Negative electrode for fluoride ion secondary battery, and fluoride ion secondary battery provided with same
A technology of fluoride ion and secondary battery, which is applied in the direction of secondary battery, battery electrode, active material electrode, etc., can solve the problems such as difficult electrochemical reactions, and achieve the effect of large battery capacity
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Embodiment 1、2
[0085] according to Figure 4 The negative electrode for fluoride ion secondary batteries of Examples 1 and 2 was produced by the manufacturing method of the negative electrode for fluoride ion secondary batteries of this embodiment shown. Both Examples 1 and 2 used Li with an average particle size of micrometers (10 μm to 100 μm). 3 AlF 6 with AlF 3 The composite, the fluoride ion-conducting fluoride having an average particle diameter of 0.1 to 100 μm, and the conductive aid having an average particle diameter of 20 to 50 nm. In addition, Li in the negative electrode for fluoride ion secondary battery was 3 AlF 6 with AlF 3 The content of the complex was set to 25% by mass. In addition, in Example 1, LiF and AlF were combined 3 The molar ratio is set to LiF:AlF 3 = 1:1 synthesis of Li 3 AlF 6 with AlF 3 The composite of LiF and AlF in Example 2 3 The molar ratio is set to LiF:AlF 3 = 2:1 synthesis of Li 3 AlF 6 with AlF 3 the complex.
reference example 1
[0089] according to Figure 4 The negative electrode for a fluoride ion secondary battery of the reference example 1 was produced by the manufacturing method of the negative electrode for fluoride ion secondary batteries of this embodiment shown. Specifically, combining LiF with AlF 3 The molar ratio is set to LiF:AlF 3 = 3:1 The negative electrode obtained by synthesis is used as Reference Example 1, which uses Li with an average particle size of micrometers (10 μm to 100 μm). 3 AlF 6 , fluoride ion-conductive fluoride with an average particle size of 0.1 to 100 μm, and a conductive aid with an average particle size of 20 to 50 nm. In addition, Li in the negative electrode for fluoride ion secondary battery 3 AlF 6 content of 25% by mass.
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