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Method for extracting anthocyanin from lunar incense fructification

An anthocyanin and Cinnamomum odorifera technology, applied in the field of extracting anthocyanins, can solve the problems of high price of plant natural pigments, low pigment substance content, difficult extraction, etc., and achieve the effects of high result rate, high purity and low raw material cost.

Inactive Publication Date: 2008-04-16
JIAYING UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The extraction of existing plant pigments mostly uses fruits, vegetables, grains, etc. as raw materials, and the content of pigment substances in plants is low, so the extraction is difficult and requires a long time of extraction, reflux, enzyme treatment, etc., so the price of plant natural pigments expensive

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] 1. Harvesting of yin xiang fruit

[0019] Harvest black and mature Yinxiang fruits in late November or early December, rinse them with deionized water 1-2 times, wash off the dust on the surface of the fruits, remove sundries, rotten fruits, etc., and dry them for later use.

[0020] 2. Pretreatment of Cinnamomum yamba fruit

[0021] (1) Fresh fruit processing. Put the Yinxiang fruit into the pot, add water to submerge the Yinxiang fruit, quickly heat to boil, keep boiling for 10 minutes, take out the fruit, the peel cracks, quickly dissipate heat and cool down, after the fruit temperature drops to room temperature, stir to disintegrate the pulp tissue, The anthocyanins of fragrant fruit were only distributed in the tissues adjacent to the pericarp, and the pulp was separated from the core, but the structure of the core shell was well preserved.

[0022] (2) Dried fruit processing. The dried fruit of Yinxiang is soaked in deionized water with a pH value of 4 for 10 t...

Embodiment 2

[0036] Put the washed yin xiang fruit into the container, add water to submerge, heat and keep boiling for 60 minutes, take out the yin yang fruit, cool down to room temperature, stir the yin yang fruit to separate the pulp from the core; add 1 kg yin yang fruit pulp and fruit core In 1 liter of 60% ethanol aqueous solution or methanol aqueous solution, use acetic acid aqueous solution or sulfuric acid aqueous solution to adjust the pH value of the mixed solution to 5, soak at 50°C for 15 minutes, stir, filter, and collect the filtrate; Recover the alcohol solvent by distillation under reduced pressure at 0.09MPa, reduce the alcohol concentration of the filtrate to 9.5%, take the clear liquid after standing for 4 hours, and obtain the anthocyanin extract of Cinnamomum burmanii; use DA201, DM301, DS401 or DM-18 macroporous adsorption resin absorbs and separates anthocyanins from Cinnamomum burmanii, then elutes them with 30% ethanol aqueous solution or methanol aqueous solution,...

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PUM

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Abstract

The present invention relates to a method for extracting anthocyanin from yin-fragrant fruit, including the following steps: (1) to put the yin-fragrant fruit in a vessel, adding water until submerging the fruit, to heat until boil and take out, to cool until room temperature, to beat so as to make the sarcocarp and fruit stone to separate; (2) to add the yin-fragrant fruit and the fruit stone into alcohol solution, and to regulate the pH value of the mixing liquid, dipping beating, filtering and collecting filtering liquid; (3) to decompress and distill the filtrate so as to recover alcohol solvent, to make the alcohol chroma of the filtrate decrease until 10 percent, then to fetch clear liquid after placing whisht, to obtain yin-fragrant anthocyanin extracting liquid; (4) to absorb and separate the yin-fragrant anthocyanin extracting liquid with big-holes adsorption resin, to wash with alcohol solution, at the same time to collect washing liquid to decompress and dry, to produce powder shape yin-fragrant fruit anthocyanin. The yin-fragrant anthocyanin pigment has high stability, stable anti-oxidation activity and simple technics as well as raw material has low cost.

Description

technical field [0001] The invention relates to a food additive, in particular to a method for extracting anthocyanins from yin xiang fruit. Background technique [0002] Food coloring is an indispensable additive in food, medicine, cosmetics and other industries. Existing food pigments are divided into two categories: synthetic pigments and natural pigments. The use of synthetic pigments seriously affects the safety of food. There have been strict restrictions on the scope and dosage of its use as food additives in the world, and even countries such as Norway It is completely forbidden to be used in food, medicine, etc.; and the synthetic food pigments such as amaranth and carmine that are still allowed to be used in my country will generate carcinogenic β-naphthylamine and α-amino-1-naphthol during metabolism in the human body . Natural pigments originate from nature, are easy to be decomposed in nature, do not accumulate in organisms, generally have no toxic and side effe...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/275A23L1/28A23L1/212A23L5/43A23L33/105A23L33/125
CPCC07H1/08A23L1/2751C09B61/00A23L5/43A23L33/105
Inventor 张镜廖富林黄思梅刁树平
Owner JIAYING UNIV
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