Method for obtaining extract from several frequently seen plants and uses of the extract
A plant extract and extract technology are applied in the directions of plant raw materials, medical preparations containing active ingredients, plant/algae/fungus/moss components, etc., and can solve the problems of high cost of cetriol and difficulty in industrialized production, etc. To achieve the effect of preventing and treating diabetes, easy to obtain and simple preparation process
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Embodiment 1
[0026] Embodiment 1: Preparation 1 of low-purity plant extract
[0027] Plant coarse powder 100kg, reflux extraction with 3 times volume of 90% ethanol three times, combine extracts, concentrate under reduced pressure, use ethyl acetate / water two-phase extraction of 1: 2 (volume / volume), combine water layer, filter, Macroporous resin column (D101 type, domestic) chromatography, gradient elution with distilled water and hydrous ethanol, collect the part containing cetraylol, concentrate and dry under reduced pressure to obtain plant extract (light yellow powder), in which cetraylol The content is 10.1%.
Embodiment 2
[0028] Embodiment 2: the preparation 1 of plant extract of lower purity
[0029] Plant coarse powder 50kg, reflux extraction three times with 90% ethanol 60 ℃ of 3 times of volumes, combine extracts, concentrate to dryness under reduced pressure, use the dichloromethane / water two-phase extraction of 1:1 (volume / volume), combine water layer , filtered, macroporous resin column (D101 type, domestic) column chromatography, gradient elution with distilled water, hydrous ethanol (ethanol: 5%-30%), and each eluent is identified with differential test solution respectively, and the combined positive The eluate from the reaction was concentrated under reduced pressure and dried at 70° C. to obtain a plant extract (slightly yellow powder), in which the content of cetriol reached 27.6%.
Embodiment 3
[0030] Embodiment 3: the preparation 2 of plant extract of lower purity
[0031] Plant meal 60kg, 3 times volume 90% methanol 50 ℃ reflux extraction three times, combine extracts, concentrate to dryness under reduced pressure, use ethyl acetate / water two-phase extraction of 1:1 (volume / volume), combine water layer , filtered, macroporous resin column (MN-200 type, domestic) column chromatography, gradient elution with distilled water, hydrous ethanol (ethanol: 5%-20%), each eluent is identified with differential test solution respectively, merges The eluate showing a positive reaction was concentrated under reduced pressure and dried at 70° C. to obtain a plant extract (slightly yellow powder), wherein the content of cetriol reached 28.2%.
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