Grain refining method for AZ31 magnesium alloy
A technology of grain refinement and alloying, which is applied in the field of metal smelting, can solve the problems of no grain refiner and refinement process, and achieve the effects of low cost, simple operation and high production efficiency
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Embodiment 1
[0029] (1) Smelting AZ31 alloy;
[0030] (2) The Fe content in the AZ31 melt obtained in the determination step (1) is 0.002%, and the Mn content is 0.003%;
[0031] (3) According to the detection result of step (2), the Al-20Mn master alloy is added in the melt obtained in step (1), so that the mass percentage of Mn is 0.1%;
[0032] (4) Keep warm at 720°C for 30 minutes to fully diffuse Fe and Mn in the melt;
[0033] (5) After the melt is refined, degassed and poured, an AZ31 alloy ingot with fine equiaxed grains can be obtained.
[0034] Grain size analysis indicated that the ingot grain size was 140 μm.
Embodiment 2
[0036] (1) Smelting AZ31 alloy;
[0037] (2) The Fe content in the AZ31 melt obtained in the determination step (1) is 0.008%, and the Mn content is 0.01%;
[0038] (3) According to the detection result of step (2), the Al-20Mn master alloy is added in the melt obtained in step (1), so that the mass percentage of Mn is 0.25%;
[0039] (4) Keep warm at 710°C for 25 minutes to fully diffuse Fe and Mn in the melt;
[0040] (5) After the melt is refined, degassed and poured, an AZ31 alloy ingot with fine equiaxed grains can be obtained.
[0041] Grain size analysis indicated that the ingot grain size was 210 μm.
Embodiment 3
[0043] (1) Smelting AZ31 alloy;
[0044] (2) The Fe content in the AZ31 melt obtained in the measurement step (1) is 0.01%, and the Mn content is 0.25%;
[0045] (3) According to the detection result of step (2), the Al-20Mn master alloy is added in the melt obtained in step (1), so that the mass percentage of Mn is 0.2%;
[0046] (4) Keep warm at 730°C for 20 minutes to fully diffuse Fe and Mn in the melt;
[0047] (5) After the melt is refined, degassed and poured, an AZ31 alloy ingot with fine equiaxed grains can be obtained.
[0048] Grain size analysis indicated that the ingot grain size was 160 μm.
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