Pn heterojunction diode made of NiO:Cu/ZnO thin films
A pn junction and diode technology, applied in the field of NiO: Cu/ZnO heterogeneous pn junction diodes, to achieve the effect of improving performance
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[0018] (3) Preparation of n-ZnO: the background vacuum of the chamber before sputtering is better than 3x10 -4 pa, the relative partial pressure of oxygen used O 2 / (O 2 +Ar)=0%-100%, the sputtering pressure is 0.5-2Pa, and the sputtering power is 50-150W. Before coating, pre-sputter for 5 min to remove impurities on the target surface. The coating time is 20-120 minutes, the substrate temperature is RT-600° C. and the temperature is 200° C. to 700° C. and annealed for 0.5 to 1 hour.
[0019] (4) Preparation of electrodes: Ni electrodes were fabricated on the edges of NiO: Cu and ZnO surfaces by thermal evaporation.
[0020] (5) Test Keithley2612A to detect the ohmic contact characteristics of the electrode and the I-V characteristics (rectification characteristics) of the heterogeneous pn junction diode.
Embodiment 1
[0022] (1) Clean the silicon wafer with the cleaning method in the semiconductor process and dry it with nitrogen;
[0023] (2) Preparation of p-NiO: Cu: A NiO: CuO ceramic target with a diameter of 50 mm was used. NiO:Cu thin films prepared by magnetron sputtering. The chamber background vacuum before sputtering is better than 3x10 -4 pa, the relative partial pressure of oxygen used O 2 / (O 2 +Ar)=30%. The sputtering pressure is 2Pa, and the sputtering power is 150W. Before coating, pre-sputter for 5 min to remove impurities on the target surface. The coating time is 40min, and the substrate temperature is 300°C.
[0024] (3) Preparation of n-ZnO: A ZnO ceramic target with a diameter of 50 mm was used. The chamber background vacuum before sputtering is better than 3x10 -4 pa, the relative partial pressure of oxygen used O 2 / (O 2 +Ar)=0%, the sputtering pressure is 0.5Pa, and the sputtering power is 75W. Before coating, pre-sputter for 5 min to remove impurities on...
Embodiment 2
[0028] (1) Clean the silicon wafer with the cleaning method in the semiconductor process and dry it with nitrogen;
[0029] (2) Preparation of p-NiO: Cu: A NiO: Cu ceramic target with a diameter of 50 mm was used. NiO:Cu thin films prepared by magnetron sputtering. The chamber background vacuum before sputtering is better than 3x10 -4 pa, the relative partial pressure of oxygen used O 2 / (O 2 +Ar)=30%. The sputtering pressure is 2Pa, and the sputtering power is 150W. Before coating, pre-sputter for 5 min to remove impurities on the target surface. The coating time is 40min, and the substrate temperature is 400°C. Preparation of n-ZnO: A ZnO ceramic target with a diameter of 50 mm was used. The chamber background vacuum before sputtering is better than 3x10 -4 pa, the relative partial pressure of oxygen used O 2 / (O 2 +Ar)=0%, the sputtering pressure is 0.5Pa, and the sputtering power is 75W. Before coating, pre-sputter for 5 min to remove impurities on the target su...
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