1312results about How to "Improve the bonding strength of the interface" patented technology

The invention discloses a brushing-proof abrasion-proof and erosion-proof ceramic paint, which is characterized by the following: selecting at least one of electric-melting brown corundum, electric-melting subwhite corundum, electric-melting white corundum, carborundum and electric melting mullite with different grain sizes as main material and at least one of compact corundum, electric-melting subwhite corundum, electric-melting white corundum, carborundum, silicon nitride and boron nitride as auxiliary material; using CA50 calcium aluminate cement or pure calcium aluminate cement as binder and nanometer micro-silica powder and active alpha-Al2O3 micropowder as reinforcer; making hyperdrying active high-effective dehydragent, sodium citrate and sodium hexametaphosphate as composite additive; loading in the strength stirrer to stir 12-17min; blending evenly; packing.

The invention belongs to the technical field of composite materials and discloses a high-entropy alloy reinforced aluminum-based composite material and a preparation method thereof. The composite material takes high-entropy alloy as a reinforcing phase and takes aluminum alloy as a base body. The preparation method of the composite material comprises the following steps: packaging high-entropy alloy particles and aluminum alloy powder into a ball milling tank, sealing and mixing the powder for 5-25 hours to obtain a mixed material; packaging the mixed material into a bag; applying a pressure of 5MPa to 15MPa at room temperature to compact the mixed material in the bag to obtain a semi-finished product; putting the compacted semi-finished product into thermal extruding equipment, preheating the semi-finished product to 400-480 DEG C, preheating a mold to 200-400 DEG C, keeping the temperature of the semi-finished product and the mold for 1-3 hours to finish the preheating process, and then performing hot extrusion formation at an extrusion pressure of 5MPa to 15MPa and at an extrusion ratio of 4 to 25 to obtain the high-entropy alloy reinforced aluminum-based composite material.

The invention relates to an in situ nano TiC ceramic particle reinforced aluminum based composite material and a preparation method thereof. According to the invention, an in situ nano TiC ceramic particle reinforced aluminum or aluminum alloy based composite material is prepared by using a combustion synthesis chemical reaction method and a hot-press technology; and the size of the TiC ceramic particle synthesized by an in situ reaction is below 100 nm, and the weight percentage content of the TiC ceramic particle is 3-30. The preparation method comprises the following steps: 1) mixing reactant powder materials in a certain proportion and then making blanks; 2) evenly mixing in a drum-type ball mill and a triturator in turn; 3) pressing at the room temperature so as to form reaction prefabricated blocks; and 4) putting a graphite mould with the prefabricated blocks in a vacuum/atmosphere protected combustion reaction furnace with a hydraulic device and then initiating a combustion reaction, immediately applying an axial pressure of 40+/-5 MPa to the prefabricated blocks once the combustion reaction occurs, and cooling the prefabricated blocks to room temperature along with the furnace after keeping the pressure for 30-40 seconds, so as to synthesize the nano TiC ceramic particle reinforced pure aluminum or aluminum alloy based composite material.

The invention discloses a high-entropy alloy particle reinforced aluminum base composite material and a stirring casting preparation process thereof. The preparation process adopts mechanical alloying to prepare high-entropy alloy powder and screen to obtain high-entropy alloy particles; the high-entropy alloy particles are sealed by adopting an aluminum alloy pipe having the same material with a basal body; the aluminum alloy pipe weighed in a segmented manner is added in the molten basal body; the high-entropy alloy particles are dispersed by a stirring mode; and the high-entropy alloy particle reinforced aluminum base composite material is prepared by a casting process. The high-entropy alloy particles are 0.1-35%; aluminum alloys are 65-99.9%; and the sum of the two is 1. The high-entropy alloy particles in the structure of the prepared composite material are uniformly dispersed; the high-entropy alloy and aluminum alloy interface bonding compatibility is excellent; the strength and the toughness are excellent; the preparation process is simple; the powder has no need to be treated; the cost is low; the stability is good; and the composite material is suitable for large-batch production and standard production, and is excellent in promotion and application prospect.

The invention discloses nano coating method and device based on ultrafast ultrahigh pressure photodynamics effect, belonging to the technical field of material surface. The invention is characterized by embedding or cold welding nanometer metal powder, nanometer nonmetal powder or compound nanometer powder which are precoated on the surface of a metal matrix in the surface layer of the metal matrix by means of laser induction mechanics effect, forming a thick nanometer particle strengthening layer or a coating layer which is called as a nano coating on the surface of the metal matrix, wherein the metal matrix is impacted and strengthened by laser. The device comprises a three-dimensional hexad working platform, a water tank, a clamp, a thermocouple, a coaxial synchronous water sender, a laser beam focusing system, a 45-degree fully-reflecting mirror, a laser beam optimizing system and a nanosecond laser. By the invention, the obtained surface nano coating has firm interface joint with the matrix and the mechanical property on the surface of the metal matrix is remarkably improved. The invention has simple technical process and lower cost, and is easy to realize automation and suitable for large-scale batch production.

The invention discloses an integrated flexible electrode and belongs to the technical field of electrochemical cells. The integrated flexible electrode is composed of three layers which are successively a polymer layer, a graphene layer and an active material layer. According to the invention, the multi-component integrated design is realized. The graphene layer is formed by dispersing and coating graphene onto the polymer layer. The active material layer is formed by coating slurry onto the graphene layer. After drying, the integrated flexible electrode material is obtained. The integrated flexible electrode material has excellent flexibility and tensile strength and is applicable to flexible cells. A preparation method of the integrated flexible electrode is simple and easy to control, can be applied to various electrode materials and has potential application value. Mass and low-cost preparation can be realized.

The invention belongs to the field of fiber material surface metallization treatment and particularly relates to an aramid fiber surface metallization treatment method which takes hypophosphite as reductant and metal salt as the plating solution of the main salt to deposit a metal coating on the surface of aramid fiber through chemical plating. The surface metallization treatment process includes the steps of unoiling, coarsening, sensitizing, activating, carrying out preplating and carrying out chemical plating. Through the metallization treatment method disclosed by the invention, a uniform compact nonporous metal coating can be plated on the surface of the aramid fiber, and therefore the electrical conductivity and the corrosion resistance of the aramid fiber can be improved and the service life of the aramid fiber can be prolonged. The aramid fiber plated with the metal coating can also be used as reinforcement of metal matrix composite material so as to improve the mechanical property of the composite material.

The invention provides a method and a device for preparing high-performance aluminum-base composite material under the action of the pulsed magnetic field with the in situ crystallization method, belonging to the technical field of material preparation. The method comprises the following steps: smelting to synthesize compound material melt at the temperature of 10-200 DEG C higher than the compound material melt liquidus temperature and pouring the compound material melt into a specially-designed crystallizer to make the compound material melt solidify under the action of the pulsed magnetic field. The pulsed magnetic field has the key parameters of the pulse width of 1-500 ms and the amplitude strength of 0.1-50T. The pulsed electromagnetic force is applied to the process of solidifying the compound material melt under the action of the pulsed magnetic field so as to refine the matrix structure and the particle reinforced phase of the compound material at the same time, control the growth of the particle reinforced phase in cluster, increase the bonding strength of the interface of the particle reinforced phase and the matrix and obviously improve the performance of the composite material.

The invention discloses a method for preparing a styrene grafted silicon dioxide superhydrophobic thin film, which comprises: firstly, adding tetraethoxysilane into mixed solution of a catalyst and an alcohol solvent to obtain nano silicon dioxide spheres by reaction; secondly, adding the nano silicon oxide spheres into the alcohol solvent, and adding a silane coupling agent and the catalyst to obtain vinyl modified nano silicon oxide spheres; and finally, adding the vinyl modified nano silicon oxide spheres into a benzene or ketone organic solvent, adding an initiator and a styrene monomer in turn to obtain the styrene grafted silicon dioxide spheres, dispersing the styrene grafted silicon dioxide under ultrasonic waves, and preparing the styrene grafted silicon dioxide by using an organic or inorganic material as a substrate and by a coating method. The preparation process is simple and high in repeatability, the cost is low, and the promotion is more convenient.

The invention discloses powder metallurgy high-speed steel and a preparation method thereof. The method is simpler than the existing powder metallurgy high-speed steel preparation method, steps of high-speed steel mother alloy smelting, atomization for making powder and hot isostatic pressing are omitted, great equipment investment is not needed and the production cost of powder metallurgy high-speed steel is reduced. The impurity content of the powder metallurgy high-speed steel prepared by adopting the method provided by the invention is low and the using performance is excellent. The powder metallurgy high-speed steel provided by the invention is prepared through the steps of 1) preparing powder mixture: weighing raw materials according to set components and proportioning ratio, and mixing and ball-milling the raw materials in a roller-type ball mill to obtain the powder mixture; 2) molding: molding the powder mixture into pressed blanks through cold isostatic pressing; 3) sintering: sintering the pressed blanks in a vacuum or inert gas atmosphere by adopting a hot-pressing sintering technology, heating the pressed blanks to 1100-1250 DEG C during sintering, preserving heat for 30-90 minutes and keeping sintering pressure to be 10-40Mpa; 4) hot forging; 5) heat treatment.

The invention discloses an emulsion type carbon fiber sizing agent containing a nano material. The sizing agent comprises the following components in percentage by mass: 0.1-2% of a main sizing agent, 0.01-1% of a nano material, 0.05-2% of an emulsion agent, 0.05-0.1% of a dispersing agent, 0.15-8% of an organic solvent and 86.9-99.64% of deionized water. The sizing agent has the advantages the interface binding strength with carbon fibers is high and the surface free energy of the sized carbon fibers is no less than 55mN/m.

The invention provides a method for connecting plastic and a metal heterostructure. The method comprises the following steps that S1, laser roughening treatment is conducted on the surface of a to-be-connected metal part, and local protrusions and dents are generated on the surface of the metal part, so that a metallic oxide layer is formed; S2, the metal part subjected to laser roughening treatment and a to-be-connected plastic part are hot-pressed, so that the metal part and the plastic part are bonded together; and S3, out-of-focus laser beams are adopted to penetrate through the plastic part so as to reach the interface between the plastic part and the metal part, and the portion, at the interface, of the plastic part is partially melted. According to the method for connecting the plastic and the metal heterostructure, operation is easy, the mechanical engaging and chemical bonding degree of the plastic and metal is increased through the required local protrusions and dents formed on the surface of the metal part and partial heating and temperature control of the interface, tight bonding of the plastic and the metal at the interface is facilitated, and the interface bonding strength and airtightness of the plastic and the metal heterostructure are improved accordingly.

The invention relates to process method for aramid fiber surface modification that includes the following steps: drying aramid fiber, sealing the dried aramid fiber with gas medium or liquid medium in glass reactor, using gama radial of 60Co irradiating for 12-15 hours, under normal temperature and normal pressure, irradiation dose is 0.1-3000kGy. The invention has the advantages of simple technology, environment protection, high efficiency and suitable for industrial manufacturing.

The invention discloses a preparation method of a SiC/Al composite material. The method comprises the following steps: carrying out ball milling on alumina and/or silicon oxide powder and a dispersant by using a ball milling medium, adding a binder, and continuously carrying out ball milling to obtain a coating slurry, wherein a mass ratio of the powder to the dispersant to water to the ball milling medium to the binder is 1:0.005-0.01:0.1-0.4:2:0.01-0.03; immersing reticulated porous SiC ceramic in the coating slurry for full absorption, centrifuging, and drying; and embedding secondary-coated reticulated porous SiC ceramic into aluminum or aluminum alloy powder, carrying out vacuum pumping heating to fuse the aluminum or aluminum alloy, introducing argon, and carrying out heat insulation and pressure maintenance to obtain the SiC/Al composite material. The SiC/Al composite material obtained through the method is a bicontinuous phase, and the control of an interface structure and an interface reaction is realized through controlling the composition and performances of the coating slurry to realize strong combination between a silicon carbide matrix and the metal Al and uniform continuous distribution in a three dimensional space, so the segregation and the discontinuousness of the silicon carbide reinforcement are avoided, and the performances of the composite material are improved.

The invention relates to the technical field of powder metallurgy and particularly relates to a ceramic part and a production method thereof. The production method comprises (1) mixing granulation: putting ceramic powder into a mixer, heating the ceramic powder, adding a binder into the ceramic powder, carrying out mixing, and carrying out granulation through an extruder to obtain feed, (2) injection molding: placing the feed in an injection molding machine and carrying out injection molding to obtain an injected blank, (3) degreasing: placing the injected blank into an air furnace, carrying out hot degreasing, carrying out heating pre-sintering, carrying out furnace cooling and taking out a blank, and (4) sintering: putting the blank in a sintering furnace, carrying out sintering, and carrying out grinding and polishing to obtain a ceramic part. Through powder injection molding process and final degreasing and high temperature sintering, a fine ceramic part having a complex shape is obtained, the product has high compactness and good uniformity and is obtained by one step molding, the operation and control are simple, product quality is stable, production efficiency is high, a production cost is low and large-scale industrial production is realized.

An aramid fibre/epoxy resin composite interface performance improving method relates to a macromolecule material modification processing method. The invention solves the problems that the interface between the prior Kevlar-49 fibre and the prior epoxy resin has weak combination and the fiber surface modification processing method is not suitable for industrialized production. The Kevlar-49 fibre surface modification processing method of the invention is as follows: firstly the Kevlar-49 fibre is dried, then the dried Kevlar-49 fibre and liquid medium are sealed in a glass reactor; under the condition of normal temperature, normal atmosphere and the protection of protective gas, a gamma ray with <60>Co as radiation source is adopted to radiate; the radiation dosage is between 0.1 and 1000 kGy and the radiation dosage rate is between 3 and 7 kGy/h. The invention has the advantages of simple operation, stable technique, reliable product quality, environmental protection and industrialized production. The method of the invention improves the fibre surface energy, thereby improving the combination intensity of the interface between the fibre and the epoxy resin matrix and exerting the comprehensive performance of Kevlar-49 fiber reinforced composite farthest.

The invention discloses a torpedo tank lining gunning repairing material, a preparation method and applications thereof, wherein the torpedo tank lining gunning repairing material comprises, by weight, 60-67 parts of a Al2O3-containing fireproof material after-using regenerating material, 3-7 parts of fireproof clay, 2-5 parts of flaky graphite, 3-7 parts of silicon carbide, 10-15 parts of an alumina homogeneous material, 3-6 parts of kyanite, 2-5 parts of alpha-Al2O3 micro-powder, 3-11 parts of a binder, and 1.2-3.4 parts of an admixture. According to the present invention, the torpedo tank lining gunning repairing material has characteristics of low raw material cost, wide regeneration material source, convenient cold-hot state gunning repairing, excellent thermal shock stability, strong repairing layer interface bonding strength, strong slag iron corrosion resistance, high torpedo tank operation rate, long service life, and the like.

The invention discloses a SiC-TaC coating/matrix collaborative modified C/C composite material and its preparation method. The composite material provided by the invention comprises two parts. The portion below the surface of the C/C composite material is the matrix modified portion with the thickness being 0.1-10mm. In addition, carbide in the C/C composite material emerges in gradient distribution. The portion which is deposited on the surface of a carbon material is a coating portion with the thickness being 10-300 microns. The preparation method of the composite material comprises the following steps of: cutting a C/C green body at the density of 0.80g/cm<3>-1.60g/cm<3> into an annular shape or a plate shape, followed by ultrasonic cleaning and drying, placing into a multifunctional CVD furnace, depositing carbide on the surface layer and surface of the C/C green body by controlling deposition parameters, further densifying the green body by the use of pyrolytic carbon so as to obtain the high-density coating/matrix collaborative modified C/C composite material. The main advantages of the invention are as follows: by the penetration of carbide through the surface layer of the C/C composite material, the thermal expansion coefficient of the matrix is raised, the interfacial bonding state is improved, a continuous transition of carbide is formed between the coating and the matrix, and the metallurgical bonding is accomplished between the coating and the matrix.