O-salicylic acid esterified oligo-chitosan salicylaldehyde Schiff base bacteriostatic agent and preparation method thereof
A technology of polychitosan water and oligochitosan, which is applied in the field of natural antibacterial agent-O-salicylated chitosan salicylaldehyde Schiff base and its preparation, can solve the problem of low antibacterial activity and no inhibition To achieve the effect of improved antibacterial performance, simple operation, and safe operating environment
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[0027] Dissolve 2.0 g of chitosan oligosaccharides with a relative molecular weight of 5000 in 60 ml of 2% by volume acetic acid solution, place in a three-necked flask equipped with a stirrer; add 60 ml of methanol, mix well and then swell for 1 h. Add the aldehyde (-CHO / -NH) dissolved in 60ml methanol to the reaction system 2 The molar ratio was 8:1), and the reaction was stirred at room temperature for 24h.
[0028] Take out the reaction solution, add dropwise 10wt% NaOH solution to adjust the pH value to be neutral, wash with 180ml acetone each time, filter 3 times; then use 180ml 5wt% NaHCO 3 The solution was soaked and stirred at room temperature for 100 minutes, filtered, and then washed with deionized water repeatedly until neutral. Finally soaked in methanol overnight, filtered and vacuum-dried at 40° C. to constant weight to obtain the oligomeric chitosan salicylaldehyde Schiff base, whose Schiff base substitution degree was 100 mol% by elemental analysis.
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