Sialon phosphor, method for producing same, and light-emitting device package using same
A technology of light-emitting device and phosphor, applied in the field of Sailun phosphor, which can solve problems such as low efficiency
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example 1
[0117] Silicon nitride (Si 3 N 4) and aluminum nitride (AlN) were used as silicon and aluminum precursors, respectively. Using a blender and a sieve, 9.6624 g of Si 3 N 4 Mixed with 0.3376 g of AlN and compacted into a BN crucible located in a piezo furnace. For sintering, the electric furnace was heated to 500°C under vacuum, and N was supplied at 500°C 2 gas. By raising the temperature from 500°C to 2050°C at 10°C / min and maintaining an air pressure of 0.9Mpa or higher, at N 2 The mixture will be sintered at 2050° C. for 5 hours under a gas atmosphere. Then, the mixture was cooled and the crucible was removed from the electric furnace. Grinding The obtained first sintered body was ground and passed through a 100-mesh sieve.
[0118] 10 g of the first sintered body and 0.1324 g of europium oxide (Eu 2 o 3 )mix. By raising the temperature from 500°C to 1900°C at 10°C / min and maintaining an air pressure of 0.9Mpa or higher, at N 2 The mixture was sintered at 1900° C...
example 2
[0120] In addition to using 9.6624g of Si 3 N 4 , 0.3376g of AlN and 0.1324g of Eu 2 o 3 And a β-sialon phosphor was prepared in the same manner as Example 1 except that the second sintering was performed at 1800°C.
example 3
[0122] In addition to using 9.6624g of Si 3 N 4 , 0.3376g of AlN and 0.1324g of Eu 2 o 3 And a β-sialon phosphor was prepared in the same manner as Example 1 except that the second sintering was performed at 1500°C.
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