A kind of epoxy anticorrosion coating modified by chlorine-containing polymer and preparation method thereof
A technology of epoxy anti-corrosion coatings and polymers, which is applied in the direction of anti-corrosion coatings, epoxy resin coatings, coatings, etc., to achieve the effects of improved stability, good impact resistance and simple process
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[0048] The preparation of the chlorine-containing polymer used in the embodiment: first use acetylene as raw material to produce the waste liquid of trichlorethylene to carry out low-temperature distillation at 55oC, nitrogen purging removes volatile matter, the low-temperature distillate obtained is carried out high-temperature distillation at 180oC, removes High-temperature distillate, keep the residual components, that is.
[0049] Various auxiliary agents used in the embodiment are commercially purchased. DMP-30 (K-54) tertiary amine curing accelerator, Changzhou Yijia New Material Technology Co., Ltd. Silicone defoamer, Jinan Guobang Chemical Co., Ltd. anionic surfactant Elementis FA601 dispersant, Xiamen Kangdilong Trading Co., Ltd. Polyether modified polydimethylsiloxane leveling agent BYK-331, Dongguan Heli Chemical Trading Co., Ltd. Silane coupling agent KH-550 is available from Guangzhou Daoer Chemical Co., Ltd.
Embodiment 1
[0051] 35 parts of E51 type epoxy resin, 15 parts of chlorine-containing polymer, 20 parts of functional filler (1:1:1 mass ratio combination of sericite powder, talc powder and barium sulfate), 12 parts of anti-rust pigment mica iron oxide , through grinding, high-speed dispersion, and filtration to obtain the main component of the resin;
[0052] Mix 15 parts of cashew nut shell oil modified amine as a crosslinking agent and 2 parts of auxiliary agent to obtain the curing agent component. The auxiliary agent is the following combination: 0.5 part of DMP-30 (K-54) tertiary amine curing accelerator, silicone Foaming agent 0.2 parts, anionic surfactant Elementis FA601 dispersant 0.5 parts, polyether modified polydimethylsiloxane leveling agent BYK-331, 0.3 parts; silane coupling agent KH-550, 0.5 parts .
[0053] Mix the resin main agent and curing agent in a ratio of 10:1, and add 30wt% diluent cardanol glycidyl ether, and spray or brush it on the surface of the substrate to ...
Embodiment 2
[0055] 45 parts of low-molecular epoxy resin, 15 parts of chlorine-containing polymer, 15 parts of functional filler (1:1.5:1 mass ratio combination of sericite powder, talc powder, and barium sulfate), 10 parts of anti-rust pigment micaceous iron oxide , through grinding, high-speed dispersion, and filtration to obtain the resin main component; 12 parts of the cross-linking agent cashew nut shell oil modified amine, and 3 parts of auxiliary agents (the composition ratio is the same as that of Example 1) were mixed evenly to obtain the curing agent component. Mix the resin main agent and curing agent in a ratio of 9:1, and the spraying method is the same as that in Example 1.
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