Tin double-layer coating on the surface of a tool and mold material and preparation method thereof
A tool and mold, double-layer technology, applied in the field of materials, can solve the problems of poor coating effect, wear and scratch, and affect the effect, and achieve the effect of small friction coefficient, smooth surface and easy operation
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Embodiment 1
[0037] The AIP-01 multi-arc ion coating machine is used, manufactured by Shenyang Yuankehang Company. The magnetic filter device inside the coating machine is manufactured by the Institute of Low Energy Nuclear Physics of Beijing Normal University. The workpiece used is wire-cut into 10mm×10mm ×4mm block material (M2 steel);
[0038] (1) Firstly, after the workpiece is mechanically ground and polished, it is cleaned with ultrasonic waves in acetone and alcohol for 15 minutes each, and then dried;
[0039] (2) Put the dried workpiece into the multi-arc ion coating machine, the sample is facing the target source, 150mm away from the target surface, the sample revolves / rotates, and then vacuumizes step by step with a mechanical pump, Roots pump, and diffusion pump to 6.5×10 -3 Pa, the temperature is controlled at 200-230°C, the bias voltage is -700V, and the duty cycle is 40%; the single arc target source is started, the current is 70A, and the voltage is 25V; 5min;
[0040] (...
Embodiment 2
[0046] The difference between this embodiment and embodiment 1 lies in that the coating time in step (4) is 60 minutes.
[0047] The thickness of the coating is measured by grinding the cross-sectional metallographic sample of the workpiece in Example 2, and measuring it under a scanning electron microscope (SEM). The total thickness of the coating is about 2.35 μm.
Embodiment 3
[0049] The difference between this embodiment and Embodiment 1 is that the workpiece is a cemented carbide milling insert of the brand YW1 produced by Zhuzhou Diamond Cutting Tool Co., Ltd.
[0050] The coating of this embodiment is the same as that of Embodiment 1, and the total thickness is about 2.1 μm.
[0051] The surface roughness of embodiment 1~3 and comparative example 1 and 2 adopts BMTExpert3D surface topography instrument to measure, and the test of membrane base binding force uses NHT / MST / AFM / type multifunctional nano-mechanical testing system (instrument model is OpenPIatformtab, supply The manufacturer is Swiss CSM Instrument Co., Ltd.), the equipment is suitable for the thickness of the film layer within the range of 0-1mm; the loading force range is 0.05-30N, the loading resolution is 0.3mN; the scratch speed is 0.4-600mm / min; the indenter It is a diamond indenter with a cone angle of 120° and a tip radius R=0.1mm.
[0052] The measurement parameters of the ...
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