Bar high-throughput preparation device and use method thereof
A preparation device and high-throughput technology, applied in the field of hot-press sintering, can solve the problems of low preparation efficiency and high preparation cost
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Embodiment 1
[0115] Batch preparation of 23 titanium matrix composite bars of different compositions with a diameter of 30 mm:
[0116] 900g of TC4, TA15, pure Ti and TC18 powder were used, respectively, with different contents of TiB 2 , C powder and TiB 2 +C is used for low-energy ball milling and powder mixing, and the designed composite material system is shown in Table 1.
[0117] Table 1
[0118]
[0119] A 23-hole porous mold with a diameter of 30 mm was designed. The porous mold was placed on the first indenter, and graphite blocks with a diameter of 30 mm and a height of 20 mm were placed in each through hole, and graphite blocks with a size of 350 × 95 mm were placed The paper roll is placed in the through hole, and the ball-milled powder is then loaded into the porous mold. Put a carbon / carbon mold protector on the outside of the porous mold. Protrusions with a diameter of 30 mm and a height of 150 mm were placed on the porous mold. A second indenter with a diameter of 4...
Embodiment 2
[0121] Batch preparation of 7 titanium matrix composite bars of different compositions with a diameter of 70 mm:
[0122] 4.8kg of TC4 and TA15 powders were used, respectively, with different contents of TiB 2 It is mixed with Si powder by low-energy ball milling, and the designed composite material system is shown in Table 2.
[0123] Table 2
[0124] Numbering material system Numbering material system 1 (1vol.%TiB+0.5wt%Si) / TC4 5 (1vol.%TiB+0.5wt%Si) / TA15 2 (3.5vol.%TiB+0.5wt%Si) / TC4 6 (1vol.%TiB+1.0wt%Si) / TA15 3 (1vol.%TiB+1wt%Si) / TC4 7 (1vol.%TiB+2.0wt%Si) / TA15 4 (3.5vol.%TiB+0.5wt%Si) / TC4
[0125] A 7-hole porous mold with a diameter of 70 mm is designed. The porous mold is placed on the first indenter, and graphite blocks with a diameter of 70 mm and a height of 20 mm are placed in each through hole. The paper roll is placed in the through hole, and the ball-milled powder is then loaded into the porous mold. Put...
Embodiment 3
[0127] Batch preparation of 7 titanium matrix composite bars of different diameters, heights and compositions:
[0128] Different quality of TC4 and different content of TiB were used respectively 2 Low-energy ball mill mixing was performed, and the composite material system was designed as shown in Table 3.
[0129] table 3
[0130]
[0131]
[0132] 7-hole porous molds with diameters of 40mm, 50mm and 60mm were designed, and the through-holes were numbered corresponding to the material system in Table 3, 1-3 had a diameter of 60mm, 4 and 5 had a diameter of 50mm, and 6 and 7 had a diameter of 40mm. The porous mold was placed on the first indenter, and a graphite block with a diameter of 60 mm and a height of 20 mm was placed in the through holes No. 1-3, and a graphite paper roll with a size of 190 mm×350 mm was placed. No. 4 and No. 5 through-holes were placed into graphite spacers with diameters of 50 mm and heights of 20 mm and 40 mm, respectively, and graphite pa...
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