Preparation of high specific surface area and narrow pore distribution porous carbon material
A high specific surface area, porous carbon material technology, applied to porous carbon materials with narrow pore distribution, with high specific surface area, can solve the problem of poor application effect of porous carbon materials, low specific surface area of porous carbon materials, pore size distribution of activated carbon Inhomogeneity and other problems, to achieve the effect of saving wood and high-quality coal, simple preparation process, and low equipment requirements
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Embodiment 1
[0031]Wash the pine needles and dry them. Under the protection of 99.9% nitrogen, carbonize at 450° C. for 3 hours to obtain carbonized products and tar, then pulverize the carbonized products and screen them with a 35-mesh sieve. Dissolve 2 grams of KOH in a mixed solution of 35 mL of water / ethanol (volume ratio 2.5:1), then add 1 gram of carbonized product to the above system, ultrasonically disperse for 5 minutes, soak for 24 hours, and finally dissolve the solvent at 70°C Evaporate to dryness, then activate the remaining mixture under the protection of inert gas (nitrogen or argon 99.9%) at 800°C for 120 minutes, cool to room temperature naturally, then wash the product with water until the pH value of the washing liquid is close to 8, using 0.1mol / Soak in L dilute hydrochloric acid for 3 hours, then wash with water until the pH value of the washing solution is close to 7, then dry in the air at 100°C for 7 hours, and finally obtain a porous carbon material with a specifi...
Embodiment 2
[0033] The experimental method is the same as in Example 1, except that the amount of the activator KOH is changed to 3 grams, and a porous carbon material is also obtained, and the specific surface area of the material is 1900m 2 / g, the pore size is mainly 1.5 nm.
Embodiment 3
[0035] The experimental method is the same as in Example 1, except that the amount of the activator KOH is changed to 4 grams, and the porous carbon material is obtained equally, and the specific surface area of the material is 2014m 2 / g, the pore size is mainly 1.5 nm.
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