Glass-ceramic plate for industrial protection and preparation method thereof

A technology of glass ceramics and industrial protection, which is applied in the field of glass ceramic plates and its preparation, can solve the problems that the performance of glass-ceramic materials is not enough for industrial protection, and the composition of the microcrystalline phase of the basic glass system has not been informed, so as to ensure Product quality stability, the effect of realizing industrial scale production

Active Publication Date: 2015-10-28
ZHEJIANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0008] Although the above-mentioned patents have informed the method of preparing wear-resistant and corrosion-resistant glass-ceramic materials, they have not informed the basic glass system and the phase composition of the microcrystalline phase, nor have they adopted continuous calendering in production, and the final prepared The performance of glass-ceramic materials is also insufficient for industrial protection

Method used

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  • Glass-ceramic plate for industrial protection and preparation method thereof
  • Glass-ceramic plate for industrial protection and preparation method thereof
  • Glass-ceramic plate for industrial protection and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0045] Embodiment 1, a kind of preparation method of industrial protective glass-ceramic plate, carries out following steps successively:

[0046] 1), according to CaO-MgO-Al 2 o 3 -SiO 2 System requirements (matching of raw material components during batching), so that the basic compound components in the raw materials reach the following weight percentages:

[0047] SiO 2 55%, MgO8%, CaO13%, Al 2 o 3 8%, FeO3%, Na 2 O+K 2 O3% (ie, Na 2 O is 0.5%, K 2 O is 2.5%), CaF 2 7%, TiO 2 3%.

[0048] Choose about 40 parts of iron tailings, about 5 parts of dolomite, about 40 parts of quartz sand, about 5 parts of potassium feldspar, about 7 parts of fluorite, and about 3 parts of titanium dioxide as raw materials, so as to ensure the The composition of the compound satisfies the above weight percentage.

[0049] 2) Fully mix the raw materials evenly, place them in a glass melting furnace and heat them to 1480-1500°C for 3 hours, put them into a clarification tank at 1500-...

Embodiment 2

[0053] Embodiment 2, a kind of preparation method of industrial protective glass-ceramic plate, carries out following steps successively:

[0054] 1), according to CaO-MgO-Al 2 o 3 -SiO 2 System requirements (matching of raw material components during batching), so that the basic compound components in the raw materials reach the following weight percentages:

[0055] SiO 2 52%, MgO8%, CaO12%, Al 2 o 3 10%, FeO5%, Na 2 O+K 2 O4% (i.e. Na 2 O is 1%, K 2 O is 3%), CaF 2 6%, TiO 2 3%.

[0056] Choose about 50 parts of iron tailings, about 5 parts of dolomite, about 30 parts of quartz sand, about 5 parts of potassium feldspar, about 7 parts of fluorite, and about 3 parts of titanium dioxide as raw materials, so as to ensure the The composition of the compound satisfies the above weight percentage.

[0057] 2) Fully mix the raw materials evenly, heat them in a glass melting furnace to 1480-1500°C for 3 hours, put them into a clarification tank at 1500-1550°C for 2 hour...

Embodiment 3

[0061] Embodiment 3, a kind of preparation method of industrial protective glass-ceramic plate, carries out following steps successively:

[0062] 1), according to CaO-MgO-Al 2 o 3 -SiO 2 System requirements (matching of raw material components during batching), so that the basic compound components in the raw materials reach the following weight percentages:

[0063] SiO 2 50%, MgO10%, CaO14%, Al 2 o 3 8%, FeO3%, Na 2 O+K 2 O4% (i.e. Na 2 O is 0.5%, K 2 O is 3.5%), CaF 2 8%, TiO 2 3%.

[0064] About 40 parts of iron tailings, about 10 parts of dolomite, about 31 parts of quartz sand, about 8 parts of potassium feldspar, about 8 parts of fluorite, and about 3 parts of titanium dioxide are used as raw materials to ensure the The composition of the compound satisfies the above weight percentage.

[0065] 2) Fully mix the raw materials evenly, heat them in a glass melting furnace to 1480-1500°C for 3 hours, put them into a clarification tank at 1500-1550°C for 2 hour...

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Abstract

The invention discloses a glass ceramic board for industrial protection and a preparation method thereof. The preparation method comprises the following steps: 1) preparing raw materials according to requirements of the system CaO-MgO-Al2O3-SiO2 and allowing the raw materials to comprise the basic compound components consisting of, by weight, 50 to 55% of SiO2, 8 to 10% of MgO, 12 to 14% of CaO, 8 to 10% of Al2O3, 3 to 5% of FeO, 2 to 4% of Na2O and K2O, 6 to 8% of CaF2 and 3% of TiO2; 2) uniformly mixing the raw materials and carrying out melting and homogenization so as to obtain glass liquid; 3) subjecting the glass liquid to continuous calendering molding and annealing; 4) directly sending an annealed glass plate to a nucleation and crystallization furnace on line for nucleation and crystallization; and 5) and subjecting a glass ceramic plate having undergone nucleation and crystallization to on-line cutting and cooling to room temperature so as to obtain the glass ceramic board for industrial protection.

Description

technical field [0001] The invention relates to the technical field of industrial protective materials, in particular to a wear-resistant and corrosion-resistant glass ceramic plate and a preparation method thereof. Background technique [0002] Iron and steel, coal, electric power, chemical industry, papermaking, building materials and other industries are the pillar industries of our country. The transportation and storage of raw materials and products in these industries require protection of related equipment and devices. For example, blast furnace mixing bins, sintering bins, feeders, ball machines, etc. in the iron and steel industry; gangue bins, medium barrels, scraper machines, bucket elevators, chutes, and under-screen funnels in the coal industry need to add a layer Wear-resistant linings; coal unloading trenches, coal hoppers, furnace front bins, dry coal grids, dumpers, slag extractors, water treatment, etc. in the power generation industry; anti-corrosion groun...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C10/08
Inventor 郭兴忠杨辉盛建松王长林温计格
Owner ZHEJIANG UNIV
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