Prepreg manufacturing method and prepreg
A prepreg, wetting technology, used in thin material processing, coating, electrical components, etc., can solve the problems of short dipping time, insufficient dipping effect, air trapped in the substrate, etc.
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preparation example Construction
[0053] 1. Preparation of liquid resin composition
[0054] With 85 parts by weight of tetrabromobisphenol A type epoxy resin (EPICOAT 5047 of Japan Epoxy Resins (JapanEpoxy Resins), epoxy equivalent 550), 15 parts by weight of cresol novolac type epoxy resin (cresol novolak type epoxy resin) (EPICLON 690 of Dainippon Ink and Chemicals (Dainippon Ink and Chemicals), epoxy equivalent 210), 2.3 parts by weight of dicyandiamide (dicyandiamide), and 0.1 parts by weight of 2-ethyl-4-methyl Imidazole was dissolved in N,N-dimethylformamide to prepare a liquid resin composition having a non-volatile fraction concentration (by weight) of 55%.
[0055] 2. Fiber substrate
[0056] Long glass fibers (Nitto Boseki, WEA-7628) having a thickness of 0.18 mm and a width of 1000 mm were used.
[0057] 3. Manufacture of prepreg
example 1
[0059] figure 1 The shown apparatus is used to impregnate a fibrous substrate with a liquid resin composition. The following are the specifications and operating conditions of the device:
[0060] (1) Substrate conveying speed: 5m / min.
[0061] (2) Diameter of wetting rollers 11, 12, 13: 300mm.
[0062] (3) The contact length between the dampening rollers 11, 12, 13 and the substrate: 150 mm, respectively.
[0063] (4) Contact time between the dampening rollers 11, 12, 13 and the substrate: 5.4 seconds in total.
[0064] After impregnation, the substrate was thermally dried at 180° C. for 2 minutes in a thermal drying device so that the resin composition content (by weight) in the prepreg was 51%.
example 2
[0066] A prepreg was manufactured using the same method as in Example 1, except that the substrate transport speed was set to 9 m / min, and the total contact time between the dampening rolls 11, 12, 13 and the substrate was 3.0 seconds.
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