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Method for preparing aventurine fluoride-free opal glass

A technology of opaque glass and Venus glass, applied in the field of preparation of Venus fluorine-free opaque glass, can solve the problems of chronic poisoning, environmental pollution, volatilization of fluoride, etc., and achieve the effect of soft color and luster

Inactive Publication Date: 2011-11-23
WUHAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the process of raw material processing, melting forming, processing, etc., fluoride dust volatiles cause environmental pollution, and at the same time, fluoride can also cause acute and chronic poisoning to humans, so the use of fluoride has been restricted
Although fluoride opacified glass has the advantages of fast grain growth, but in its production process, there are problems such as difficult control of grain growth and environmental pollution caused by fluoride volatilization.
[0004] At present, sodium fluorosilicate is expensive in the market, resulting in a shortage of raw materials for the manufacture of fluoride opacified glass products and an increase in costs

Method used

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  • Method for preparing aventurine fluoride-free opal glass
  • Method for preparing aventurine fluoride-free opal glass
  • Method for preparing aventurine fluoride-free opal glass

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A preparation method of Jinxing fluorine-free opacified glass, it comprises the steps:

[0020] 1) selection of raw materials: the basic composition scope of the Venus fluorine-free opacified glass used in the present invention is shown in Table 1:

[0021] Table 1 (number of parts by mass)

[0022]

[0023] Calculate the ingredients based on the content of the components in Table 1, and obtain the ingredient list. Use mineral raw materials and chemical raw materials to introduce various oxides, weigh and mix them to obtain glass batches. The glass raw material ingredient list is shown in Table 2.

[0024] Table 2 glass raw material ingredient list

[0025] raw material

Purity (%)

Dosage

SiO 2

98.5

76.14

Al 2 o 3

99.5

0.503

CaCO 3

98.5

14.503

MgCO 3

99.0

4.245

Na 2 CO 3

98.5

17.01

P 2 o 5

99.5

2.51

h 3 BO 3 ...

Embodiment 2

[0032] A preparation method of Jinxing fluorine-free opacified glass, it comprises the steps:

[0033] 1) Selection of raw materials: the basic composition range of the Venus fluorine-free opacified glass used in the present invention is shown in Table 3:

[0034] Table 3 (number of parts by mass)

[0035]

[0036]

[0037] Calculate the ingredients based on the content of the components in Table 3, and obtain the ingredient list. Use mineral raw materials and chemical raw materials to introduce various oxides, weigh and mix them to obtain glass batches. The list of glass raw material ingredients is shown in Table 4.

[0038] Table 4 glass raw material ingredient list

[0039] raw material

Purity (%)

Dosage

SiO 2

98.5

70.71

al 2 o 3

99.5

0.503

CaCO 3

98.5

16.316

MgCO 3

99.0

4.245

Na 2 CO 3

98.5

20.829

P 2 o 5

99.5

2.51

...

Embodiment 3

[0046] A preparation method of Jinxing fluorine-free opacified glass, it comprises the steps:

[0047] 1) selection of raw materials: the basic composition range of the Venus fluorine-free opacified glass used in the present invention is shown in Table 5:

[0048] Table 5 (number of parts by mass)

[0049]

[0050] Calculate the ingredients based on the content of the components in Table 5 to obtain the ingredient list, introduce various oxides with mineral raw materials and chemical raw materials, weigh and mix them to obtain glass batch materials. The glass raw material ingredient list is shown in Table 6.

[0051] Table 6 glass raw material ingredient list

[0052] raw material

Purity (%)

Dosage

SiO 2

98.5

66.50

Al 2 o 3

99.5

1.761

CaCO 3

98.5

16.316

MgCO 3

99.0

5.094

Na 2 CO 3

98.5

20.829

P 2 o 5

99.5

2.51

h 3 BO...

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Abstract

The invention relates to a method for preparing aventurine fluoride-free opal glass. The method for preparing aventurine fluoride-free opal glass is characterized by comprising the following steps: 1) carrying out burden calculation on the ingredient contents of oxides so as to obtain a charger sheet, introducing various oxides respectively by using raw mineral materials and raw chemical materials, and weighing and mixing the oxides so as to obtain a glass batch; 2) putting the glass batch obtained in the step 1) into a horseshoe flame glass smelting kiln to carry out smelting, then enabling the obtained product to enter a cooling part, wherein the temperature of the cooling part is controlled between 1300 DEG C and 1350 DEG C; 3) uniformly adding aventurine frits with the particle size of 1-15 mm into the cooling part so as to obtain a glass flow with aventurines; and 4) enabling the glass flow with aventurines obtained in the step 3) to flow to a forming machine arranged at the lower part of the horseshoe flame glass smelting kiln by a feed channel connected with the cooling part of the horseshoe flame glass smelting kiln, thereby obtaining the aventurine fluoride-free opal glass. The aventurine fluoride-free opal glass prepared by using the method disclosed by the invention not only has the characteristics of opal glass, but also has small plate crystals, therefore, the aventurine fluoride-free opal glass is sparkling.

Description

technical field [0001] The invention relates to a preparation method of Jinxing fluorine-free opacified glass. Background technique [0002] The opacified glass mainly includes fluoride opacified glass, phosphate opacified glass, oxide opacified glass, and phase-separated opacified glass. Due to its special optical properties and decorative properties, opal glass is widely used in instrumentation, architectural lighting, medical equipment, arts and crafts decoration, daily utensils, antique white porcelain bottles, art, etc. Compared with transparent glass, opal glass Turbid glass has the characteristics of soft color, high cleanliness and elegance. In recent years, the application of opacity glass has become more and more extensive, and the production scale is also gradually expanding, showing a good market development prospect. [0003] The mechanism of glass opacification mainly includes crystal grain opacification, phase separation opacification, unmelted particle opac...

Claims

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Application Information

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IPC IPC(8): C03C3/097
Inventor 何峰程金树谢俊
Owner WUHAN UNIV OF TECH
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