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Nano multi-phase high-temperature material

A high-temperature material and nanotechnology, applied in the field of nano-multiphase high-temperature materials, can solve the problems of poor high-temperature stability, insufficient heating temperature, and insufficient anti-oxidation performance, and achieve excellent thermal shock resistance, good high-temperature stability, and high temperature. The effect of infrared radiant energy

Inactive Publication Date: 2008-05-21
白伟杰
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The inventive nanoparticle composite material described by this patents does have several benefits compared with existing composites that use harmful chemicals or heavy metals like PTFE (Polytetrafluoroethylene). It doesn't emit any dangerous gases during production but it works well at temperatures above 2000 °C for long periods without losing its effectiveness over time due to factors such as moisture absorption from water vapor transmission through pores within layers inside the composition itself. Additionally, there may be some advantages associated with adding specific elements into the mixture used instead of pure metal powders when making these mixtures.

Problems solved by technology

Technological Problem: Nanotechnology involves creation of structures made from tiny objects within certain dimensions through techniques like chemistry synthesis, molecular dynamics simulations, scanning probe microscope analysis, laser ablation, hydrocracking, etc., where there can exist multiple types of atomic groups such as quantum dots, monolayers, colloidal particles, nanoclustules, and other small subsystems containing these specific atom arrangements. These specialized structures provide unique features including improved mechanical performance compared to regular ones due to their low density and lack of long range order. However, current methods require expensive equipment and involve complicated processes involving complex steps, making them difficult to use commercially.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] The preparation of the nanocomposite high-temperature ceramic material is carried out according to the main crystal phase: nanoscale yttrium hydroxide and aluminum hydroxide mixture powder = 60%: 40%.

[0028] The main crystal phase is a submicron silicon powder obtained by grinding with a high-energy ball mill.

[0029] Preparation of nanoscale yttrium hydroxide and aluminum hydroxide mixture powder: mix the precursor aluminum nitrate and yttrium nitrate in a molar ratio of 3:5, and add distilled water to fully dissolve it to prepare a mixed solution of yttrium nitrate and aluminum nitrate , add ammonia water to make it precipitate, and after the reaction is complete, it will be dehydrated to become a mixture of nano-scale aluminum hydroxide and yttrium hydroxide, which will be dried to form a mixed powder of aluminum hydroxide and yttrium hydroxide, which can be stored for later use.

[0030] Mix 60 grams of the main crystal phase with 40 grams of nanoscale yttrium hy...

Embodiment 2

[0033] The preparation of the nanocomposite ceramic electric heating material is carried out according to the main crystal phase: nanoscale yttrium hydroxide and aluminum hydroxide mixture powder = 80%: 20%.

[0034] Mix 80 grams of the main crystal phase with 20 grams of nanoscale yttrium hydroxide and aluminum hydroxide mixture powder, granulate, shape, and sinter at a temperature of 1000-1200 ° C to form a nano-composite high-temperature ceramic with electrical properties Material. Coat the two ends of the material with silver paste, and then infiltrate into silver electrodes at 800°C to form a nanocomposite ceramic electrothermal material with electric heating function.

[0035] Detect the electrical properties of the nano-composite ceramic electrothermal material: the resistivity is (50-500)Ω·cm, the heating temperature is 800-900°C, and the temperature coefficient αT is 1000-2000ppm / °C.

Embodiment 3

[0037] The preparation of the nanocomposite ceramic electric heating material is carried out according to the main crystal phase: nanoscale yttrium hydroxide and aluminum hydroxide mixture powder = 70%: 30%.

[0038] Mix 70 grams of the main crystal phase with 30 grams of nanoscale yttrium hydroxide and aluminum hydroxide mixture powder, granulate, shape, and sinter at 1000-1300°C to form nano-composite high-temperature ceramics with electrical properties Material. Coat the two ends of the material with silver paste, and then infiltrate into silver electrodes at 800°C to form a nanocomposite ceramic electrothermal material with electric heating function.

[0039] Detect the electrical properties of its nanocomposite ceramic electric heating material: the resistivity is (0.1-500) Ω·cm, the heating temperature is 800-1000°C, and the temperature coefficient αT is 1000-3000ppm / °C.

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Abstract

The invention relates to the technical field of nanometer functional materials and electric heating, in particular to a nanocomposite high-temperature ceramic material and a membrane material. Its components and the weight percentage of the components include 60-80% of the main crystal phase, 20-40% of the mixture powder of nano-scale yttrium hydroxide and aluminum hydroxide, or its components include the main crystal phase, nano-scale hydrogen A mixture powder of yttrium oxide and aluminum hydroxide, a binder phase and an organic solvent. The binder phase is a submicron lead-free glass powder, which is ground from lead-free glass powder through high-energy ball milling equipment. The main crystal phase is submicron powder silicon made by high energy ball milling equipment. The nano-composite high-temperature material of the present invention has the following effects: high heating temperature; raw materials do not contain toxic substances such as lead, mercury, cadmium, hexavalent chromium, polybrominated diphenyl ether, benzene, etc., and are environmentally friendly materials without environmental pollution; Infrared radiation energy and high electric-thermal radiation conversion efficiency; excellent thermal shock resistance.

Description

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Claims

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Application Information

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Owner 白伟杰
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