Method for preparing black tea essence by taking black tea as raw material and usage of black tea essence obtained thereby as well as in cigarette
A kind of black tea essence, black tea technology, applied in the direction of essential oil/spice, tobacco, application, etc.
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Embodiment 1
[0067] Embodiment 1: prepare Keemun black tea essence of the present invention
[0068] (1) Dry Keemun black tea at a temperature of 90°C for 120 minutes, then crush it into 30 meshes using a pulverizer from Shanghai Dianjiu Traditional Chinese Medicine Machinery Manufacturing Co., Ltd., weigh 25g of 30 mesh Keemun black tea powder and place Add 250mL of absolute ethanol to the simultaneous distillation extraction device sold by Guan Instrument Equipment Co., Ltd., soak for 15 minutes, then heat and reflux extraction at a temperature of 90°C for 3 times, each time for 1h, and combine the extracts for 3 times, using Shanghai Xiyu Electromechanical System The vacuum filtration device sold by Shanghai Kexing Instrument Co., Ltd. was used for suction filtration to obtain the filtrate and tea extraction residue. The filtrate was concentrated to 25 mL at a temperature of 50 ° C and a vacuum of 0.09 MPa using a rotary evaporator sold by Shanghai Kexing Instrument Co., Ltd.
[0069] (...
Embodiment 2
[0073] Embodiment 2: prepare Keemun black tea essence of the present invention
[0074] This embodiment is carried out in the same manner as embodiment 1, except that the following points:
[0075] (1) Dry Keemun black tea at a temperature of 90°C for 150 minutes, then crush it into 30 meshes using a grinder from Shanghai Dianjiu Traditional Chinese Medicine Machinery Manufacturing Co., Ltd., weigh 30g of 30 mesh Keemun black tea powder and place it in simultaneous distillation Add 300mL of absolute ethanol to the extraction device, soak for 10 minutes, then heat and reflux at 90°C for 3 times, each time for 1.5h, combine the 3 extractions, and use a vacuum pump sold by Shanghai Xiyu Electromechanical System Co., Ltd. The filter device was used for suction filtration, and the filtrate was concentrated to 30 mL at a temperature of 45 °C and a vacuum of 0.1 MPa using a rotary evaporator sold by Shanghai Kexing Instrument Co., Ltd.
[0076] (2) Filter the tea extract obtained in...
Embodiment 3
[0080] Embodiment 3: prepare Keemun black tea essence of the present invention
[0081] This embodiment is carried out in the same manner as embodiment 1, except that the following points:
[0082] (1) Dry Keemun black tea at a temperature of 95°C for 120 minutes, then crush it into 30 mesh with a pulverizer from Shanghai Dianjiu Traditional Chinese Medicine Machinery Manufacturing Co., Ltd., weigh 25g of 30 mesh Keemun black tea powder and place it in simultaneous distillation In the extraction device, add 300 mL of ethyl acetate, soak for 10 minutes, then heat and reflux extraction at a temperature of 95 ° C for 3 times, each time for 1 hour, combine the 3 extractions, and use a vacuum filtration device sold by Shanghai Xiyu Electromechanical System Co., Ltd. Suction filtration to obtain the filtrate and tea extract residue, and the filtrate was concentrated to 25 mL using a rotary evaporator sold by Shanghai Kexing Instrument Co., Ltd. at a temperature of 45°C and a vacuum ...
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