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Methods and apparatus for chemical-mechanical polishing utilizing low suspended solids polishing compositions

a technology of suspended solids and polishing compositions, which is applied in the direction of grinding machines, manufacturing tools, lapping machines, etc., can solve the problems of adverse effects on the tss level of slurry, achieve the effect of reducing the variability of substrate removal rate and/or defectivity, enhancing the performance characteristics of the substrate polishing process, and desirably improving the polishing

Inactive Publication Date: 2010-06-10
CABOT MICROELECTRONICS CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

[0010]When the TSS level of the low level abrasive slurry is maintained within a tight variance, the performance characteristics of the substrate polishing process are desirably enhanced. For example, the variability in substrate removal rate and / or defectivity desirably can be reduced due to the reduced variability in TSS level. This is particularly pronounced in slurries containing low levels of suspended particulate abrasive material. The tight process control provided by the methods and apparatus of the present invention can lead, for example, to improved polishing productivity, reduced levels of reworking, more predictable substrate throughput, and reduced production costs relative to conventional polishing methods without tight TSS control.

Problems solved by technology

In some cases the slurry TSS level may be adversely affected by insufficient mixing or agitation in the slurry delivery system, in which case the TSS level may be adjusted by changing the mixing parameters or configuration of the slurry delivery system.

Method used

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  • Methods and apparatus for chemical-mechanical polishing utilizing low suspended solids polishing compositions
  • Methods and apparatus for chemical-mechanical polishing utilizing low suspended solids polishing compositions
  • Methods and apparatus for chemical-mechanical polishing utilizing low suspended solids polishing compositions

Examples

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Effect test

example 1

Evaluation of Total Suspended Solids (TSS) Sensor with iDiel™ 6600 Dilution

[0033]This example illustrates a commercial TSS meter sold under the trade name COSMOS-25 XL, available from Rosemont Analytical Inc. (LaHabra, Calif.).

[0034]The purpose of this test was to evaluate the feasibility of monitoring the dilution of a commercial slurry concentrate, iDiel™ 6600 and detecting the suspended solids concentration using an in-line total suspended solids (TSS) meter.

[0035]A dilution evaluation was performed to verify the responses of in-line TSS readings as parts-per-million (ppm) with step-down addition of various volumes of a DI water diluent. The TSS data was collected during 14 different dilution stages. Significant observations made during this evaluation include the observation that the tested TSS sensor had an accuracy range for TSS in the range of about 0.1% to about 6.1% over the TSS range of 0.1 percent by weight to about 0.6 5 percent by weight solids. The variability in repea...

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Abstract

The present invention provides chemical-mechanical polishing (CMP) methods and apparatus suitable for polishing a substrate utilizing a low suspended solids slurry composition. The CMP methods of the invention comprise polishing a substrate with CMP slurry containing a low suspended solids level (e.g., about 0.01 percent by weight to about 1.0 percent by weight) of a particulate abrasive material in a CMP apparatus, while continuously monitoring and accurately maintaining a predetermined total suspended solids (TSS) level in the slurry. Preferably, maximum TSS variability of the slurry is less than about 20 percent (i.e., ±20% of the target TSS level), more preferably less than about 10 percent TSS variability (i.e., ±10% of the target TSS level) during the course of the polishing process.

Description

CROSS-REFERENCE TO RELATED APPLICATIONS[0001]This application claims the benefit of U.S. Provisional Patent Application Ser. No. 61 / 201,001, filed on Dec. 5, 2008, which is incorporated herein by reference.FIELD OF THE INVENTION[0002]This invention relates to polishing methods and apparatus for polishing a substrate. More particularly, this invention relates to chemical-mechanical polishing methods and apparatus utilizing low suspended solids abrasive polishing compositions.BACKGROUND OF THE INVENTION[0003]Compositions and methods for chemical-mechanical polishing (CMP) the surface of a substrate are well known in the art. Polishing compositions (also known as polishing slurries, CMP slurries, and CMP compositions) for polishing metal-containing surfaces of semiconductor substrates (e.g., integrated circuits) typically contain abrasives, various additive compounds, and the like, and frequently are used in combination with an oxidizing agent. Such CMP compositions are often designed ...

Claims

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Application Information

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IPC IPC(8): B24B1/00B24B37/04B24B57/02
CPCB24B57/02B24B37/04
Inventor CHANG, SHEI-KAIMYERS, THEODORE
Owner CABOT MICROELECTRONICS CORP