Method for manufacturing polyurethane automobile auxiliary spring
A manufacturing method, polyurethane technology, applied in the direction of coating, etc., can solve the problems of low production efficiency, high mold cost, high labor cost, etc., and achieve the effects of low production cost, simple and practical preparation method, and high production efficiency
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Embodiment 1
[0017] Embodiment 1: wherein every mass part is 100kg
[0018] Step 1: Preparation of polyurethane prepolymer
[0019] Weigh 100 parts by mass of polyethylene adipate diol with a number average molecular weight of 2000, put it into a reaction kettle, heat to 130°C, evacuate until the residual pressure in the kettle is less than 500pa, dehydrate for 3 hours, and cool down to 120°C Finally, put in 19 parts by mass of 1,5-naphthalene diisocyanate, heat up to 130°C and react for half an hour to obtain a prepolymer;
[0020] Step 2: Preparation of chain extender
[0021] Weigh 100 parts by mass of polyethylene adipate diol with a number average molecular weight of 2000 that has been dehydrated, put it into a preparation kettle and keep it warm at 55°C, weigh 10 parts by mass of distilled water, and 10 parts by mass of emulsifier; 500rpm Stir vigorously for 10 minutes and set aside;
[0022] Step 3: Preparation of polyurethane elastomer particles
[0023] Add the prepared prepol...
Embodiment 2
[0032] Embodiment 2: wherein every mass part is 500kg
[0033] Step 1: Preparation of polyurethane prepolymer
[0034] Weigh 100 parts by mass of polyethylene adipate diol with a number average molecular weight of 2000, and put it into a reaction kettle. Heat to 130°C, evacuate until the residual pressure in the kettle is less than 500pa, dehydrate for 3 hours, cool down to 120°C, add 25 parts by mass of 1,5-naphthalene diisocyanate, raise the temperature to 130°C and react for half an hour to obtain the prepolymer .
[0035] Step 2: Preparation of chain extender
[0036] Weigh 100 parts by mass of polyethylene adipate diol with a number average molecular weight of 2000 that has been dehydrated, put it into a preparation kettle and keep it warm at 55°C, weigh 10 parts by mass of distilled water, and 10 parts by mass of emulsifier; 500rpm Stir vigorously for 10 minutes and set aside.
[0037] Step 3: Preparation of polyurethane elastomer particles
[0038] Put the prepared...
Embodiment 3
[0047] Embodiment 3: wherein every mass part is 200kg
[0048] Step 1: Preparation of polyurethane prepolymer
[0049] Weigh 100 parts by mass of polyhexanediol adipate diol with a number average molecular weight of 2000, and put it into a reaction kettle. Heat to 130°C, evacuate until the residual pressure in the kettle is less than 500pa, dehydrate for 3 hours, cool down to 70°C, add 30 parts by mass of 3,3'-dimethyl-4,4'-biphenyl diisocyanate, and heat up to React at 100°C for 2 hours to obtain the prepolymer.
[0050] Step 2: Preparation of chain extender
[0051] Weigh 100 parts by mass of polyhexanediol adipate diol with a number average molecular weight of 2000 that has been dehydrated, put it into a preparation kettle and keep it warm at 55°C, weigh 10 parts by mass of distilled water, and 10 parts by mass of emulsifier; 500rpm Stir vigorously for 10 minutes and set aside.
[0052] Step 3: Preparation of polyurethane elastomer particles
[0053] Put the prepared p...
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Abstract
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