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Nickel-containing high-toughness controllably degradable magnesium alloy material, preparation method therefor and use thereof

a controllable, high-toughness technology, applied in the field of magnesium alloys, can solve the problems of increasing construction period and cost, affecting the construction efficiency of the project, and the problem of petroleum problems in china, and achieve the effects of reducing the engineering degree of difficulty, improving construction efficiency, and remarkably improving the tensile strength and plasticity of the alloy material

Inactive Publication Date: 2021-02-11
CHONGQING UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The invention provides a magnesium alloy material that has high strength and durability, but can be controlled to degrade over time. This helps to solve problems with existing packing tools made of steel, which can be difficult to drill and mill, and can cost a lot of money. The new material helps to shorten construction times and reduce costs.

Problems solved by technology

With the rapid progress of economy, the petroleum problem in China has become one of the important problems with national concern.
However, most of the existing common packing tools are made of steel, and have the defects of difficult drilling and milling, long-time consumption, difficult removal of powders and fragments after drilling and so on, which greatly increases the construction period and cost.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0103]The present example provides a nickel-containing, high-strength and high-toughness, controllably degradable magnesium alloy material, including following components in percentage by mass: 6.9% of Ni, 18% of Y, and the balance of Mg and unavoidable impurities, wherein Mg, Ni and Y form an Mg12YNi-type long-period stacking ordered phase, an Mg5Y phase and an Mg2Ni phase, a volume fraction of the Mg12YNi-type long-period stacking ordered phase is 66%, a volume fraction of the Mg5Y phase is 4%, and a volume fraction of the Mg2Ni phase is 2%.

[0104]A method for preparing a nickel-containing, high-strength and high-toughness, controllably degradable magnesium alloy material provided in the present example includes following steps:

[0105](1) accurately blending materials according to formula amounts, wherein a nickel source, a yttrium source and a magnesium source are added in forms of magnesium-yttrium alloy and nickel-yttrium alloy, respectively;

[0106](2) casting: smelting using a re...

example 2

[0108]The present example provides a nickel-containing, high-strength and high-toughness, controllably degradable magnesium alloy material, including following components in percentage by mass: 2.3% of Ni, 5.3% of Y, and the balance of Mg and unavoidable impurities, wherein Mg, Ni and Y form an Mg12YNi-type long-period stacking ordered phase, an Mg5Y phase and an Mg2Ni phase, a volume fraction of the Mg12YNi-type long-period stacking ordered phase is 23%, a volume fraction of the Mg5Y phase is 6%, and a volume fraction of the Mg2Ni phase is 1.8%.

[0109]A method for preparing a degradable magnesium alloy material provided in the present example is the same as that of Example 1, and unnecessary details will not be given herein.

example 3

[0110]The present example provides a nickel-containing, high-strength and high-toughness, controllably degradable magnesium alloy material, including following components in percentage by mass: 8.5% of Gd, 4.5% of Y, 0.5% of Ni, 0.8% of Mn, and the balance of Mg and unavoidable impurities, wherein Mg, Gd, Y and Ni form an Mg12YNi-type long-period stacking ordered phase, an Mg12GdNi-type long-period stacking ordered phase, an Mg5Gd phase, an Mg5Y phase and an Mg2Ni phase, and wherein a volume fraction of the two long-period stacking ordered phases is 15%, a volume fraction of the Mg5Gd phase and the Mg5Y phase is 12%, and a volume fraction of the Mg2Ni phase is 1.2%.

[0111]A method for preparing a degradable magnesium alloy material provided in the present example is different from the preparation method provided in Example 1 in that the homogenization treatment is carried out at a temperature of 540° C. for 4 h; the extrusion deformation is carried out at a temperature of 450° C., an...

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Abstract

The present disclosure provides a nickel-containing high-toughness controllably degradable magnesium alloy material, a preparation method therefor and use thereof, and relates to the technical field of magnesium alloys. The magnesium alloy material comprises the following components in percentage by mass: 0.3 to 8.5% of Ni, 0.5 to 28% of RE, with the balance being Mg and unavoidable impurities. RE represents rare earth elements. By adding Ni and RE elements to introduce an Mg12RENi-type long-period phase, an Mg2Ni phase and an MgxREy phase, the magnesium alloy material provided by the present disclosure significantly improves mechanical properties of the alloy material, the tensile strength being up to 510 MPa. At the same time, the presence of the Mg12RENi-type long-period phase and Mg2Ni phase enables the alloy material to be controllably degradable, and enables the degradation rate to be adjustable between 360 and 2400 mm / a. Downhole fracturing tools manufactured by using the magnesium alloy alleviates the technical problem existing in current downhole tools and satisfy the requirements in the field of oil and gas exploitation.

Description

CROSS-REFERENCE TO RELATED APPLICATION[0001]The present disclosure claims priority of Chinese patent application with the filing number 201811237934.1 filed on Oct. 23, 2018 with the Chinese Patent Office, and entitled “Nickel-containing High-toughness Controllably Degradable Magnesium Alloy Material, Preparation Method therefor and Use thereof”, the contents of which are incorporated herein by reference in entirety.TECHNICAL FIELD[0002]The present disclosure relates to the technical field of magnesium alloy, in particular to a nickel-containing, high-strength and high-toughness, controllably degradable magnesium alloy material, a preparation method therefor and use thereof.BACKGROUND ART[0003]With the rapid progress of economy, the petroleum problem in China has become one of the important problems with national concern. According to statistical data of the national statistical bureau, the net petroleum import in China is increasing continuously, and the dependency of petroleum in ...

Claims

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Application Information

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Patent Type & Authority Applications(United States)
IPC IPC(8): C22F1/06C22C23/06C22C1/02B22D7/00
CPCC22F1/06B22D7/005C22C1/02C22C23/06C22C23/00
Inventor WANG, JINGFENGGAO, SHIQINGLIU, SHIJIEWANG, KUIPAN, FUSHENG
Owner CHONGQING UNIV