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45results about How to "Low oxygen content" patented technology

Preparation method of molybdenum-niobium alloy sputtering target

The invention discloses a preparation method of a molybdenum-niobium alloy sputtering target. The method comprises the following steps: (1) molybdenum powder and niobium powder are put in a mixing tank of a mixing machine for uniformly mixing to obtain mixed powder; (2) the cold isostatic pressing is performed for the mixed powder to obtain a slab; and the slab is pre-sintered under the vacuum or hydrogen atmosphere protection condition to obtain a molybdenum-niobium alloy prefabricated blank; (3) the surface of the molybdenum-niobium alloy prefabricated blank is turned and milled; and the hot isostatic pressing is performed to obtain a molybdenum-niobium alloy part; and (4) the mechanical processing and the surface grinding are performed for the molybdenum-niobium alloy part to obtain the molybdenum-niobium alloy sputtering target. The preparation method is simple in process, and saves raw materials; the introduction of impurity elements can be reduced in the preparation process; the prepared molybdenum-niobium alloy sputtering target is uniform in components, free of segregation and fine in grains; the theoretic density can reach above 99%; the oxygen mass content is lower than 500 ppm; and the requirements of the sputtering target can be preferably satisfied.
Owner:JINDUICHENG MOLYBDENUM CO LTD

Method for recycling copper from acid waste etching solution

The invention discloses a method for recycling copper from an acid waste etching solution. The method is characterized by comprising the following steps that firstly, an organic phase and the acid waste etching solution are subjected to 1-5 levels of extraction according to the volume ratio of 1-30:1, and copper is extracted; secondly, the load organic phase obtained in the first step and purified water are subjected to 1-5 levels of washing according to the volume ratio of 0.1-10:1; thirdly, the load organic phase washed in the second step and a copper sulphate solution including sulfur acid of 130-250 g/L and copper ions of 1-50 g/L are subjected to 1-3 levels of back extraction according to the volume ratio of 1-10:1, the organic phase obtained through back extraction is returned to the first step to be repeatedly used, and a water phase is a copper sulphate solution; fourthly, metal stainless steel 304 or stainless steel 316 or metal titanium is used as a cathode, the copper sulphate solution obtained in the third step is electroplated under the current density of 50-400 A/m<2>, electroplated copper is obtained, and the copper sulphate solution obtained after the copper is electroplated is returned to the third step to be repeatedly used. According to the method for recycling copper from the acid waste etching solution, the copper can be separated selectively from the acid waste etching solution, the technology is simple, and the separation effect is good.
Owner:陈飙

Method for recovering copper from acid waste etching solution

The invention relates to a method for recovering copper from an acid waste etching solution. The method is characterized by comprising the following steps of: (1) preparing an organic phase by adopting an Lix series extraction agent with the volume ratio of 5-20% and 80-90% of kerosene or No. 200 solvent oil; (2) performing copper extraction by using the organic phase and the acid waste etching solution according to the volume ratio of (1-30): 1; (3) washing the loaded organic phase obtained in the step (2) and pure water according to the volume ratio of (0.1-10): 1; (4) performing back extraction by using the loaded organic phase after washing in the step (3) and a copper sulfate solution according to the volume ratio of (1-10): 1, and returning the organic phase after back extraction to the step (2) for reuse, wherein a water phase is the copper sulfate solution; and (5) performing copper electrodeposition on the copper sulfate solution obtained in the step (4), and returning the copper sulfate solution after copper electrodeposition to the step (4) for reuse. According to the method for recovering the copper from the acid waste etching solution, disclosed by the invention, the copper can be selectively separated from the acid waste etching solution, the process is simple and the separation effect is good.
Owner:陈飙

Deoxidation and organic sulfur hydro-conversion bifunctional catalyst, and preparation method and application thereof

The invention relates to a deoxidation and organic sulfur hydro-conversion bifunctional catalyst, and a preparation methods and an application thereof, and belongs to the technical field of gas purification. The catalyst, by oxide, comprises, by mass, 1-50 parts of an active component, 0.1-20 parts of an active assistant and 30-89.1 parts of a carrier. The invention also relates to three preparation methods of the catalyst. The catalyst has deoxidation and organic sulfur hydro-conversion bifunctions, and can be used in the purification process of raw gases of sulfur-containing and CO-and-H2-containing industrial coal-to-water gas, semi-water gas, coke oven gas and carbide furnace gas. The catalyst can simultaneously realize deoxidation and organic sulfur hydro-conversion purposes, shortens the process flow, simplifies the flow, reduces the energy consumption and saves the cost. The preparation methods of the catalyst have the advantages of simplicity, strong operability and low preparation condition requirements. The catalyst has a high deoxidation rate and a high organic sulfur hydro-conversion rate, and allows the volume content of oxygen in an obtained product obtained after deoxidation to be lower than 100ppm and the organic sulfur conversion rate to be greater than 95%.
Owner:HAO HUA CHENGDU TECH

High-purity nickel-based high-temperature alloy and preparation method of spherical powder of high-purity nickel-based high-temperature alloy

The invention discloses a high-purity nickel-based high-temperature alloy and a preparation method of spherical powder of the high-purity nickel-based high-temperature alloy. The alloy comprises the following steps of selecting high-purity metal ingredients, smelting in a vacuum induction suspension smelting furnace, realizing pure smelting by controlling parameters such as smelting vacuum degree, refining temperature, time and the like, then pouring to obtain a steel ingot, and preparing the steel ingot into a bar; carrying out smelting, atomizing and powdering on the bar through EIGA and PREP technologies to obtain spherical metal powder; adopting vibrating screening and airflow classification, and classifying spherical powder under the protection of inert gas. According to the method, the content of nonmetal impurities is effectively controlled through raw material smelting control, atomization process control and post-treatment control, so that chemical elements of the powder have extremely high purity, and the high-purity high-temperature alloy spherical powder is not prone to generating cracks and other defects in the subsequent laser additive printing and laser cladding process and is good in binding force, high in strength, good in toughness and good in mechanical property, and the powder can be used for repairing high-end parts.
Owner:盘星新型合金材料(常州)有限公司

High-altitude municipal wastewater treatment method based on nitrogen and phosphorus capture and whole-course autotrophic nitrogen removal

The Tibet region in China has the characteristics of high altitude, low air oxygen content, large day and night temperature difference and low night temperature, so that a traditional activated sludgeprocess adopted for domestic sewage treatment at present confronts with the problems of low aeration efficiency, high energy consumption, weak functional microorganism activity and the like when being applied to the Tibet region; meanwhile, the treatment of a large amount of residual sludge threatens the ecological environment of the Tibet region. According to the method, a chemical enhanced primary treatment (CEPT) process and an integrated partial nitrosation-anaerobic ammonia oxidation (CPNA) process are combined, so that the capture of carbon and phosphorus in the inlet water and the whole-course autotrophic nitrogen removal under a low-oxygen condition are realized. The captured carbon source is used for producing biogas through anaerobic fermentation, and can supplement heat for a CPNA process under a low-temperature condition. The CEPT-CPNA process has the advantages of low energy consumption and less residual sludge generation, can solve many problems in the traditional method, and belongs to a sustainable sewage treatment process suitable for a high-altitude environment.
Owner:SOUTHEAST UNIV +1

Novel intelligent efficient polymer solution deoxidizing system

A novel intelligent efficient polymer solution deoxidizing system comprises a vacuum pump assembly, a trace oxygen meter, a vacuum system electromagnetic valve, a drying and buffering assembly, a polymer solution deoxidizing assembly, a nitrogen system electromagnetic valve, a nitrogen generator, a system control circuit and a liquid crystal touch screen. The intake end of the vacuum pump assembly is connected with the output end of the trace oxygen meter through a stainless steel pipe. The input end of the trace oxygen meter is connected with one end of the vacuum system electromagnetic valve through a stainless steel pipe, and the other end of the vacuum system electromagnetic valve is connected with the output end of the drying and buffering assembly through a silicone tube; the input end of the drying and buffering assembly is connected with the suction end of the polymer solution deoxidizing assembly; the charge end of the polymer solution deoxidizing assembly is connected with one end of the nitrogen system electromagnetic valve; the other end of the nitrogen system electromagnetic valve is connected with the output end of the nitrogen generator through a stainless steel pipe; a system control circuit is connected with the vacuum pump assembly, the vacuum system electromagnetic valve and the nitrogen system electromagnetic valve through power lines.
Owner:北京东航科仪仪器有限公司

Method for smelting COST-FB2 steel through gas-phase nitriding under negative pressure condition

The invention relates to a method for smelting COST-FB2 steel through gas-phase nitriding under a negative pressure condition. The method comprises the following steps that firstly carbon deep deoxidation is performed under the condition of high vacuum degree, deoxidation is completed after the surface of molten steel is stable and bubbles do not rush out any longer; then an alloy element for promoting nitrogen dissolution is added and completely molten, and then gas-phase nitriding is started; during gas-phase nitriding, nitriding pressure during gas-phase nitriding is calculated by using thermodynamic calculation software Factsage, the molten steel temperature is accurately controlled, and the nitriding time is calculated and determined through the surface area of the molten steel, the volume of the molten steel and the nitrogen balance content; when gas-phase nitriding is about to be completed, the alloy element boron and the volatile manganese are added, then through argon filling,pressurization is performed until the high pressure is reached, pressurization casting is performed under the condition that the nitrogen partial pressure is kept unchanged, the under-pressure stateis kept in the solidification process, vacuum breaking is performed after complete solidification, and a COST-FB2 steel cast ingot which has the content of N being 0.015%-0.03% and the content of O being less than or equal to 0.0035%, is uniform in component and compact in structure is prepared.
Owner:NORTHEASTERN UNIV

Transport vehicle for storing fresh fruits

The invention discloses a transport vehicle for storing fresh fruits. The transport vehicle comprises a head, a body and wheels, a storage box is fixedly connected into the vehicle body; a ventilationopening is formed in the side wall, close to the vehicle head, of the vehicle body. An impeller is rotationally connected to the part, close to the ventilation opening, in the vehicle body; the ventilation opening is in sealed connection with an air inlet pipe of a right-angle structure. The end, away from the ventilation opening, of the air inlet pipe directly faces blades of the impeller, a permanent magnet is fixedly connected to a rotating shaft of the impeller, an electromagnet is electrically connected to the magnetic plate, an air exchange opening is formed in the top of the side, awayfrom the ventilation opening, of the vehicle body, and an oxygen concentration meter is arranged in the air exchange opening in a communicating mode. The transport cart has the advantages that the impellers are driven to rotate through wind pressure generated when the transport cart runs, so that under the action of electromagnetic induction and thermoelectric power, on one hand, gas components are transferred through a magnetic field generated by the electromagnet, and on the other hand, the storage box absorbs heat to keep fruits in a low-oxygen and low-temperature environment, and the respiratory action is reduced.
Owner:刘红亮

A kind of preparation method of sulfur dioxide gas in sugar industry

ActiveCN103569972BAdjustable production volumeLess sublimated sulfurSulfur compoundsCombustionSulfur
The invention relates to a preparation method of a sulfur dioxide gas in a sugar industry. The preparation method concretely comprises the following steps: adding concentrated sulfuric acid and sulphur to a reaction vessel; after material addition is finished, and heating till the reaction is started to generate the sulfur dioxide gas; cooling the generated sulfur dioxide gas to 60-70 DEG C, wherein the mass ratio of the concentrated sulfuric acid to the sulphur is (5-7):1, and the mass concentration of the concentrated sulfuric acid is 93%-98.3%. The method disclosed by the invention can be used for producing the sulfur dioxide gas by oxidizing elemental sulfur by utilizing the concentrated sulfuric acid, can well solve multiple problems of the sulfur dioxide gas used for preparing sugar through the traditional sulphur combustion, and has the advantages that quantity control of the sulfur dioxide gas is easy to control, and sublimed sulfur of the sulfur dioxide gas is little; the generated sulfur dioxide gas is high in purity, low in oxygen content, low in temperature and easy to cool; raw materials are easily obtained and low in cost and the quantity of the used sulphur is remarkably reduced; a device for preparing the sulfur dioxide gas is simple and small in occupied area.
Owner:中粮糖业辽宁有限公司
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