Nano bamboo carbon powder and preparation method thereof

A technology of nano-bamboo charcoal and bamboo charcoal powder, which is applied in the field of bamboo charcoal powder and its preparation, and can solve problems such as difficulty in realizing nanometerization, insufficient carbonization and cracking, and affecting the scope of application.

Active Publication Date: 2009-06-10
SHANGHAI ZHONGDA TECHNOLOGY DEVELOPMENT CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are still deficiencies. Because the firing temperature of the earthen kiln is difficult to reach high temperature, generally can only reach more than 800 degrees, and the temperature distribution in the furnace is very uneven, so the carbonization cracking is neither ...

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] The bamboo charcoal fired in the earthen kiln is re-carbonized in an electric furnace with a temperature of 1600°C and a carbonization time of 24 hours. The carbonized and cooled bamboo charcoal is pulverized to a particle size of ≤1.5um with a flat jet mill. Take 5 kg of the carbon powder, add 1 kg of butyl titanate coupling agent TTS, anionic surfactant W-9201 kg, dispersant polyacrylic acid sodium salt W-5111 kg, defoamer SAT0.1 kg, deionized water 92 kg. After mixing evenly, grind it in a two-way rotating ball mill for about 40 hours. The speed of the ball mill is 4500 rpm, dilute with deionized water, and disperse ultrasonically for 5 minutes. Use a laser particle size analyzer to test the particle size. When the diameter of the bamboo carbon powder does not reach less than 300nm, continue grinding in the ball mill until the average particle diameter of bamboo carbon powder particles reaches 60-300nm after testing, and then dry to obtain nano bamboo carbon powder....

Embodiment 2

[0038] Bamboo charcoal fired in an earthen kiln is re-carbonized in an electric furnace with a temperature of 1500°C and a carbonization time of 30 hours. The carbonized bamboo charcoal is crushed to a particle size of ≤1.5um with a flat jet mill, and 20 kg of the carbon powder is taken, 22.2 kg of butyl titanate coupling agent TTOP-12.2 kg, anionic surfactant W-9207 kg, dispersed Agent polyacrylic acid sodium salt W-51113.5 kg, antifoaming agent polysiloxane SAT1 kg, deionized water 66.3 kg, after mixing evenly, grind in a two-way rotating ball mill for about 60 hours, the speed of the ball mill is 4250 rpm, use Dilute with ionized water, disperse by ultrasonic for 5 minutes, test its particle size with a laser particle size analyzer, when the average particle size does not reach less than 300nm. Continue grinding in a ball mill until the average particle size of the bamboo carbon powder reaches 60-300nm after being tested, and then dry to obtain the nanometer bamboo carbon p...

Embodiment 3

[0040] Bamboo charcoal fired in an earthen kiln is re-carbonized in an electric furnace with a temperature of 1300°C and a carbonization time of 38 hours. The carbonized and cooled bamboo charcoal is pulverized to a particle size of ≤1.5um with a flat jet mill. Get 12 kg of this carbon powder, add silane coupling agent A-1721.6 kg, anionic surfactant W-9203 kg, dispersant polyacrylic acid sodium salt W-5112 kg, defoamer SAH-2330.5 kg, deionized water 81 kg Kilogram. After mixing evenly, grind it in a two-way rotating ball mill for about 50 hours. The speed of the ball mill is 4000 rpm, dilute with deionized water, and disperse ultrasonically for 5 minutes. Use a laser particle size analyzer to test its particle size. After testing, the average particle size If it is not less than 300nm, continue to grind in the ball mill until the average particle size of the bamboo carbon powder reaches 60-300nm after being tested, and then dry to obtain the nanometer bamboo carbon powder. ...

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PUM

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Abstract

The invention discloses nanometer bamboo charcoal powder and a preparation method thereof. The method is characterized in that bamboo charcoal baked by an earth kiln is used, then a high-temperature electric box electric furnace is used for carbonization, the carbonization temperature is between 1,200 and 1,600 DEG C, the carbonization time is between 24 and 48 hours, carbide is crushed by a flat fluid jet mill into the particle size which is less than or equal to 1.5 um, and then the carbide, a coupling agent, an anion surfactant, a non-ionic interfacial agent-sodium polyacrylate salt used as a dispersant, a modified polysiloxane defoaming agent, and deionized water are mixed evenly and then are placed in a two-way rotary ball mill for grinding. The rotating speed of the ball mill is between 4,000 and 4,500r/m, and the grinding time is between 48 and 96 hours. A grinding mixture is diluted by the deionized water, is subjected to ultrasonic treatment, and is tested by a laser particle size analyzer (the measurement range is between 3 and 3,000 nm), the particle size and the particle size distribution are measured by a wet method, and the mixture is regarded not to reach the standard when the particle size is more than 300nm. Then the mixture continues to be ground in the ball mill until the average particle size of the mixture reaches 60 to 300 nm through the detection, and then is dried to obtain the nanometer bamboo charcoal powder.

Description

【Technical field】 [0001] The invention belongs to a bamboo carbon powder and a preparation method thereof, in particular to a nanometer bamboo carbon powder and a preparation method thereof. 【Background technique】 [0002] Bamboo is an important forest resource in our country. It grows fast, can become useful in a short period of time, and has strong regeneration ability. It can be successfully afforested once, and can be felled and used sustainably. In the past, bamboo was mainly used to make agricultural tools, fuel, furniture, daily necessities, handicrafts, building materials, flooring and papermaking, etc., with low utilization value. [0003] With the development of science and technology, bamboo charcoal is fired from bamboo in China, which greatly expands its application field. Due to the special structure of bamboo charcoal, its molecular structure is hexagonal, the carbon is dense, the specific gravity is large, the pores are many, and the mineral content is rich....

Claims

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Application Information

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IPC IPC(8): C01B31/02C01B31/08
Inventor 潘跃进吴东来
Owner SHANGHAI ZHONGDA TECHNOLOGY DEVELOPMENT CO LTD
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