Propylene/alpha-olefin block interpolymers
A technology of olefin block and block copolymer, which is applied in the field of propylene/α-olefin block interpolymer, and can solve the problems of unrealized block copolymer.
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Embodiment 2
[0310] Metallocene-catalyzed:
[0311] This example illustrates the calculation of composition values for propylene-ethylene copolymers prepared using metallocene catalysts synthesized according to Example 15 of USP 5,616,664. A propylene-ethylene copolymer was made according to Example 1 of US Patent Application 2003 / 0204017. The propylene-ethylene copolymer was analyzed as follows. Use the corresponding to 100.4MHz 13 Data were collected with a Varian UNITY Plus 400 MHz NMR spectrometer at the C resonance frequency. Acquisition parameters were chosen to ensure quantitative 13 C data acquisition. Data were acquired using the following conditions: gated 1H decoupling, 4000 transients per number-average file, 7sec pulse repetition delay, spectral width of 24,200Hz and file size of 32K data points, with the probe tip heated to 130°C. Samples were prepared by adding approximately 3 mL of a 50 / 50 mixture of tetrachloroethane-d2 / o-dichlorobenzene (relaxation agent) at 0.025 ...
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