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406 results about "Substance amount" patented technology

Amount of substance (also called chemical amount) is a quantity defined by standards to measures the size a group of individual elementary entities, such as atoms, molecules and electrons, along with other particles. The International System of Units (SI) defines the amount of substance to be equal to the number of elementary entities present.

Preparation method and application of phosphorus-nitrogen-carbon-containing aggregate and intumescent flame retardant

The invention discloses a preparation method of a phosphorus-nitrogen-carbon-containing aggregate and intumescent flame retardant of a nano-sheet structure. The preparation method is characterized in that phytic acid, melamine and a solvent are prepared, the substance amount ratio of the phytic acid to the melamine is 1: 3 to 1: 15, and 20-50 ml of the solvent is added into every 0.01 mol of the melamine; the melamine is added into a reaction container provided with a thermometer and a stirrer, the solvent is added with stirring, the phytic acid is added at the temperature of 20-40 DEG C, and a reaction is conducted with stirring for 20-50 minutes, so that reaction liquid is obtained; and the reaction liquid is poured into a reaction still to react for 24-56 h at the temperature of 70-120 DEG C, cooling and suction filtration are conducted, solid is washed with ethyl alcohol and then washed with water till the pH is 7, and the solid is dried, so that the flame retardant is obtained. The preparation method is simple and environmentally friendly, and the synthesized phosphorus-nitrogen-carbon-containing aggregate and intumescent flame retardant of the nano-sheet structure has good compatibility with a polymer matrix and has good flame retardance.
Owner:SOUTHWEAT UNIV OF SCI & TECH

Method for preparing hydroxyapatite-natural macromolecular nano compound with one-pot method

The invention discloses a method for preparing a hydroxyapatite-natural macromolecular nano compound with a one-pot method. The method disclosed by the invention has the core characteristics that raw material powder is directly added, and mainly comprises the following steps: adding calcium salt and phosphate into a natural macromolecular solution according to the amount of substance ratio of Ca/P of 5 to 3; adjusting the pH of the system to 10 to 12 by using an alkali solution, wherein calcium ions, phosphate ions and hydroxyl ions in the system and natural macromolecules have an in-situ co-precipitation reaction; washing a reaction product to be neutral, and drying to obtain the hydroxyapatite-natural macromolecular nano compound; grinding and sieving to prepare nano composite particle products with different specifications. The method disclosed by the invention is simple and has moderate reaction conditions and small energy consumption; the obtained hydroxyapatite-natural macromolecular nano compound has good granularity, rigidity, microscopic appearance and crystallinity, and can be widely applied to the fields of bone defect repairing tissue engineering materials and medical equipment and the like of dental department, orthopedic surgery and the like.
Owner:HUBEI SAILUO BIOLOGICAL MATERIAL CO LTD

Graphene nano sheet and SnS2 composite nano material and synthesis method thereof

The invention discloses a graphene nano sheet and SnS2 composite nano material and a synthesis method thereof. The composite material is characterized by being formed by compounding a graphene nano sheet and a SnS2 nano material, wherein the substance amount ratio of the graphene nano sheet to the SnS2 nano material is 1:1-4:1. The preparation method comprises the following steps of: preparing a graphite oxide nano sheet from graphite by using a chemical oxidation method, then dissolving L-cysteine into deionized water, adding stannic chloride, and dissolving the stannic chloride with full stirring, wherein the molar ratio of the L-cysteine to the stannic chloride in the solution is 6:1-12:1; and adding the graphite oxide nano sheet into the solution, performing ultrasonic treatment so that the graphite oxide nano sheet is fully dispersed in the hydrothermal reaction solution, and synthesizing the graphene nano sheet and SnS2 composite nano material by a one-step hydrothermal method, wherein the mass ratio of the graphene nano sheet to the SnS2 nano material in the composite material is 1:1-4:1. The method has the characteristics of mild reaction condition and simple process. The synthesized graphene nano sheet and SnS2 composite nano material serving as an electrode material of a new energy battery or serving as other materials has wide application.
Owner:ZHEJIANG UNIV

Method for accurately measuring absorbed phase density of methane on shale

The invention relates to a method for accurately measuring absorbed phase density of methane on shale. The method comprises the following steps: 1) smashing a piece of shale sample to be 60-80 meshes, and dividing the powder into two; 2) performing a volumetric method isothermal adsorption experiment on the first shale sample, and obtaining a calculation model of the amount n, adsorbing CH4, of the adsorbed state methane substance; 3) performing a weight method isothermal adsorption experiment on the second shale sample, and obtaining a calculation model of the mass m, adsorbing CH4, of the adsorbed state methane; 4) performing adsorbed phase volume correction on the calculation model of the amount n, adsorbing CH4, of the adsorbed state methane substance, obtained in the step 2) and the calculation model of the mass m, adsorbing CH4, of the adsorbed state methane, obtained in the step 3), so as to obtain the corrected substance amount calculation model and the corrected mass calculation model of the adsorbed state methane; 5) according to a definition formula of the amount of substance, combining with the two calculation models in the step 4), and determining the mass m, adsorbing CH4, and the volume V adsorption of the adsorbed state methane; 6) according to the definition of the density, determining an exact adsorption value of the adsorbed phase density rho of methane on the shale.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Composite anode material LiMnPO4-Li3V2(PO4)3/C for lithium ion battery and preparation method of material

The invention relates to a composite anode material LiMnPO4-Li3V2(PO4)3/C for a lithium ion battery and a preparation method of the material. LiMnPO4 and Li3V2(PO4)3 in the LiMnPO4-Li3V2(PO4)3/C are stoichiometric compounds; a substance amount ratio of the LiMnPO4 to the Li3V2(PO4)3 is equal to 1/x, wherein x is more than 0 and is less than or equal to 1; and the carbon content in the compound is 1wt%-8wt%. The preparation method of the composite anode material comprises the following steps of: dissolving a lithium source compound, a manganese source compound, a vanadium source compound and a phosphorus source compound in de-ionized water according to a mol ratio of Li to Mn to V to P of (1+3x) to 1 to 2x to (1+3x), thus obtaining a solution, wherein x is more than 0 and is less than or equal to 1; secondly, carrying out spray drying on the solution to obtain precursor powder; heating the precursor powder in a tube furnace; mixing products after heat treatment with a carbon source matter, carrying out ball milling on the mixture to obtain slurry, and then drying the slurry; pre-sintering the slurry in inert atmosphere, and then roasting and cooling the slurry to obtain the composite material LiMnPO4-Li3V2(PO4)3/C. The composite anode material for the lithium ion battery prepared by the method has high capacity and good rate capability, and is applicable to a power battery.
Owner:新乡市中天新能源科技股份有限公司

Lithium adsorbent and preparation method of lithium adsorbent

The invention discloses a lithium adsorbent and a preparation method of the lithium adsorbent. The preparation method comprises the following steps: step S1: sufficiently mixing an aluminum chloride solution with the lithium compound to form a reaction preliminary body, wherein the amount of substance of the aluminum chloride to the lithium compound is (1.8 to 2.2) to 1, and the lithium compound is one of the lithium hydroxide, lithium carbonate and lithium chloride; step S2: adding a sodium hydroxide solution in the reaction preliminary body, wherein the amount of the substance of the sodium hydroxide to the aluminum chloride is (2.5 to 3.5) to 1; reacting to generate LiCl.2.2-2.8Al(OH)3.2.7-3.9H2O so as to form a first product; step S3, performing solid-liquid separation, drying, grinding and smashing on the first product to form a second product; step S4, adding adhesive and the liquid chlorine in the second product to realize mixing granulation, thereby forming a third product; and step S5, crushing and sieving the third product to obtain the lithium adsorbent. The preparation process of the lithium adsorbent is simple and efficient, the prepared lithium adsorbent is excellent in property, and the raw material has great selectivity, so that the preparation cost of the lithium adsorbent is effectively saved.
Owner:ЦИНХАЙ СОЛТ ЛЕЙК ИНДАСТРИ ГРУП КО ЛТД

Discoloration indicator for shelf life of perishable product and preparation method thereof

ActiveCN102735796ADistinguishable color changeAdjustable color change rateAnalysis using chemical indicatorsGold nanorodExtinction
The invention provides a discoloration indicator for shelf life of a perishable product and a preparation method thereof. The preparation method comprises the following steps: 1) preparing a surfactant aqueous solution containing chloride or bromide ions, a soluble ascorbate aqueous solution, a soluble weak acid or weak acid salt aqueous solution and a soluble silver salt solution, wherein concentration of each of the four aqueous solutions is not less than 0.1 mM; and 2) mixing gold nanorod with a largest extinction wavelength not less than 700nm with the four solutions in the step 1) to obtain the indicator, and conducting a metachromatism. During mixing, concentration of gold nanorod in the indicator needs to be adjusted to realize an optical density of the solution no less than 0.1cm<-1> at 500-520nm; usage amount of soluble silver salt in the indicator is no less than 4 times an amount of substance of gold in the gold nanorod solution matter; and usage amount of other reagent is adjusted according to shelf life of an indicating object. According to the invention, discoloration process of the perishable product with change of temperature is tracked and recorded to simulate a metamorphic process of the product to be indicated, and quality and shelf life of the product are visually indicated through the color.
Owner:PEKING UNIV

Composite flocculating agent for flocculation treatment of fracturing flow-back fluid and preparation method thereof

The invention provides a composite flocculating agent for flocculation treatment of a fracturing flow-back fluid and a preparation method thereof. The composite flocculating agent comprises the following raw materials: water glass, a coupling agent, an acrylamide monomer, a cationic monomer, a crosslinking agent and an initiating agent, wherein according to amounts of substances, the ratio of water glass to the acrylamide monomer is 1 to (1-10), and the ratio of the acrylamide monomer to the cationic monomer is (0.5-10) to 1; and according to mass, the amount of a silane coupling agent KH570 accounts for 0.005-0.05% of that of water glass, the amount of the crosslinking agent accounts for 0.005-0.1% of that of the acrylamide monomer, and the amount of the initiating agent accounts for 0.005-0.1% of the total mass of the acrylamide monomer and the cationic monomer. The preparation method disclosed by the invention is used for preparing the SiO2-cationic polyacrylamide composite flocculating agent by adopting an aqueous solution polymerization process, does not introduce an organic solvent, cannot cause pollution to the environment, and is simple in production process, mild in reaction and easy to perform; and the flocculating agent disclosed by the invention has a good flocculation treatment effect in a flocculation treatment process of a shale gas fracturing flow-back fluid.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Method for preparing flaky calcite calcium carbonate crystal

The invention relates to a method for preparing a flaky calcite calcium carbonate crystal, which comprises the following steps of: according to the substance amount ratio of calcium chloride to sodium carbonate as 1.4-1.8:1, adding boric acid or oxalic acid as a crystal shape control agent accounting for 0.8-4.2 percent of the mass of the sodium carbonate into 0.52-3.96mol/L of sodium carbonate solution, and controlling the solution temperature to be 40-90 DEG C; taking 1.24-6.32mol/L of calcium chloride solution, and controlling the solution temperature to be 40-90 DEG C; dropwise adding the calcium chloride solution into the sodium carbonate solution, stirring as dropwise adding, then stirring at constant temperature for 0.5-2 hours, settling at room temperature for 12-36 hours, and filtering to obtain precipitates; and repeatedly washing the precipitates with water to be neutral, removing adsorbed chloride ions, then filtering, and carrying out vacuum drying at the temperature of 40-80 DEG C to prepare the flaky calcite calcium carbonate crystal. A product is confirmed as a calcite crystal through X-ray diffraction analysis; and a scanning electron microscope result shows that the crystal is regularly flaky. The method has the advantages of low cost, simple process and regular product appearance.
Owner:HENAN UNIV OF URBAN CONSTR
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