Method for growing yttrium ferrite crystal by guided mold pulling method
The technology of pulling method and yttrium ferrite is applied in the field of growing yttrium ferrite crystal by guided mode pulling method. The effect of uniform distribution of processes and components
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[0044] (1) Synthesis of polycrystalline raw materials: Accurately weigh Fe with a purity of 99.99% according to the ratio of Y / (Y+Fe) to 40.0% 2 o 3 and Y 2 o 3 Drugs, put the weighed drugs into a corundum mortar and grind them evenly, then press them into tablets on a tablet press, and then perform high-temperature sintering at a temperature of 1200°C for 15 hours to prepare polycrystalline raw materials.
[0045] (2) Single crystal growth: Using the guided mold pulling method, the iridium crucible is used as the crystal growth container, the guided mold is installed in the center of the crucible, and a circular iridium sheet with holes is placed on the upper surface of the guided mold. Add the prepared polycrystalline raw material in the crucible again, heat the crucible under nitrogen atmosphere to melt the polycrystalline raw material into a molten body, and make the molten body 5 of the polycrystalline raw material not pass through the gap in the lower part of the guide...
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