Staged Feed Alkylation Reactor and Alkylation Process

An alkylation reactor and reactor technology, applied in chemical/physical/physical chemical nozzle reactors, chemical/physical/physical chemical mobile reactors, petroleum industry, etc., can solve the problem of increasing side reactions, inappropriate Heat release and other issues

Active Publication Date: 2016-03-02
CHINA PETROLEUM & CHEM CORP +1
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

This reactor is not suitable for the sulfuric acid alkylation reaction process, because the heat exchange method adopted is the heat extraction method of circulating materials, which is not suitable for the sulfuric acid alkylation reaction with large exothermic heat. The liquid storage tank at the lower part of the reactor and The use of reaction material circulation operation mode will increase the side reaction

Method used

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  • Staged Feed Alkylation Reactor and Alkylation Process
  • Staged Feed Alkylation Reactor and Alkylation Process
  • Staged Feed Alkylation Reactor and Alkylation Process

Examples

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Embodiment 1～3

[0037] use as figure 1 For the reactor with the structure shown, the gap between the upper bed and the lower bed is 100mm. The total width of the slots of the upper bed static assembly and the rotating assembly is 1 / 3 of its circumference. The rotating assembly and the stationary assembly are respectively provided with 3 layers, the overlapping position of the stationary toothed ring assembly and the rotating toothed ring assembly is 1 / 2 of the total bed height, and the gap distance between the stationary toothed ring assembly and the reactor shell is 50mm. The gap distance between the stationary toothed ring assembly and the rotating toothed ring assembly is 50 mm, and the thickness of the stationary toothed ring assembly is 0.5 times the thickness of the rotating toothed ring assembly. The lower bed rotating bed is made of stainless steel mesh packing, the bed porosity of the stainless steel mesh packing is 0.95, and the specific surface area is 4000m 2 / m 3 , the wire d...

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Abstract

The invention discloses a segmented feeding alkylation reactor and an alkylation reaction method. The reactor comprises a reactor cylinder, a head, a partition, an upper bed, a rotary bed, a composite bed, and an Material pipe, feeding distribution pipe, rotating shaft, supplementary material inlet, material outlet, recirculating cooling air inlet and recirculating cooling air outlet. The present invention also provides an alkylation reaction method, which adopts the above-mentioned segmented feed alkylation reactor, wherein isobutane and concentrated sulfuric acid first form an acid hydrocarbon emulsion in the upper bed layer, and then mix with the The hydrocarbon enters the rotating bed for alkylation reaction, and the reacted material realizes the demulsification process of the emulsion in the composite bed layer.

Description

technical field [0001] The invention relates to an alkylation reactor and an alkylation reaction method, in particular to an alkylation reactor and an alkylation reaction that adopts isobutane and C3-C5 olefins to feed in stages to catalyze the alkylation reaction. chemical reaction method. Background technique [0002] With the development of the economy, especially the rapid development of the transportation industry, the emission of vehicle exhaust is one of the main sources of air pollution. Improving the quality of gasoline is the most important way to reduce the pollution of vehicle exhaust. The alkylated oil obtained by the alkylation reaction of isobutane and C3-C5 olefins has the characteristics of no sulfur, high octane number, small difference between the octane number of the research method and the octane number of the motor method, and is a high-quality An important blending component of clean gasoline. [0003] Alkylation reaction is a traditional technology ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J19/28B01J19/26C10G50/00
CPCB01J19/26B01J19/28C10G50/00
Inventor 方向晨彭德强王璐瑶孟凡飞王阳峰王岩陈新陈建兵
Owner CHINA PETROLEUM & CHEM CORP
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