A kind of preparation method of rose fragrance type leather

A technology of rose fragrance and rose essence, applied in leather impregnation, small raw hide/large raw hide/leather/fur treatment, small raw hide/large raw hide/leather hide/fur chemical treatment, etc., can solve uneven surface, color spots, etc. problem, to improve the slow release effect, reduce leather odor, and achieve the effect of round and pleasant aroma

Inactive Publication Date: 2011-12-07
SHANGHAI INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional leather flavoring is to directly spray the essence on the surface of the finished leather, but it is easy to cause defects such as uneven surface and stains

Method used

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  • A kind of preparation method of rose fragrance type leather
  • A kind of preparation method of rose fragrance type leather
  • A kind of preparation method of rose fragrance type leather

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0014] The rose essence capsules used in the examples of the present invention are nano rose essence capsule emulsions with an average particle size of 91 nm and a particle size distribution coefficient of 0.034. The preparation method (see patent: 201010147881.1) includes the following steps:

[0015] First, add 0.4 parts by weight of rose essence and 2.0 parts by weight of Tween 20 in the beaker, mix and stir fully at a speed of 1100r / min for 5 minutes, and slowly add deionized water to the beaker, and continue at the same speed Stir until the emulsion is uniform;

[0016] Then, under magnetic stirring, slowly add 1 mol / L hydrochloric acid solution dropwise to adjust the pH value of the system to 2.0, then slowly add 0.8 parts by weight of n-butyl cyanoacrylate (BCA), stir while dropping, drop Complete, close the bottle mouth, keep stirring to make it fully polymerized, stop the reaction after 2 hours, adjust the pH value of the system to 7.0 with 1 mol / L sodium hydroxide so...

Embodiment 1

[0025] A preparation method of rose-scented leather, comprising the following preparation steps:

[0026] (1) After retanning, dyeing and fatliquoring the leather, control the mass ratio of leather to water, i.e. m 皮革 :m 水 Carry out rehumidification treatment at a ratio of 1:7.5, at a temperature of 30°C and a rotational speed of 600 r / min, rehumidify for 6 hours to obtain system 1;

[0027] The leather is cowhide;

[0028] (2), adjust the pH of the system 1 obtained in step (1) to 5 with a sodium bicarbonate solution with a mass fraction of 0.5%, then add rose essence capsules to control the mass ratio of rose essence capsules to leather, namely m 香精 :m 皮革 The ratio is 3:1 to obtain system 2. Heat system 2 to 40°C and rotate at 800 r / min. After perfuming for 9 hours, take out the perfumed leather and dry it in a naturally ventilated place to obtain a rose-scented leather. .

[0029] A kind of rose fragrance type leather of above-mentioned gained, after measuring essence ...

Embodiment 2

[0031] A preparation method of rose-scented leather, comprising the following preparation steps:

[0032] (1) After retanning, dyeing and fatliquoring the leather, control the mass ratio of leather to water, i.e. m 皮革 :m 水 Perform rehumidification treatment at a ratio of 1:9, at a temperature of 35°C and a rotational speed of 800 r / min, rehumidify for 7 hours to obtain system 1;

[0033] The leather is cowhide;

[0034] (2), adjust the pH of the system 1 obtained in step (1) to 6 with a sodium bicarbonate solution with a mass fraction of 0.5%, then add rose essence capsules to control the mass ratio of rose essence capsules to leather, namely m 香精 :m 皮革 The ratio is 5:1 to obtain system 2. Heat system 2 to 50°C and rotate at 1000 r / min. After perfuming for 8 hours, take out the perfumed leather and dry it in a naturally ventilated place to obtain a rose-scented leather. .

[0035] A kind of rose-scented leather obtained above has a fragrance utilization rate of 27.50% aft...

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Abstract

The invention discloses a method for preparing rose-flavored leather. The leather after retanning, dyeing and fatliquoring is subjected to rehumidification treatment at a mass ratio of m leather:m water of 1:7.5-10, and the rotating speed is 600-800 r/min. , when the temperature is 30-40°C, rehumidify for 6-8 hours; use sodium bicarbonate solution to adjust the pH of the system to 5-7, then add rose essence capsules, and the mass ratio is m essence: m leather is 3-8:1, Finally, the temperature of the system is raised to 40-60°C. When the rotation speed is 600-1200r/min, after perfuming for 6-9 hours, the perfumed leather is taken out and dried in a naturally ventilated place to obtain a rose-scented leather. The fragrance utilization rate of the rose-flavored leather prepared by the invention is 34.92%. The rose-flavored leather has a pleasant fragrance and a remarkable rose fragrance. After being placed for 40 days, it still has an obvious rose fragrance and has good fragrance slow-release properties.

Description

technical field [0001] The invention relates to a rose-flavored leather and a preparation method thereof, in particular to a preparation method of a rose-flavored leather processed by a wet processing technique. Background technique [0002] The leather industry is closely related to people's lives. In recent years, aromatic leather has become one of the development trends of functional leather. Combining fragrance with leather is an effective means to improve product grade and added value, and it is also the common demand of consumers and the leather industry. Aromatic leather has a pleasant aroma and high grade. It can be used in automobile cushion leather, sofa leather, clothing leather, luggage leather and other products, and has an extremely broad market. Rose essence is an important additive that is deeply loved by consumers. It is currently mainly used in daily consumer goods such as textiles and leather, and plays a vital role in the quality of end products. The tr...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C14C9/00
Inventor 胡静肖作兵周如隽邓维钧牛云蔚朱建才王明熙李臻马双双
Owner SHANGHAI INST OF TECH
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