Chemical process for the production of 1,3-diglyceride oils
A kind of technology of diglyceride oil and triglyceride, applied in 1 field
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Embodiment 1
[0025] Nusun oil (400 g) was placed in a 1 L round bottom flask and dried by heating the oil to 90° C. under vacuum for 30 minutes. Glycerol (80 g) and NaOH (1 g) were added to the dry oil with vigorous stirring. After reacting at 145° C. for 3 hours, the reaction mixture was cooled, and then the reaction mixture was centrifuged to separate the oil phase from residual glycerin for color measurement. The color of the oil phase was 12.5 red and 70 yellow. The initial Nusun oil colors were 0.8R and 4.1Y.
Embodiment 2
[0027] The same procedure as in Example 1 was adopted, except that the reaction time was 4 hours.
Embodiment 3
[0029] The same procedure as in Example 1 was used, except that the reaction time and temperature were 170° C. and 1 hour, respectively.
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