Method for preparing block of nano aluminum alloy in ultrahigh strength
An ultra-high-strength, aluminum alloy technology, applied in the field of aluminum alloy and nano-material preparation, can solve the problem of inability to import, and achieve the effects of simple equipment, easy process control, and easy mass production scale.
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Embodiment l
[0030] The alloy composition is 9.9% by weight Zn, 2.9% by weight Mg, 1.9% by weight Cu, 0.1% by weight Zr, 0.1% by weight Ni, and the rest is Al. The alloy material was melted in an induction furnace and heated to 810° C. for 10 minutes to homogenize it. It is degassed by conventional hexachloroethane and sodium fluorosilicate refining, and then cast into pre-alloyed ingots. Put the above pre-alloyed ingot into non-vacuum air atomization equipment. The aluminum alloy powder is produced by heating in an intermediate frequency induction furnace and raising the temperature to 800°C, and refining and degassing with conventional hexachloroethane and sodium fluorosilicate. The atomizing gas is nitrogen, the atomizing pressure is 0.4MPa, and the diameter of the draft tube is 3.1mm.
[0031] A vertical rotor ball mill and stainless steel balls and pots were selected, the ball-to-material ratio was 40:1, the ball milling temperature was -120°C, and Al alloy powder with an average gr...
Embodiment 2
[0033]The alloy composition is 10.2% by weight Zn, 3.1% by weight Mg, 1.9% by weight Cu, 0.1% by weight Zr, 0.1% by weight Ni, and the rest is Al. The alloy material was melted in an induction furnace and heated to 830° C. for 10 minutes to homogenize it. It is degassed by conventional hexachloroethane and sodium fluorosilicate refining, and then cast into pre-alloyed ingots. Put the above pre-alloyed ingot into non-vacuum air atomization equipment. Use medium frequency induction furnace to heat and raise the temperature to 820°C, use conventional hexachloroethane and sodium fluorosilicate to refine and degas to produce aluminum alloy powder. The atomizing gas is nitrogen, the atomizing pressure is 0.5MPa, and the diameter of the draft tube is 3.2mm.
[0034] A vertical rotor ball mill and stainless steel balls and pots were selected, the ball-to-material ratio was 35:1, the ball milling temperature was -140°C, and Al alloy powder with an average grain size of 32nm was forme...
Embodiment 3
[0036] The alloy composition is 10.6% by weight Zn, 2.8% by weight Mg, 2.0% by weight Cu, 0.2% by weight Zr, 0.2% by weight Ni, and the rest is Al. The alloy material was melted in an induction furnace and heated to 840° C. for 10 minutes to homogenize it. It is degassed by conventional hexachloroethane and sodium fluorosilicate refining, and then cast into pre-alloyed ingots. Put the above pre-alloyed ingot into non-vacuum air atomization equipment. The aluminum alloy powder is produced by heating in an intermediate frequency induction furnace and raising the temperature to 840°C, and using conventional hexachloroethane and sodium fluorosilicate for refining and degassing. The atomization gas is argon, the atomization pressure is 0.6MPa, and the diameter of the guide tube is 3.3mm.
[0037] A high-energy horizontal rotor ball mill and stainless steel balls and tanks were selected, the ball-to-material ratio was 50:1, the ball milling temperature was -150°C, and Al alloy pow...
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