and meanwhile, the catalytic charing effect is achieved, and the flame retardant efficiency of ammonium polyphosphate is improved; and the preparation method can be widely applied to fields of flame retardant materials such as epoxy resin, polyurethane, polystyrene, polylactic acid or polyolefin.
Owner:CHINA UNIV OF GEOSCIENCES (WUHAN)
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