Method for preparing silk feather protein powder for preparation of protein filament
A technology of feather protein powder and feather protein, which is applied to the preparation method of peptide, single-component protein rayon, chemical instruments and methods, etc., can solve the problems of potential safety hazards, complicated procedures, and large amino acid damage in feather powder. Achieve the effect of high product quality, simple process and convenient industrial scale production
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Embodiment 1
[0028] Take 500g of feather powder (commercially available chicken feather, duck feather, goose feather), crush the feather powder through a 20-mesh sieve, then take the feather powder and send it to the batching kettle, according to the quality of the feather powder (kg): 1% dilute The ratio of the volume (L) of hydrochloric acid aqueous solution is 1:10, pump dilute hydrochloric acid aqueous solution into the batching kettle, stir and mix evenly, soak for 6 hours, and separate the supernatant (this liquid can be used to supplement the next batch of soaked feathers Powder), get feather powder after acid leaching.
[0029] Feather powder after acid leaching is sent into another batching kettle, and a silicate aqueous solution with a mass concentration of 3% is pumped into the batching kettle (the mass of feather powder after acid leaching (kg) and the volume of silicate aqueous solution (L ) ratio of 1:8. The aqueous silicate solution is a mixture of sodium silicate and potass...
Embodiment 2
[0036] Take 500g of feather powder (commercially available chicken feather, duck feather, goose feather), crush the feather powder through a 40-mesh sieve, then take the feather powder and send it to the batching kettle, according to the quality of the feather powder (kg): the mass fraction is 1% The volume (L) ratio of the dilute hydrochloric acid aqueous solution is 1:10. Pump the dilute hydrochloric acid aqueous solution into the batching tank, stir and mix evenly, soak for 6 hours, and separate the supernatant to obtain the feather powder after acid leaching.
[0037] Feather powder after acid leaching is sent into another batching kettle, and a silicate aqueous solution with a mass concentration of 3% is pumped into the batching kettle (the mass of feather powder after acid leaching (kg) and the volume of silicate aqueous solution (L ) ratio of 1:12. The aqueous silicate solution is a mixture of sodium silicate and potassium silicate, wherein the mass ratio of sodium silic...
Embodiment 3
[0044] Get 500g of feather powder (commercially available chicken feathers, duck feathers, and goose feathers), pulverize the feather powder through a 20-mesh sieve, then get the feather powder and send it into the batching kettle, according to the quality (kg) of the feather powder: 1% dilute The ratio of the volume (L) of hydrochloric acid aqueous solution is 1:10, pump dilute hydrochloric acid aqueous solution into the batching tank, stir and mix evenly, soak for 6 hours, and separate the supernatant to obtain feather powder after acid leaching.
[0045] Feather powder after acid leaching is sent into another batching kettle, and a silicate aqueous solution with a mass concentration of 3% is pumped into the batching kettle (the mass of feather powder after acid leaching (kg) and the volume of silicate aqueous solution (L ) ratio of 1:15. The aqueous silicate solution is a mixture of sodium silicate and potassium silicate, wherein the mass ratio of sodium silicate to potassiu...
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