Etching device using etching chamber
a technology of etching device and etching chamber, which is applied in the manufacture of semiconductor/solid-state devices, basic electric elements, electrical equipment, etc., can solve the problems of vaporization of a portion of the etchant, limited commercial use of dry etching device, and high cost of the device for performing dry etching, so as to improve the product yield, prevent the vaporization of the etchant, and improve the selectivity of etching
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Benefits of technology
Problems solved by technology
Method used
Image
Examples
preparation example 1
n Nitride Film Etchant Composition Containing a Silylphosphine Oxide-Based Compound
[0143](1) Preparation of Silylphosphine Oxide-Based Additive Compound
[0144]A silylphosphine oxide-based compound according to one aspect of the present invention was prepared.
[0145]First, H3PO4 anhydride (100%, 300 g) and Tetra-Ethyl-Ortho-Silicate (TEOS, 99%, 30 g) were mixed, and then, stirred at 60 rpm for 10 minutes to be mixed.
[0146]Next, the mixture was first reacted while being stirred at 60 rpm for 8 hours at a temperature of 60° C.
[0147]Next, after the first reaction was completed, a temperature of a reactor was raised to 120° C., the mixture was stirred at 60 rpm for 12 hours, and the secondary reaction was carried out.
[0148]Next, after the secondary reaction was completed, the temperature of the reactor was raised to 260° C., the mixture was stirred at 60 rpm for 3 hours, and a tertiary reaction was carried out.
[0149]Finally, after the tertiary reaction was completed, the temperature of the...
preparation example 2
d Silicon Nitride Film Etchant
[0152]Preparation of Composition
[0153]Without mixing the (1) silylphosphine oxide-based compound of Preparation Example 1, only phosphoric acid (H3PO4, 85 wt %) and water (H2O, 15.0 wt %) were mixed to prepare the phosphoric acid etchant composition.
preparation example 3
n Nitride Film Etchant Composition Containing Silyl Phosphate-Based Compound
[0154](1) Preparation of Silyl Phosphate-Based Additive Compound
[0155]A silyl phosphate-based compound according to one aspect of the present invention was prepared.
[0156]First, H3PO4 anhydride (100%, 300 g) and Tetra-Ethyl-Ortho-Silicate (TEOS, 99%, 30 g) were mixed, and then, stirred at 60 rpm for 10 minutes to be mixed.
[0157]Next, the mixture was first reacted while being stirred at 60 rpm for 8 hours at a temperature of 80° C.
[0158]Next, after the first reaction was completed, the temperature of the reactor was raised to 120° C., and the mixture was stirred at 60 rpm for 12 hours, and the secondary reaction was carried out.
[0159]Finally, after the secondary reaction was completed, the temperature of the reactor was cooled to room temperature to obtain a silyl phosphate-based compound.
[0160](2) Preparation of Silicon Nitride Film Etchant Composition Containing Silyl Phosphate-Based Compound
[0161]The silyl...
PUM
| Property | Measurement | Unit |
|---|---|---|
| pressure | aaaaa | aaaaa |
| temperature | aaaaa | aaaaa |
| pressure | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More 


