Nano multi-phase high-temperature material
A high-temperature material and nanotechnology, applied in the field of nano-multiphase high-temperature materials, can solve the problems of poor high-temperature stability, insufficient heating temperature, and insufficient anti-oxidation performance, and achieve excellent thermal shock resistance, good high-temperature stability, and high temperature. The effect of infrared radiant energy
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Embodiment 1
[0027] The preparation of the nanocomposite high-temperature ceramic material is carried out according to the main crystal phase: nanoscale yttrium hydroxide and aluminum hydroxide mixture powder = 60%: 40%.
[0028] The main crystal phase is a submicron silicon powder obtained by grinding with a high-energy ball mill.
[0029] Preparation of nanoscale yttrium hydroxide and aluminum hydroxide mixture powder: mix the precursor aluminum nitrate and yttrium nitrate in a molar ratio of 3:5, and add distilled water to fully dissolve it to prepare a mixed solution of yttrium nitrate and aluminum nitrate , add ammonia water to make it precipitate, and after the reaction is complete, it will be dehydrated to become a mixture of nano-scale aluminum hydroxide and yttrium hydroxide, which will be dried to form a mixed powder of aluminum hydroxide and yttrium hydroxide, which can be stored for later use.
[0030] Mix 60 grams of the main crystal phase with 40 grams of nanoscale yttrium hy...
Embodiment 2
[0033] The preparation of the nanocomposite ceramic electric heating material is carried out according to the main crystal phase: nanoscale yttrium hydroxide and aluminum hydroxide mixture powder = 80%: 20%.
[0034] Mix 80 grams of the main crystal phase with 20 grams of nanoscale yttrium hydroxide and aluminum hydroxide mixture powder, granulate, shape, and sinter at a temperature of 1000-1200 ° C to form a nano-composite high-temperature ceramic with electrical properties Material. Coat the two ends of the material with silver paste, and then infiltrate into silver electrodes at 800°C to form a nanocomposite ceramic electrothermal material with electric heating function.
[0035] Detect the electrical properties of the nano-composite ceramic electrothermal material: the resistivity is (50-500)Ω·cm, the heating temperature is 800-900°C, and the temperature coefficient αT is 1000-2000ppm / °C.
Embodiment 3
[0037] The preparation of the nanocomposite ceramic electric heating material is carried out according to the main crystal phase: nanoscale yttrium hydroxide and aluminum hydroxide mixture powder = 70%: 30%.
[0038] Mix 70 grams of the main crystal phase with 30 grams of nanoscale yttrium hydroxide and aluminum hydroxide mixture powder, granulate, shape, and sinter at 1000-1300°C to form nano-composite high-temperature ceramics with electrical properties Material. Coat the two ends of the material with silver paste, and then infiltrate into silver electrodes at 800°C to form a nanocomposite ceramic electrothermal material with electric heating function.
[0039] Detect the electrical properties of its nanocomposite ceramic electric heating material: the resistivity is (0.1-500) Ω·cm, the heating temperature is 800-1000°C, and the temperature coefficient αT is 1000-3000ppm / °C.
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