Metallic pigment and coating material containing same
A technology of metallic pigments and covering layers, applied in the direction of multi-color effect coatings, coatings, fibrous fillers, etc., can solve the problems of not having corrosion resistance, not being able to obtain width, hindering the effect of improving the brightness of surface modifiers, and achieving Effects of improving adhesion, improving brightness and corrosion resistance
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Embodiment 1
[0106] First, a metallic pigment paste (trade name: 7640NS, manufactured by Toyo Aluminum Co., Ltd.), which is a paste of aluminum flakes, was washed with mineral spirits and filtered. The non-volatile content of the paste after washing and filtering was 70.0% by mass.
[0107] In a 1-liter separable flask, 599.5 g of mineral spirits were added to 171.4 g of the paste, and stirred to form a slurry. Stirring was continued, nitrogen gas was purged and released into the system to form a nitrogen atmosphere, and then the temperature was raised to 80°C. Unless otherwise specified, the following operations are carried out in accordance with this condition.
[0108] Add 0.85 g of acrylic acid, 8.3 g of epoxidized 1,2-polybutadiene, 9.5 g of trimethylolpropane triacrylate, 3.8 g of divinylbenzene, and azobis Isobutyronitrile (AIBN) 0.67g. After adding the monomer and AIBN, it was allowed to react for 4 hours, then 1.3 g of dimethylaminoethyl methacrylate, 0.6 g of trimethylolpropan...
Embodiment 2
[0116] 3.6 g of the surfactant solution was diluted with 66.0 g of cyclohexanone, added to 70.0 g of the paste obtained in Example 1, and kneaded at room temperature for 20 minutes to obtain a slurry. The obtained slurry was added a little at a time to 1 liter of heptane which had been vigorously stirred, and dispersed. The dispersion liquid was filtered, washed and filtered with heptane, and the resulting cake was spread in a vat and allowed to dry naturally overnight. The dried metallic pigment powder was passed through a sieve with a mesh size of 100 μm to obtain a metallic pigment for powder coating. Then, this metallic pigment is referred to as Pigment C. Table 1 shows the amount (% by mass) of the surface modifier relative to the metallic pigment in Pigment C.
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Abstract
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