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Forming method of curtain coating flim and device thereof and solution film preparing method

A technology of solution film making and casting film, applied in the direction of flat products, household appliances, other household appliances, etc., can solve the problem of uneven optical properties, and achieve the effect of suppressing uneven thickness

Inactive Publication Date: 2012-09-26
FUJIFILM CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] However, although it is possible to improve the production efficiency of the film by using the method of Japanese Patent Laid-Open No. 2006-306059, the optical characteristics (in-plane retardation Re or thickness direction retardation Rth, etc.) unevenness becomes a problem

Method used

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  • Forming method of curtain coating flim and device thereof and solution film preparing method
  • Forming method of curtain coating flim and device thereof and solution film preparing method
  • Forming method of curtain coating flim and device thereof and solution film preparing method

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Experimental program
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Embodiment

[0247] (Experiments 1~8)

[0248] Experiments 1 to 8 were carried out according to the following method. Regarding the details of each experiment, Experiment 1 will be described in detail, and the description of the same parts as Experiment 1 will be omitted for Experiments 2 to 8, and the different parts will be described.

[0249] (experiment 1)

[0250] The formulations of the compounds used to prepare the dope 24 are shown below.

[0251] The solid content will be constituted according to the following composition ratio, namely

[0252] Cellulose triacetate (degree of substitution 2.86) 100 parts by mass,

[0253] 10 parts by mass of triphenyl phosphate (TPP),

[0254] Delustering agent (AEROSIL R972) 0.03 parts by mass

[0255] Appropriately added to a mixed solvent composed of the following, and stirred and dissolved to prepare a dope 24, that is,

[0256] 80 parts by mass of dichloromethane,

[0257] Methanol 13.5 parts by mass,

[0258] 6.5 parts by mass of n-b...

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PUM

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Abstract

The invention provides a forming method of a curtain coating film and a device thereof and a solution film preparing method. The curtain coating film forming procedure includes a condensed solution flowing procedure, a curtain coating procedure, a film heating procedure, a surface layer forming procedure, a film drying procedure, a film cooling procedure, a ripping procedure and a support body heating procedure repeatedly and successively. In the condensed solution flowing procedure, the condensed liquid flows to an annular band. In the film heating procedure, a curtain coating film is formed from the condensed liquid. The surface of the film is made smooth through the heating the curtain coating film in the film heating procedure. The surface layer is formed on the film surface of the surface forming procedure. The curtain coating film is dried in the film drying procedure. The curtain coating film is cooled into a state capable of conveying independently in the film cooling procedure. The curtain coating film is ripped from the annular band in the ripping procedure. The annular band is heated in the support body heating procedure after the ripping procedure.

Description

technical field [0001] The invention relates to a casting film forming method and device and a solution film forming method. Background technique [0002] A polymer film (hereinafter referred to as a film) is widely used as an optical film because of its excellent translucency, flexibility, and light-weight thin film. Among them, cellulose ester-based films using cellulose acylate and the like are used in optical films. The optical film is typified by a photosensitive film, and there are a protective film for a polarizing plate, a retardation film, and the like. A protective film or retardation film for a polarizing plate is a component of a liquid crystal display device whose market has been expanding in recent years. [0003] As a method for producing a membrane, there is a solution membrane-forming method. The solution film forming method has a cast film forming step, a film independent step, a peeling step, and a wet film drying step. In the cast film forming step, a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J5/18
CPCB29C41/10B29C41/28B29D7/01C08J5/18C08L2203/16
Inventor 中村直贵铃木绅由
Owner FUJIFILM CORP