Preparation method of magnetic peach gum
A peach gum and magnetic technology, applied in the field of preparation of magnetic peach gum, to achieve good magnetic properties and adsorption properties, good application prospects, and easy-to-obtain raw materials
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Embodiment 1
[0018] (1) Wash 5 grams of raw peach gum, remove impurities and add it to 100 milliliters of deionized water for soaking to make it fully swell, then use a beater to beat it into a slurry, and then put it in a condition where the pH is 11 Heated to 85°C under low temperature and stirred for 5 hours to obtain peach gum aqueous solution;
[0019] (2) add ferric chloride and ferrous chloride to the peach gum aqueous solution that step (1) makes, make the concentration of ferric chloride be 1 mol / liter, make the concentration of ferrous chloride be 0.5 mol / liter, Stir for 30 minutes to obtain an aqueous solution of peach gum containing iron salt;
[0020] (3) drop the peach gum aqueous solution containing iron salt that step (2) makes into 50 milliliters of concentrations and be in the aqueous ammonia solution of 8 mol / liter, promptly make magnetic peach gum.
Embodiment 2
[0022] (1) Clean 0.5 gram of raw peach gum, remove impurities and add it to 20 milliliters of deionized water for soaking to make it fully swell, then use a beater to beat it into a slurry, and then put it under the condition that the pH is 14 Heated to 95°C under low temperature, and stirred for 0.5 hours to obtain an aqueous solution of peach gum;
[0023] (2) add ferric chloride and ferrous sulfate in the peach gum aqueous solution that step (1) makes, make the concentration of ferric chloride be 0.1 mol / liter, make the concentration of ferrous chloride be 0.05 mol / liter , stirred for 2 minutes to obtain an aqueous solution of peach gum containing iron salt;
[0024] (3) the peach gum aqueous solution that step (2) makes contains iron salt is dripped in the sodium hydroxide aqueous solution that 5 milliliters of concentrations are 10 mol / liter, promptly makes magnetic peach gum.
Embodiment 3
[0026] (1) Clean 4 grams of raw peach gum, remove impurities and add it to 100 milliliters of deionized water for soaking to make it fully swell, then use a beater to beat it into a slurry, and then put it in the condition that the pH is 9 Heated to 70°C under low temperature and stirred for 6 hours to obtain peach gum aqueous solution;
[0027] (2) add ferric nitrate and ferrous gluconate in the peach gum aqueous solution that step (1) makes, make the concentration of ferric nitrate be 1 mol / liter, make the concentration of ferrous gluconate be 0.05 mol / liter, stir 120 Minutes, make the peach gum aqueous solution that contains iron salt;
[0028] (3) the peach gum aqueous solution that step (2) makes contains iron salt is dripped in the potassium hydroxide aqueous solution that 40 milliliters of concentrations are 0.2 mol / liter, promptly makes magnetic peach gum.
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