Preparation process and quality control method of inula and ochre soup formula granules
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Embodiment 1
[0089] This example is a preparation process of the formula granules of Xuanfu Daizhe Decoction.
[0090] Raw material formula: Inula 5.0kg, ginseng 3.3kg, ginger 8.4kg, ocher 1.7kg, licorice 5.0kg, pinellia 5.0kg, jujube 5.0kg.
[0091] Preparation process: add water to decoct three times, add 8 times the amount of water to the first decoction, soak for 0.5 hours, and extract for 1 hour; add 8 times the amount of water to the second decoction, extract for 1 hour; liquid, stand still, 4000r / min centrifugal filtration, the filtered water extract is concentrated under reduced pressure to a clear paste with a relative density of 1.05, and mixed evenly. Spray drying at a temperature of 80°C and a feeding speed of 0.4R / min. After adding dextrin, the weight ratio of dextrin to clear paste is 1:2, granulate, and dry below 60°C to make 10kg spin-coated Daizhe soup formula granules.
Embodiment 2
[0093] Raw material formula: Inula 5.0kg, ginseng 3.3kg, ginger 8.4kg, ocher 1.7kg, licorice 5.0kg, pinellia 5.0kg, jujube 5.0kg.
[0094] Preparation process: add water to decoct three times, add 8 times the amount of water to the first decoction, soak for 0.5 hours, and extract for 1 hour; add 8 times the amount of water to the second decoction, extract for 1 hour; solution, let it stand, 4000r / min centrifugal filtration, the filtered water extract is concentrated under reduced pressure to a clear paste with a relative density of 1.05, mixed evenly, when the feed temperature is 55°C, the inlet air temperature is 200°C, and the air outlet Spray drying at a temperature of 100°C and a feeding speed of 0.6 R / min. After adding lactose, the weight ratio of lactose to clear paste is 1:5, granulate, and dry below 60°C to make 10kg of spin-coated ocher soup Formula granules.
Embodiment 3
[0096] Raw material formula: Inula 5.0kg, ginseng 3.3kg, ginger 8.4kg, ocher 1.7kg, licorice 5.0kg, pinellia 5.0kg, jujube 5.0kg.
[0097] Preparation process: add water to decoct three times, add 8 times the amount of water to the first decoction, soak for 0.5 hours, and extract for 1 hour; add 8 times the amount of water to the second decoction, extract for 1 hour; liquid, stand still, 4000r / min centrifugal filtration, the filtered water extract is concentrated under reduced pressure to a clear paste with a relative density of 1.05, and mixed evenly. Spray drying at a temperature of 100°C and a feeding speed of 0.5 R / min. After adding dextrin, the weight ratio of dextrin to clear paste is 1:2, granulate, and dry below 60°C to make 10kg spin-coated Daizhe soup formula granules.
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