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A refractory material for the cooling section of CDQ coke oven and its preparation method

A technology for CDQ coke ovens and refractory materials, applied in the field of refractory materials and their preparation, can solve the problems of high cost of brick silicon carbide, difficulty in applying refractory materials in the cooling section, and easy cracking, so as to improve wear resistance and save maintenance Time and production cost reduction effects

Active Publication Date: 2016-03-16
武汉钢铁有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Similarly, the brick silicon carbide of this invention has high cost, and metal aluminum is easy to generate gas and crack easily, so it is difficult to apply to the refractory material in the cooling section.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] A refractory material for the cooling section of CDQ ovens, the raw material composition and weight percentage are: 30% of homogenized bauxite with a particle size of 5-1mm; 25% of mullite with a particle size of 3-1mm; corundum 5% with a particle size of 3-1mm %, 3% of andalusite with a particle size not exceeding 0.1mm, 10% of corundum powder with a particle size of ≤0.088mm, 15% of mullite powder with a particle size of ≤0.088mm, 1% of superfine kaolin powder with a particle size of ≤0.01mm, and silicon carbide with a particle size of ≤1mm 7% powder, 3% ferrosilicon powder with 60% silicon, 1% carbon black with plastic fixed carbon content of 70%, plus organic silicon solution accounting for 3% of the total weight percentage of the above raw materials.

[0038] Preparation steps:

[0039]1) First mix 30% of homogenized bauxite with a particle size of 5~1mm; 25% of mullite with a particle size of 3~1mm; 5% of corundum with a particle size of 3~1mm; Add 3% silicone so...

Embodiment 2

[0048] A refractory material for the cooling section of CDQ ovens, the raw material composition and weight percentage are: 39.5% of homogenized bauxite with a particle size of 5-1mm; 13% of mullite with a particle size of 3-1mm; 7% of corundum with a particle size of 3-1mm %, 4% of andalusite with a particle size not exceeding 0.1mm, 12% of corundum powder with a particle size of ≤0.088mm, 8% of mullite powder with a particle size of ≤0.088mm, 10% of superfine kaolin powder with a particle size of ≤0.01mm, and silicon carbide with a particle size of ≤1mm 5% powder, 1% ferrosilicon powder with 70% silicon, 0.5% carbon black with plastic fixed carbon content of 66%, plus organic silicon solution accounting for 5% of the total weight percentage of the above raw materials.

[0049] Preparation steps:

[0050] 1) First mix 39.5% of homogenized bauxite with a particle size of 5~1mm; 13% of mullite with a particle size of 3~1mm; 7% of corundum with a particle size of 3~1mm; Add 5% s...

Embodiment 3

[0059] A refractory material for the cooling section of CDQ ovens, the raw material composition and weight percentage are: 36.5% of homogenized bauxite with a particle size of 5-1mm; 10% of mullite with a particle size of 3-1mm; 15% of corundum with a particle size of 3-1mm %, 8% of andalusite with a particle size not exceeding 0.1mm, 3% of corundum powder with a particle size of ≤0.088mm, 20% of mullite powder with a particle size of ≤0.088mm, 2% of superfine kaolin powder with a particle size of ≤0.01mm, and silicon carbide with a particle size of ≤1mm 3% powder, 0.2% ferrosilicon powder with 75% silicon, 2.3% carbon black with plastic fixed carbon content of 70%, plus organic silicon solution accounting for 1.5% of the total weight percentage of the above raw materials.

[0060] Preparation steps:

[0061] 1) First mix 36.5% of homogenized bauxite with a particle size of 5~1mm; 10% of mullite with a particle size of 3~1mm; 15% of corundum with a particle size of 3~1mm; Add...

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PUM

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Abstract

The invention discloses a refractory material for a coke dry quenching furnace cooling section. The refractory material comprises the following components in percentage by weight: 30-40% of homogenized alumina of which the granularity is 5-1mm, 10-25% of mullite of which the granularity is 3-1mm; 5-20% of corundum of which the granularity is 3-1mm, 3-15% of andalusite of which the granularity is not more than 1mm, 3-15% of corundum powder of which the granularity is less than or equal to 0.088mm, 8-25% of mullite powder of which the granularity is less than or equal to 0.088mm, 1-10% of superfine kaolin powder of which the granularity is less than or equal to 0.01mm, 3-12% of silicon carbide powder of which the granularity is less than or equal to 1mm, 0.1-6% of ferrosilicon powder, 0.1-4% of carbon black with plasticity and an organic silicon solution which accounts for 3-6% of the total weight percentage of the raw materials. The preparation method comprises the steps of mixing homogenized alumina, mullite, corundum and andalusite, and adding the organic silicon solution; adding the superfine kaolin powder and carbon black with plasticity, and mixing; adding the corundum powder and mullite powder of which the granularity is less than or equal to 0.088mm, the silicon carbide powder of which the granularity is less than or equal to 1mm, and the ferrosilicon powder, and mixing; molding; drying; firing; cooling. The refractory material disclosed by the invention can be used for increasing the strength of the refractory material for the coke dry quenching furnace cooling section by at least 50%, increasing the wear-resisting property by 2-3.5 times, prolonging the service life to reach 5-8 years, and reducing the cost.

Description

technical field [0001] The invention relates to a refractory material and a preparation method thereof, in particular to a refractory material for a cooling section of a CDQ coke oven and a preparation method thereof. Background technique [0002] At present, the service life of CDQ coke ovens does not exceed 5 years, generally around 4 years. The main reason for the short service life is that the cooling section of CDQ coke ovens is worn and damaged. Especially in recent years, with the increase of output, the volume of CDQ coke ovens has been increasing, such as the increase of 7 meters or 7 meters 3 coke ovens; while the strength of the coke loaded is increased, the hardness is high, and the wear is also increased, so that the dry The wear amount of the cooling section of the coke quenching oven reached 37.2cm 3 / h, the wear rate reaches 50-70mm / year, and even some coke ovens can no longer be used normally after being used for less than a year. According to the applican...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/66C04B35/622
Inventor 徐国涛盛军波吕永劲陈胜春崔会明朱建文
Owner 武汉钢铁有限公司
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