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The invention relates to a catalyst for dehydrogenating propane to prepare propone, which uses thermal-resistant oxide as carrier, uses palladium-group metal as main catalyst, uses IV A group metal and rare-earth metal as agents, uses halogen as modifier, and uses inorganic oxide with high temperature resistance as adhesive. The inventive catalyst under high temperature and low pressure has higher propane transfer rate, propone selectivity and reaction stability. And the preparation comprises that at 60-100Deg. C, immerging thermal-resistant oxide with rare-earth metal water solution for 2-10h, at 60-180Deg. C baking for 2-10h, at 400-600Deg. C baking for 3-10h, immerging said carrier and the water solution which contains palladium metal and IVA metal at 60-100Deg. C for 2-10h, and baking for 2-10h at 60-180Deg. C, adding adhesive, protruding agent and acid gel solvent, protruding and shaping, baking for 2-10h at 60-180Deg. C, activating for 3-10h at 400-600Deg. C, and reducing for 2-10h in hydrogen flow at 400-600Deg. C.

A method to promote the activity of a catalyst for dehydrogenation of propane to propylene is as follows: (1) an inorganic oxide bonding agent, a promoter and an acid solvent are added into a heat-resistant oxide; then after the oxide bonding agent, the promoter, the acid solvent and the oxide are kneaded evenly, the oxide is molded by rolling or band-extruding; (2) the catalyst carrier prepared is dried for 2 to 10 hours under the temperature of 60 centigrade degrees, and calcined under the temperature of 400 to 800 degrees; (3) the calcined carrier is immersed in a rare earth metal water solution under the temperature of 60 to 100 centigrade degrees for 2 to 10 hours; (4) the catalyst carrier modified by the rare earth is immersed in a water solution comprising platinum metal elementsand the fourteenth metal elements under the temperature of 400 to 600 centigrade degrees for 2 to 10 hours, and then the carrier is filtered, washed with distilled water, dried under the temperature of 60 to 180 centigrade degrees for 2 to 10 hours, and calcined under the temperature of 400 to 600 centigrade degrees for 2 to 10 hours; (5) the catalyst prepared is activated in the air under the temperature of 400 to 600 centigrade degrees for 3 to 10 hours, and reduced in a hydrogen flow under the temperature of 400 to 600 centigrade degrees for 2 to 10 hours; the reduced catalyst is used for catalytic reaction for dehydrogenation of propane to propylene.

Described are nanoparticulate formulations of a benzodiazepine, such as lorazepam, that does not require the presence of polyethylene glycol and propylene glycol as stabilizers, and methods of making and using such formulations. The formulations are particularly useful in aerosol and injectable dosage forms, and comprise nanoparticulate benzodiazepine, such as lorazepam, and at least one surface stabilizer. The formulations are useful in the treatment of status epilepticus, treatment of irritable bowel syndrome, sleep induction, acute psychosis, and as a pre-anesthesia medication.

The invention belongs to the field of modified polypropylene composite material, and relates to a low-VOC scratch-resistant modified polypropylene composite material which is applicable to manufacturing automobile interior trim parts, and comprises the components based on the parts by weight: 60-90 parts of polypropylene, 5-20 parts of toughening agent, 5-20 parts of mineral filler, 0.1-4 parts of odor adsorbent, 5-15 parts of wear-resistant agent / scratch-resistant agent and 0.1-3 parts of auxiliary agent, wherein the odor adsorbent is a mixture of three selected from clay, bentonite, porous silicon dioxide, activated aluminium oxide or molecular sieve; and the wear-resistant agent / scratch-resistant agent is one or a mixture of two in polytetrafluoroethylene micro powder or reaction-type polyorganosiloxane. The modified polypropylene composite material not only has better impact-resistant performance and strength, but also has excellent scratch-resistant performance and low-VOC diffusion characteristic; and the needed raw materials have wide source and can be conveniently and easily obtained.

The invention relates to a preparation method of a cold-formed soap. The method has simple process steps, and substitutes traditional aqueous solution of sodium hydroxide with sodium hydroxide or a dispersion of sodium hydroxide and glycerol; sodium hydroxide is completely soluble in glycerol but disperses in glycerol, so as to avoid fast reaction after mixing of sodium hydroxide solution with oil too, reduce the initial reaction rate of saponification, and effectively control saponification reaction rate; along with the saponification reaction, the reaction product of glycerol continuously increases to help more fully dispersion of sodium hydroxide, accelerate the reaction rate of sodium hydroxide and the remaining oil. Since the method employs an anhydrous formula, water evaporation process is not needed after soap formation by liquid soap, and the production cycle is significantly shortened; and the nutrition substances are added in solid form powder to effectively prevent the contact reaction of non-alkali-resistant nutrients and alkali hydroxide molecules, so as to retain the active nutrient ingredients in the soap and give full play to the role of skin care of the nutrients.

The invention provides nano zero-valent iron with montmorillonite serving as a carrier, and a preparation method and application thereof. The method comprises the steps of dissolving ferrous sulfate, adding soluble starch and montmorillonite particles into the ferrous sulfate solution in proportion, and obtaining mixed liquid; stirring after performing ultrasound treatment to the obtained mixed liquid, and obtaining precursor solution; adding the obtained precursor solution into sodium borohydride or potassium borohydride solution in proportion under the conditions of continuous stirring, continuing stirring for a period of time, performing solid-liquid separation, and obtaining the solid which is the nano zero-valent iron with montmorillonite serving as the carrier. According to the prepared nano zero-valent iron with montmorillonite serving as the carrier, interlayer and surface spaces of montmorillonite can be fully utilized, the activity and the stability are high, polymerization of the nano zero-valent iron can be reduced, and the nano zero-valent iron has remarkable effect when used for treating waste water containing hexavalent chromium.

The invention belongs to the technical field of materials and discloses a flexible low-smoke halogen-free flame-retardant wire and cable material and a preparation method thereof. The wire and cable material is prepared by using the following raw materials in parts by weight: 100 parts of ethylene-vinyl acetate copolymer, 1 to 70 parts of polyethylene, 30 to 100 parts of flame retardant, 5 to 20 parts of smoke suppressor, 0.1 to 5 parts of coupling agent, 1 to 20 parts of plasticizer, 0.1 to 10 parts of crosslinking agent, 3 to 15 parts of lubricant and 0.1 to 1 part of antioxidant. The wire and cable material disclosed by the invention is a thermoplastic sulfurized elastomer material, can be used for preparing insulating layers and sheath layers of wires and cables, and has the characteristics that no halogen is contained, the flame-retardant effect is good, the smoking amount is low, the surfaces of the insulating layers and sheath layers are smooth and do not stick with one another, the flexibility is good, the mechanical strength is high, the wear resistance is good, the processing fluidity is good, the process is simple and the material can be recycled.

A block copolymer comprises three block segments of a first segment, a second segment, and a third segment, and containing a polyalkenyl ether main chain, wherein the first segment is hydrophilic or hydrophobic, the second segment is hydrophobic, and the third segment is ionic; and at least one of the block segments has a structure represented by General Formula (1) below: —(CRaRb-CRc(OR1))—  (1) wherein Ra, Rb, and Rc are respectively H or CH3; R1 is selected from the group consisting of linear, branched, or cyclic alkyl groups of 1 to 18 carbon atoms, —(CH(R2)—CH(R3)—O)l—R4, and —(CH2)m—(O)n—R4; l and m are an integer from 1 to 12; n is 0 or 1; R2 and R3 are H or CH3; R4 is selected from the group consisting of H, linear, branched or cyclic alkyl groups of 1 to 6 carbon atoms, -Ph, -Pyr, -Ph-Ph, -Ph-Pyr, —CHO, —CH2CHO, —CO—CH═CH2, —CO—C(CH3)═CH2, —CH2COOR5, -PhCOOR5, —CH2SO3R5, and -PhSO3R5; the hydrogen on the carbon atoms constituting R4 except R5 moiety may be replaced by a linear or branched alkyl group of 1 to 4 carbon atoms, and the carbon in the aromatic ring may be replaced by nitrogen; and R5 is H, an alkyl group of 1 to 5 carbon atoms, or mono- or higher-valent cation.

The invention is directed to stable crosslinked water-soluble swellable polymers and methods for making same. More particularly, the invention relates to a composition comprising expandable polymeric particles having anionic sites and labile crosslinkers and stable crosslinkers, said particle mixed with a fluid and a cationic crosslinker that is capable of further crosslinking the particle on degradation of the labile crosslinker and exposure of the anionic sites so as to form a gel. A particularly important use is as an injection fluid in petroleum production, where the expandable polymeric particles are injected into target zone and when the heat and / or suitable pH of the target zone cause degradation of the labile crosslinker and the particle expands, the cationic crosslinker crosslinks the polymer to form a gel, thus diverting water to lower permeability regions and improving oil recovery.

The invention relates to a preparation and an application of two-component self-compacting concrete for a slab ballastless track. The preparation of the two-component self-compacting concrete is characterized in that the two-component self-compacting concrete is formed by mixing a dry mixture with a liquid in the ratio of 1:(0.05-0.15), wherein the dry mixture is formed by mixing components in parts by mass as follows: 100 parts of a bonding component, 0-30 parts of an inert mineral additive, 150-400 parts of fine aggregate, 150-300 parts of coarse aggregate, 0-2.0 parts of a water reducing agent, 5-20 parts of an expansion component, 0-10 parts of a viscosity regulating component, 0-0.5 parts of fiber and the like; and the liquid is formed by mixing components in parts by mass as follows: 100 parts of water, 0-4.0 parts of the water reducing agent, 0-3 parts of the viscosity regulating component and the like. According to the preparation and the application of the two-component self-compacting concrete for the slab ballastless track, the sensibility of the self-compacting concrete can be reduced, loss of the self-compacting concrete is reduced, and environment-friendly construction is realized. The two-component self-compacting concrete is applicable to the slab ballastless track of a high speed railway and is also applicable to the field of bridges, civil buildings, repair and strengthening and the like.

The invention provides a process for producing high molecular composite wood-plastic materials by using straws of agricultural plants, belonging to a process for utilizing the straws of agricultural plants. The process is that the straws of agricultural plants are crushed and dried, then the achieved straw powder is processed soakage treatment, and then modified straw powder is achieved after being dried, further dry powder is achieved by processing high-speed mixing and cooling mixing to the modified straw powder and other raw materials of which the plastic is the main material, and then the dry powder is squeezed out to produce grains, the materials after producing grains are squeezed out and shaped, consequently high molecular composite wood-plastic materials are manufactured. Owing to the process of the high molecular composite wood-plastic materials, the sound adhesion between the plant fibers existed in the straw powder after being processed superficial treatment by a plurality of modifiers, and plastics can be truly realized and the perfect property of materials can be achieved.

The invention discloses a nano inorganic antibacterial fiber masterbatch and a preparation method thereof. The nano inorganic antibacterial fiber masterbatch is composed of, by weight, 1-30 parts of fiber resin, 1-50 parts of nano inorganic antibacterial powder, 1-5 parts of silicon oil, 1-10 parts of a silane coupling agent, 1-5 parts of isocyanate and 0.1-0.5 part of an antioxidant. The preparation method includes: adding the nano inorganic antibacterial powder into a sand mill, then adding the silane coupling agent, and grinding at a high speed until a paste state is achieved; adding the isocyanate, and grinding at a high speed to obtain organic-inorganic hybrid nanopowder; jointly subjecting the nanopowder and the fiber resin to twin-screw extrusion for preparing the masterbatch. The prepared nano inorganic antibacterial fiber masterbatch is widely applicable to various fibers.

The invention discloses an ionic liquid-lithium salt gel polymer electrolyte and preparation and application thereof. The novel ionic liquid-lithium salt gel polymer electrolyte is prepared by freeze-drying with the polymer serving as a substrate, the ionic liquid serving as dispersant and the lithium salt serving as a conductive medium, and is assembled into a super capacitor with activated carbon electrodes. The ionic liquid-lithium salt gel polymer electrolyte, as the material of the super capacitor, has good flexibility, excellent electrical conductivity and superb cycle stability. Compared with the same type of gel electrolytes, the electrolyte has higher specific capacitance, energy density and power density.

The invention relates to yttria-stabilized zirconia powder and a preparation method thereof. The yttria-stabilized zirconia powder has the composition characteristics that yttria is taken as a stabilizer of a zirconia material; the powder comprises a doping system formed by one or more following third components: alumina, ceria, lanthana, copper oxide, magnesium oxide and calcium oxide, wherein the weight of the yttria is 2-8mol%, and the total doping weight of the alumina, the ceria, the lanthana, the copper oxide, the magnesium oxide and the calcium oxide is 0-5wt%. According to the yttria-stabilized zirconia powder and the preparation method, the deficiencies of an existing liquid phase preparation process of nanometer zirconia powder are overcome, and the prepared nanometer ZrO2 composite powder has the performance of uniformity in dispersion of components, uniform grain size, super-fineness, high sintering activity, good liquidity and the like. Furthermore, the preparation method is simple in process and low in cost and is easy to industrialize.

There invention discloses aqueous dispersions of nanoparticulate aerosol formulations, dry powder nanoparticulate aerosol formulation, propellant-based aerosol formulations, methods of using the formulations in aerosol delivery devices, and methods of making such formulations. The nanoparticles of the aqueous dispersions or dry powder formulations comprise insoluble drug particles having a surface modifier on the surface thereof.

An extrusion process for manufacturing thermosetting powder coating compositions is disclosed. A base material is fed to an extruder body such as from a pre-mix hopper; in one embodiment, hard to incorporate additives, such as pigments, are added to the base material after they exit from the pre-mix hopper and before they exit from the extruder body. In another embodiment, hard to incorporate additives in a dried form are added with the base material. The combined base material and hard to incorporate additives are mixed through at least a portion of the extruder body to form a homogeneous thermosetting powder coating composition. The output of the extruder body may be monitored for composition accuracy, wherein the amount of hard to incorporate additives added is dynamically adjusted based upon the monitored output. The process may be repeated for thermosetting powder coating compositions having distinct hard to incorporate additives utilizing a common base material in the pre-mix hopper. Use of one or more hyperdispersed pigments in the formation of a powder coating is also disclosed.

The invention discloses a preparation method for graphene conductive slurry. The preparation method comprises the steps of dissolving a dispersing agent into a solvent firstly, and performing ultrasonic oscillation to form a uniform solution; then adding graphene and a conductive carbon material into the solution to be mixed and stirred; next, performing full dispersion through a way of ultrasonic oscillation; and finally transferring the well-dispersed slurry to a high-speed shearing emulsification homogenizing machine to be sheared and dispersed to obtain the uniform and consistent and fully-dispersed graphene conductive slurry. The preparation method is simple and easy to implement and applicable to engineering production.

A composition that includes a hydrated inorganic filler and a polymer blend is disclosed. The polymer blend includes a polymerization or copolymerization product of one or more ethylenically unsaturated monomers. In addition, the polymer blend includes an aliphatic polyketone. The incorporation of aliphatic polyketone with polyethylene based polymers or copolymers results in dramatic improvements in both drip resistance and char strength; moreover, the composition of the present invention can use reduced amounts of hydrated inorganic filler relative to conventional polyethylene based compositions. This reduction in the amount of hydrated filler is expected to lead to improvements in physical properties and extrudability not otherwise possible. These properties make the compositions of the present invention particularly useful as an outer layer for electrical wires, optical fibers, or cables containing at least one wire, optical fiber, or both.

An extrusion process for manufacturing powder coating compositions is disclosed. The process generally includes a shear mixing step done at ambient temperature and a focused heating step in which the shear mix is heated to a higher temperature for a shorter time than in conventional methods. The focused heating provides for a shorter heat history, resulting in enhanced coating properties. The mixture may be cooled before it leaves the extruder.

A thermosetting powder coating composition extruder system including an extruder body and an injection system is disclosed. The extruder body includes segments surrounding one or more rotating screws. A first segment's main inlet receives material, such as from a pre-mix hopper, and a final segment's outlet discharges extrudate. A low pressure injector injects additives, particularly those that are hard to incorporate, into one or more segments at one or more injection positions at the main inlet or between the main inlet and the outlet. The injector includes a source of pressurization coupled to a pressure vessel, a pressure regulator maintaining the pressure at or below a given level, a flow regulator, and an injection port. A sensor adjacent the outlet monitors the physical characteristics of the extrudate and is coupled to a controller of the low pressure injector for dynamic control thereof.

The invention discloses a modified calcium carbonate with heat-isolating heat-insulating effect. The modified calcium carbonate is characterized by being prepared from the following raw materials in parts by weight: 90-95 parts of calcium carbonate, 5-7 parts of polyphenyl granules, 4-6 parts of hollow glass microballoons, 2-3 parts of adhesive mortar, 2-4 parts of bentonite, 2-3 parts of diatomite, 4-6 parts of epoxide resin, 5-7 parts of phenolic resin glue, 1-2 parts of polyethylene wax, 1-2 parts of zinc stearate and 3-4 parts of modified titanium dioxide. The modified calcium carbonate disclosed by the invention enhances the heat-isolating heat-insulating effect by being added with a small quantity of hollow glass microballoons with environmental-friendly heat-isolating effect and the mortar included in building materials and is enhanced in dispersing effect by being added with the modified titanium dioxide. According to the modified calcium carbonate, a filler produced through a simple production process has good binding force and is suitable for the addition application of a floor, a wall brick, a coating and the like.

The invention discloses a lithium-sulfur battery cathode material, a preparation method, and a lithium-sulfur battery, and belongs to the technical field of lithium-sulfur battery materials. The lithium-sulfur battery cathode material is a carbon-sulfur composite material, which is coated by a carbon cladding layer with a micro-porous structure. In the preparation method, under a vacuum condition, the raw materials are heated, just in one step, the sulfur and the carbon matrix are uniformly combined, the carbon precursor is carbonized, and the coating on the carbon-sulfur composite material is achieved. Compared with the conventional low-temperature coating method, the carbon cladding layer, which is carbonized at a high temperature and has a micro-porous structure, can form interactions just like the chemical bonds with the carbon-sulfur composite material; so that the micro-porous carbon cladding layer and the carbon-sulfur composite material are tightly combined together, thus the sulfur and discharge products cannot be easily dissolved in the electrolyte, the shuttling effect is prevented, the utilization rate of sulfur is improved, at the same time, the conductivity of the cathode material is better improved, and the cycle stability and capacity retention rate of the lithium-sulfur battery are both improved.

To provide: a production method using a catalyst which can substantially suppress leaching of active metal components and exhibit high activity for both reactions of transesterification of glycerides and esterification of free fatty acids each contained in a fat or oil; and the catalyst. A method for producing fatty acid alkyl esters and / or glycerin comprising a step of bringing a fat or oil into contact with an alcohol in the presence of a catalyst, wherein the catalyst is at least one catalyst selected from the group consisting of the following (I) to (V):(I) a metal oxide having an ilmenite structure and / or a slyrankite structure;(II) an oxide containing a metallic element belonging to the Group 12 and a metallic element belonging to the Group 4;(III) a mixed oxide containing a metallic element belonging to the Group 12 and a tetravalent transition metallic element;(IV) a metal oxide containing zirconium and at least one metallic element selected from the group consisting of metallic elements belonging to the Groups 4, 5 and 8; and(V) a metal oxide containing anatase type titanium oxide and / or rutile type titanium oxide, and the metal oxide containing a sulfur component of 700 ppm or less.

The invention discloses a fermentation rice milk drink and a preparation method thereof, which adopts fermentation rice as raw material that is processed through immersion, water bathing, cooking, fermentation, beating and pulp refining, and then the pH value of the obtained emulsion is adjusted; thermostable alpha-amylase Unikamyl HT is added according to a portion of 10 kilograms of the material being added with 3 to 5ml of thermostable alpha-amylase Unikamyl HT; then the obtained starch milk is sent into the ejector device through a flow meter; through flash cooking, the temperature of the obtained material should rise to 95 to 98 DEG C; then thermal insulation, enzyme stabilization, cooling and pH value regulation are done; efficient glucoamylase Unikase GA is added according to the portion of 10 kilograms of the material being added with 5 to 15ml of efficient glucoamylase Unikase GA; the temperature of the obtained material should rise to 100 DEG C, and the killing of enzyme is done; next, the obtained material are added with water, citric acid, xanthan and sodium carboxymethyl cellulose; the temperature raises by 55 to 60 DEG C so as to do secondary homogeneous; finally, the super-high-temperature sterilization and aseptic packing are done. The fermentation rice has specific flavor of rice wine, and is characterized by sweet and fragrant taste, light yellow or ivory color, being rich in nutrition and with the functions of health care and skin-maintaining and stable storage.

The invention provides a method for preparing silicon dioxide-coated quantum dots. The method comprises the following steps of: dispersing CdSe / CdS core-shell structural quantum dots into cyclohexane to obtain first mixed liquid; adding n-hexane, surfactant and ethyl orthosilicate into the first mixed liquid to obtain second mixed liquid; adding ammonia water into the second mixed liquid to carry out reaction; and depositing and separating a reaction product to obtain the silicon dioxide-coated quantum dots. The method firstly disperses the CdSe / CdS core-shell structural quantum dots into the cyclohexane to obtain the first mixed liquid, and then adds the n-hexane into the first mixed liquid serving as a dispersant. Since the n-hexane has similar polarity to the cyclohexane, the quantum dots can be dispersed into the n-hexane well. SiO2 formed by the hydrolysis of the ethyl orthosilicate can be coated on the quantum dots to the largest extent to obtain SiO2-coated CdSe / CdS core-shell structural quantum dots with uniform particle size. Compared with the prior art, the method for preparing the silicon dioxide-coated quantum dots has the advantages of few experimental procedures, simple operation and easy control.

Coated carbon nanotubes coated with 0.01-100 parts by weight of at least one type of aromatic condensation polymer selected from the group consisting of wholly aromatic polyamides, wholly aromatic polyesters, aromatic polyester carbonates, aromatic polycarbonates, semi-aromatic polyesters and wholly aromatic azoles, with respect to 100 parts by weight of the carbon nanotubes, as well as a process for their production. Aromatic condensation polymer compositions comprising 0.01-100 parts by weight of the coated carbon nanotubes and 100 parts by weight of an aromatic condensation polymer, and molded articles formed using them.

The invention relates to equipment for producing reconstituted tobacco through a dry-method paper making method. The equipment comprises a fiber decomposing device, a basal piece forming device, a pulp spraying device and a drying device. The production equipment is provided with various types of material ports and a built-in pipeline humidifying device, and a multi-pipeline feeding mode is adopted to enable the feeding uniformity and controllability to be improved; sprayed pulp contains much tobacco powder, tobacco extracts and adhesives and is large in viscosity; through the equipment, the pulp can be fully dispersed, and the phenomenon that hot air flowing in a drying oven is distributed unevenly to cause the pulp to be partially over-dried can be avoided.

The invention discloses a graphene infrared heat radiation coating and a preparation method thereof. The graphene infrared heat radiation coating comprises, by mass, 20-45% of film forming resin, 1-10% of graphene, 30-50% of an infrared radiation functional one-dimensional nano-material, 1.5-5% of a hard functional auxiliary filler, and 0-3% of a resin curing agent. Two-dimensional graphene is compounded with the one-dimensional infrared radiation functional filler, and the hard functional material is assisted, so the above three materials have synergistic effects to make a coating layer formed by the graphene infrared heat radiation coating have high radiance, high surface-directional heat conduction coefficient and excellent wear and scratch resistance. The preparation method has the advantages of guaranteeing of the stable performances of a coating dispersion system, easy control of technologic conditions, realization of stable performances of the prepared graphene infrared heat radiation coating, and effective reduction of the production cost.

The invention relates to a method for preparing a carbon nanotube static conductive coating on the surface of an EVA thin film, which comprises the following steps that: first, a carbon nanotube is added into ethanol solvent with the concentration more than or equal to 60 vt percent to be stirred into suspension under the action of dispersant and binder, ball milled to prepare dispersion liquid; and the dispersion liquid is oscillated in ultrasonic wave at 20 to 40DEG C, diluted and sprayed onto the surface of the EVA thin film, dried and cured to prepare the carbon nanotube static conductive coating. The method has simple process and is convenient to operate, and the prepared coating does not fall off or cohere after being used for a long time.

A method for sensing a stimulus comprising providing a sensing assembly having a first structure and a second structure, wherein the first structure is made of a material different than the second structure and each of the first structure and the second structure is nanoscale. The method further includes providing an inductive antenna operably coupled to the sensing assembly, disposing the sensing assembly upon a spatial area, exposing the sensing assembly to the stimulus thereby producing a detectable change in the sensing assembly, and wirelessly coupling a reader with the inductive antenna to obtain a signal representative of the detectable change in the sensing assembly.