Method for measuring deuteration rate of single crystal of potassium dideuterium phosphate
A technology of potassium dideuterium phosphate single crystal and deuteration rate, applied in the direction of removing certain components and weighing, can solve the problems of difficult to determine whether the crystal decomposition is complete, the deuteration rate is inaccurate, the method is cumbersome, etc. The effect of easy promotion and use, economic promotion and use, and simple method
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[0013] Example: Put a pair of covered platinum crucibles on a NETZSCH STA449C thermogravimetric analyzer, close the covers, weigh until constant weight, and reset to zero. Put the DKDP crystal sample in the front platinum crucible, close the cover and weigh to constant weight, the reading is 23.9672mg, and then perform the measurement parameters (measurement type, operator, sample number, name, sample quality, heating program, temperature correction , sensitivity correction, etc.) setting, the temperature rise program is that the initial temperature is 30°C, slowly heated to 260°C at a rate of 5°C / min, and then kept at a constant temperature for 1 hour, then slowly heated at a rate of 5°C / min to 450°C, and then kept at a constant temperature for 1 hour Hour. Click "Initialize Working Conditions" to initialize the experimental temperature program first, and then click "Start" to conduct experimental measurements. The real-time curve during the experimental measurement process ...
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