Soldering flux composition containing acrylic resin used for soldering and soldering paste composition
A technology of composition and flux, applied in the direction of welding medium, welding equipment, welding/cutting medium/material, etc., can solve problems such as easy cracking, circuit short circuit, circuit metal corrosion, etc., and achieve crack suppression and separation suppression , the effect of inhibiting thermal denaturation
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[0079] The present invention will be described in detail below with reference to Examples and Comparative Examples. In addition, this invention is not limited to these Examples.
[0080] Synthesis of a compound containing a saturated alkyl group having a straight chain structure with 2 to 20 carbons
Synthetic example 1
[0082] 243.4g (3.38mol) of acrylic acid and 630.3g (2.6mol) of 2-hexyldecanol (CAS registration number: 2425-77-6) were added to a 2,000ml 4-neck flask equipped with a stirrer and a reflux condenser. OXOCOL1600, manufactured by Nissan Chemical Industry Co., Ltd.), 74.1 g (0.39 mol) of p-toluenesulfonic acid monohydrate, 4 g of p-methoxyhydroquinone, and 900 g of toluene were reacted under reflux for 6 hours. The solution was neutralized with a saturated aqueous sodium bicarbonate solution, extracted with ethyl acetate, and then concentrated to obtain 756 g of a compound (1) represented by the following general formula (7) (yield: 98%).
[0083] [chemical formula 7]
[0084] ···Formula (7)
Synthetic example 2
[0086] 756 g of a compound represented by the following general formula (8) was obtained under the same conditions as in Synthesis Example 1 except that 2-stearyl alcohol (trade name: FINE OXOCOL 180T, manufactured by Nissan Chemical Industries, Ltd.) was used as the raw material alcohol (2) (Yield: 98%).
[0087] [chemical formula 8]
[0088] ···General formula (8)
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