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Traditional Chinese medicinal composition Qinpi Jiegu Capsules and quality detection method of preparations of composition

A composition and capsule technology, applied in the field of medicine, can solve the problems of inaccurate product quality detection of Qinpi Jiegu capsule preparations, quality standards need to be improved, etc., and achieve the effects of product quality safety, quality control, and analysis time saving.

Active Publication Date: 2012-07-25
JINKE TIBETAN MEDICINE QINGHAI PROV
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  • Abstract
  • Description
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AI Technical Summary

Problems solved by technology

Therefore, the product quality inspection of Qinpi Jiegu Capsule preparation is not accurate, and the quality standard needs to be improved

Method used

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  • Traditional Chinese medicinal composition Qinpi Jiegu Capsules and quality detection method of preparations of composition
  • Traditional Chinese medicinal composition Qinpi Jiegu Capsules and quality detection method of preparations of composition
  • Traditional Chinese medicinal composition Qinpi Jiegu Capsules and quality detection method of preparations of composition

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Experimental program
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Effect test

Embodiment 1

[0194] Embodiment 1: quality detection method

[0195] Identification:

[0196] A. Identification of Qin Pi:

[0197] Take 5g of the content of Qinpi Jiegu Capsules, a traditional Chinese medicine composition, add 20ml of petroleum ether with a boiling range of 30-60°C, ultrasonically treat for 10min, discard the petroleum ether, evaporate the dregs, add 1ml of 1mol / L hydrochloric acid solution and 30ml of ethyl acetate , sonicated for 30min, filtered, the filtrate was evaporated to dryness, and the residue was dissolved by adding 2ml of methanol, which was used as the test solution; take 1g of the reference medicinal material of Qinpi, and prepare the reference medicinal solution in the same way as the preparation of the test solution; according to thin-layer chromatography (Chinese Pharmacopoeia 2010 edition one appendix VIB) test, draw each 5 μ l of above-mentioned two kinds of solutions, point respectively on the same silica gel G thin-layer chromatographic plate, be 8: 6...

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Abstract

The invention discloses a traditional Chinese medicinal composition, Qinpi Jiegu Capsules, and a quality detection method of a preparation of the composition, belonging to the technical field of medicine. The existing traditional Chinese medicinal composition, Qinpi Jiegu Capsules, and the quality standards of the preparations of the composition are improved, the identification method of ash bark is improved on the basis of the existing standard, and an identification method of Pyrethrum tatsienense is added. The method is used for measuring the contents of aesculin and aesculetin in the ash bark at the same time under a same mobile phase, and a method for measuring the content of sipeimine in Fritillaria cirrhosa in the preparations is added, so as to further ensure safe, uniform, stable and controllable product quality and ensure the clinic curative effect of the composition and the administration safety of patients.

Description

technical field [0001] The invention relates to a quality detection method of a traditional Chinese medicine composition, in particular to a quality detection method of the Chinese medicine composition Qinpi Jiegu Capsule and its preparation, and belongs to the technical field of medicine. Background technique [0002] Qinpi Jiegu Capsule is the exclusive dosage form product of Qinghai Jinhe Tibetan Medicine Pharmaceutical Co., Ltd., which is included in the National Compilation of Chinese Patent Medicine Standards, Department of Orthopedics and Traumatology, standard number: WS-10901(ZD-0901)-2002-2011Z. Qinpi Jiegu Capsules preparation is made of medicinal materials in the following weight ratio: 113.0g of Qinpi, 80.0g of Chuanxi Feverfew Chrysanthemum, 57.0g of keel, and 80.0g of Chuan Fritillaria. The traditional preparation method of Qinpi Jiegu Capsules is as follows: take the prescribed amount of Qinpi, Western Sichuan Feverfew Chrysanthemum, keel, and Chuan Fritillar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90G01N30/88
Inventor 张义智王海苹江玉娟魏永义杨文钰
Owner JINKE TIBETAN MEDICINE QINGHAI PROV
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