Frozen confectionery products
A technology for frozen desserts and products, applied in the fields of frozen desserts, food science, cocoa, etc., can solve the problems of low psychoactive substances and no significant effect on emotional state.
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Embodiment 1
[0029] Example 1: Removal of theobromine and caffeine from cocoa powder
[0030] Cocoa powder with reduced levels of theobromine and caffeine was prepared as follows.
[0031] First, the fat content was determined by removing the fat from standard cocoa powder (typically containing 15% fat) by gasoline extraction. This is because the measurement of theobromine and caffeine by HPLC must be based on completely defatted cocoa powder. Petrol extraction does not remove theobromine or caffeine. The amounts of theobromine and caffeine in the defatted cocoa powder were determined by HPLC analysis to be 22 mg / g and 1.5 mg / g, respectively.
[0032] Another sample from the same cocoa batch was then subjected to Soxhlet extraction with ethanol to remove theobromine and caffeine. A 500ml round bottom flask was filled with approximately 250-300ml of ethanol (96% analytical grade, BDH) and placed in a thermostatic mantle heater in a fume hood. A Soxhlet extractor (Quickfit EX5 / 55 34 / 35) ...
Embodiment 2
[0038] White chocolate suitable for coating ice cream was prepared according to the recipe shown in Table 1. Heat the chocolate to about 45°C.
[0039] Table 1
[0040] Element
[0041] Theobromine, defatted cocoa powder (prepared in Example 1) was mixed into the molten chocolate at two ratios (2% and 10%) to produce two different brown chocolates. Composition and GABA / theobromine / caffeine content are given in Table 2.
[0042] Table 2
[0043] Composition (wt%)
[0044] Coated ice cream stick products were produced using each of these chocolates as follows. Ice cream (-18°C) was supported on a stick and dipped into molten chocolate (45°C) to form a coating. In each case the ratio of coating to ice cream was 12.5 g coating to 34.5 g ice cream. Product A contains 6.1 mg of theobromine and 44 mg of GABA in 47 g of product. Product B contains 1.2 mg of theobromine and 48 mg of GABA in 47 g of product. These amounts are expressed in Table 3 as weight pe...
Embodiment 3
[0049] To further reduce the theobromine and caffeine content of the cocoa powder, the hot extraction described in Example 1 was carried out for two additional seven hour cycles for a total extraction time of 21 hours. The amounts of caffeine and theobromine were determined as described above. Theobromine content was determined to be 0.9mg / g (i.e. less than 3% of the original starting level for standard cocoa powder) and the caffeine content was 0.039mg / g (i.e. less than 4% of the original starting level for standard cocoa powder) .
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