The invention belongs to the technical field of material
science and engineering, and discloses calcining equipment for preparing high-purity
tantalum oxide, which comprises a
workbench, a fluotantalic acid solution produced by a
tantalum-
niobium liquid-liquid extraction method is used as a
raw material,
ammonia water and
ammonia gas are used for neutralizing and precipitating, and the high-purity
tantalum oxide is prepared by controlling different factors such as
ammonia water concentration, tantalum liquid concentration, ammonia flushing speed and neutralizing temperature.
Tantalum oxide particles are produced, then the produced
tantalum oxide particles are poured into the spherical shell, the calcining
crucible is started, heat conduction is conducted on the
tantalum oxide particles in the spherical shell through temperature rising of the calcining
crucible, and therefore the
tantalum oxide particles are calcined, meanwhile, the motor is driven, and the motor drives the rotating shaft and the spherical shell to rotate; in the rotating process of the spherical shell, the tantalum oxide particles can be subjected to rolling heating at the bottom of the inner wall of the spherical shell, the calcining effect on the tantalum oxide particles is improved, the tantalum oxide particles can be heated more uniformly, the conversion efficiency of the tantalum oxide particles can be increased, and the
surface structure of the particles can be optimized.