Topical composition for delivery of salicylate esters or salicylate salts
A technology of salicylic acid ester and composition, which is applied in the direction of salicylic acid active ingredient, drug combination, ointment delivery, etc.
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Embodiment 1-14
[0074] The preparation of embodiment 1-14-methyl salicylate ointment
[0075]1. Emulsion Preparation
[0076] A. Oil Phase Preparation: Combine all components except water while mixing and heating with a water bath (50-60° C.) to obtain a clear and transparent solution.
[0077] B. Add hot water (60-90° C.) to the oil phase and obtain a water-in-oil (W / O) type emulsion. The emulsion was mixed for 5-10 minutes using a propeller type mixer. During subsequent cooling, when the temperature drops below the cloud point of the surfactants in the mixture, the emulsion changes its physical structure, transitioning from a W / O emulsion to an O / W emulsion. The results of Examples 1, 2 and 4-7 resulted in the formation of unstable emulsions, whereas the formulations in Examples 3, 8-14 corresponded to stable oil-in-water emulsions. In one embodiment, the ratio between the oil and the salicylate component is optimized with respect to the hydrophilic-lipophilic balance (HLB) of the surf...
Embodiment 15
[0094] Table 3: Ethyl salicylate composition
[0095] oil phase
[0096] Ethyl Salicylate 12%
[0097] Myvacet9-45K 4%
[0098] L-Menthol 6%
[0099] D,L-camphor 6%
[0100] Vitamin E Acetate 4%
[0101] Lecithin S-80 1%
[0102] Ethanol 1%
[0103] Solutol HS-15 4%
[0104] Tocophersolan 4%
[0105] Aqueous phase 58%
[0106] Total 100%
[0107] Emulsion Stability +++
Embodiment 16
[0109] Table 4: Octyl Salicylate (Ethylhexyl Salicylate) Composition
[0110] oil phase
[0111] Octyl Salicylate 10%
[0112] MCT Oil 6%
[0113] L-Menthol 6%
[0114] D,L-camphor 6%
[0115] Vitamin E Acetate 2%
[0116] Lecithin S-80 1%
[0117] Ethanol 1%
[0118] Cremophor RH-40 5%
[0119] Tocophersolan 4%
[0120] Aqueous phase 59%
[0121] Total 100%
[0122] Emulsion Stability ++
[0123] Examples 15 and 16 were prepared in a manner similar to that of Examples 1-14.
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