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4results about How to "Improve crystal structure" patented technology

Catalyst for preparing acrylic acid and butyl ester using lactic acid method and preparation method thereof

The invention discloses a catalyst used for preparing acrylic acid and butyl ester by the dehydration of butyl lactate and a preparation method thereof. The catalyst is a composite catalyst, comprising a main catalyst A and auxiliary catalysts B, C, D and E, wherein, A is calcium sulphate, B is sulphuric acid, C is phosphate, D is alkaline matter and E is promoter. The preparation method comprises the steps as follows: five compositions A, B, C, D and E are sufficiently mixed, baked for 2-10 hours at the temperature of 200-800DEG C and formed for standby. The catalyst has high catalytic activation; under the catalysis of the catalyst, the molar yield reaches 75.1 percent and the molar selectivity of the acrylic acid and butyl ester reaches 71.5 percent. The preparation method has the advantages that the crystal structure of the main catalyst can be improved so as to be beneficial for carrying out the reaction; and the introduction of different auxiliary catalysts and quantities is helpful to improve the conversion ratio of the raw material and the product selectivity and is beneficial for improving the strength of the catalyst.
Owner:溧阳常大技术转移中心有限公司

Process for the preparation of rare earth metals by electrolysis of oxides in a fluoride system

PendingCN122279684AImprove oxidation resistance and corrosion resistancereduce lossElectrolysisPhosphoric acid
This invention discloses a method for preparing rare earth metals by electrolytic oxides using a fluoride system, belonging to the field of rare earth metal preparation technology. This invention modifies graphite anodes used in rare earth molten salt electrolysis. It improves oxidation and corrosion resistance, reduces anode wear, lowers replacement frequency, and increases production efficiency, yielding high-purity, low-carbon rare earth metal lanthanum. A three-dimensional network framework material is constructed using Prussian blue self-assembly and SiC is deposited to obtain a composite framework material. During pre-calcination with graphite and other materials, the derivatives optimize the crystal structure and interfacial bonding, enhancing the strength of the pre-shaped anode material and ensuring the integrity and performance stability of the electrode structure. Thirdly, the pre-shaped anode material is impregnated with a specific impregnation solution, altering the gas diffusion path and resistance, inhibiting oxidation reactions, and high-temperature sintering generates substances that fill the pores, forming a dense microstructure. Simultaneously, the compounds formed by phosphoric acid enhance cohesion and adhesion, improving oxidation and molten salt corrosion resistance, and extending the service life of the graphite anode.
Owner:BAOTOU XIJUN RARE EARTH

A luminescent composite material, its preparation method and application

PendingCN122080529Areduce interfacial tensiongood compatibilityPolymer scienceButanedioic acid
This invention relates to the field of advanced petrochemical new materials technology, and discloses a luminescent composite material, its preparation method, and its application. The composite material comprises the following components: homopolymer polypropylene, polybutylene succinate, a compatibility modification system, double-modified rare-earth strontium aluminate luminescent powder, dispersant, antioxidant, weathering agent, toughening agent, nucleating agent, and silane coupling agent. This invention employs a compatibility modification system composed of maleic anhydride-grafted PP-g-PBS copolymer and double-modified nano-montmorillonite. The maleic anhydride-grafted PP-g-PBS copolymer constructs a chemical link between the polypropylene and polybutylene succinate molecular chains through a grafting reaction, reducing the interfacial tension between the two resins. The double-modified nano-montmorillonite, after ionic liquid intercalation and silane grafting treatment, exhibits increased interlayer spacing and improved surface activity, uniformly dispersed in the matrix, and acts as a physical crosslinking point, improving the compatibility of the matrix resin and preventing phase separation.
Owner:HUAIYIN INSTITUTE OF TECHNOLOGY

A method for improving the starch structure and digestibility of sprouted corn flour, the sprouted corn flour prepared therefrom, and its applications.

PendingCN122074620AImprove drying efficiencySolve mildewSeed preservation by dryingIn vitro digestionResistant starch
This invention relates to the field of food processing technology, specifically to a method for improving the starch structure and digestibility of sprouted corn flour, the prepared sprouted corn flour, and its applications. A method for improving the starch structure and digestibility of sprouted corn flour includes the following steps: S1, preparation of sprouted corn: soaking and germinating corn kernels to obtain sprouted corn; S2, microwave treatment: subjecting the sprouted corn to microwave treatment; S3, forced-air drying: subjecting the microwave-treated sprouted corn to forced-air drying until constant weight, obtaining dried sprouted corn; S4, pulverization: pulverizing and sieving the dried sprouted corn to obtain sprouted corn flour. This method not only significantly improves the drying efficiency of sprouted corn but also improves the starch structure characteristics of the sprouted corn flour, particularly increasing the content of resistant starch and reducing in vitro digestibility, thereby providing a high-quality raw material for developing corn-based foods with low digestibility or low glycemic index.
Owner:QIQIHAR UNIVERSITY