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Trace uranium sample pretreatment equipment

A sample pretreatment and trace uranium technology, applied in the preparation of test samples, analysis materials, instruments, etc., can solve the problems that affect the analysis speed and effect, many operation steps, and difficult operation

Active Publication Date: 2015-03-11
CHINA INSTITUTE OF ATOMIC ENERGY
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Problems solved by technology

[0004] However, the measurement of trace uranium by time-resolved fluorescence method is significantly affected by interfering ions in the solution. In the post-processing application, the sample needs to be pre-treated by solvent extraction.
The process of sample pretreatment by solvent extraction has many steps, and almost every step is a quantitative operation. Therefore, it is difficult to operate in the glove box and the processing time is long. The analysis time of a single sample is about 40 minutes. The processed sample system is not stable. Unification, which directly affects the analysis speed and effect

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Embodiment Construction

[0022] The technical solutions in the embodiments of the present invention will be clearly and completely described below in conjunction with the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of them. Based on the implementation manners in the present invention, all other implementation manners obtained by persons of ordinary skill in the art without making creative efforts belong to the scope of protection of the present invention.

[0023] In time-resolved fluorescence, trace uranium samples need to be pretreated to pre-separate interfering ions. Therefore, the trace uranium sample pretreatment device and the trace uranium sample pretreatment method of the present invention can be used instead of manual methods to perform the pretreatment. In the present invention, the trace uranium sample to be pretreated is adsorbed on the trace uranium sample adsorb...

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Abstract

The invention provides trace uranium sample pretreatment equipment which comprises a sample conveying device, a washing device and a soaking solution applying device, wherein the sample conveying device is used for conveying at least one trace uranium sample adsorbate on which a trace uranium sample is adsorbed; the washing device is used for washing the at least one trace uranium sample adsorbate conveyed through the sample conveying device; the soaking solution applying device is used for applying a soaking solution into the washed trace uranium sample adsorbate so as to leach the trace uranium sample from the trace uranium sample adsorbate. According to the trace uranium sample pretreatment equipment provided by the embodiment of the invention, the trace uranium sample analysis efficiency is improved, the working amount of operators is alleviated, the working efficiency in trace uranium sample pretreatment is improved, and the great practical significance in large-scale sample analysis and timing control is achieved.

Description

technical field [0001] The invention relates to the technical field of trace uranium sample pretreatment, in particular to trace uranium sample pretreatment equipment. Background technique [0002] The analysis of trace uranium is one of the important contents in the determination of uranium content, such as tailings and waste liquid in uranium ore hydrometallurgy, tailings and tail gas in uranium conversion, waste liquid and waste organic phase in post-treatment process, The content of trace uranium in purified water and other materials in the treatment of three wastes is a reflection of process efficiency and product recovery rate. The analysis of trace uranium runs through all links of the entire nuclear fuel cycle. The uranium content of water and soil in environmental samples belongs to the range of trace uranium. The analysis of trace uranium is a daily analysis item, especially for the environmental monitoring of rare earth mines and nuclear facilities. A large number...

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N35/02G01N1/28
Inventor 梁靓吴继宗苏涛谈树苹郑维明余辉
Owner CHINA INSTITUTE OF ATOMIC ENERGY