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A Prediction Method of Durable and Instantaneous Limit Mechanical Properties of Polymers

A polymer and mechanical technology, applied in the direction of applying stable tension/pressure to test the strength of materials, etc., can solve the problems of large workload, small predicted time scale, and unsatisfactory time-temperature equivalent performance, achieving wide time scale, Simplify the test process and predict the effect of the method is simple and effective

Active Publication Date: 2017-10-24
HUBEI INST OF AEROSPACE CHEMOTECHNOLOGY
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The main defects of the main curve prediction method are: affected by the characteristics of the polymer material, the time-temperature equivalent performance of the fracture strain is not ideal; the prediction time scale is too small; the stress-strain test is a destructive test, and the workload is large

Method used

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  • A Prediction Method of Durable and Instantaneous Limit Mechanical Properties of Polymers

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Embodiment Construction

[0011] Below in conjunction with embodiment the present invention is further described.

[0012] Predict the tensile strength and breaking strain of nitrate plasticized polyether (NEPE) propellant in the ignition state at -20℃, and predict whether permanent damage will occur after storage for 5 years. It is known that the glass transition temperature of the propellant is -47.8°C, and the tensile strength at room temperature σ m =0.75MPa, fracture strain ε b =1.13 (test conditions: 25°C, 100mm / min). The ignition peak time of the propellant-charged engine is t f =25ms, the stress at the most dangerous part of the grain column during storage is not greater than 0.20MPa, the strain is not greater than 0.15, and the upper limit of the storage temperature is 25°C.

[0013] Step 1, condition selection and sample preparation.

[0014] In the stage of condition selection and sample preparation, the predicted objects are all viscoelastic materials.

[0015] The materials that need ...

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Abstract

The invention is a method for predicting the permanent and instantaneous limit mechanical properties of polymers for the performance evaluation of viscoelastic materials. Including the following steps: condition selection and sample preparation, mechanical test, curve preparation and data prediction. In the selection of conditions and sample preparation, the target is all viscoelastic materials. During the mechanical test, perform stress relaxation test, creep failure test and stress relaxation failure test at a series of temperatures to obtain data such as relaxation modulus and failure time; in the curve preparation and data prediction stage, according to the mechanical test results and prediction goals, make The relaxation modulus-time curve and the relaxation modulus master curve at a series of temperatures can be used to determine the relationship between a set of ultimate mechanical properties and action time, and obtain the predicted value of the permanent and instantaneous fracture strain or fracture strength of the polymer. The invention has the advantages that the method is simple and effective, the data is accurate and reliable, the test operation is convenient, the test process is simplified, and the test conditions are reasonable.

Description

technical field [0001] The invention relates to a technique for evaluating the mechanical properties of viscoelastic materials in extreme states, in particular to a method for predicting the permanent and instantaneous limit mechanical properties of polymers. Background technique [0002] In the prior art, the stress-strain master curve prediction method is usually used, which utilizes the time-temperature equivalent principle of polymer viscoelasticity, uses high temperature to simulate the permanent state, and uses low temperature to simulate the transient state. A series of stress-strain tests with different strain rates at different temperatures are carried out on the material to obtain the ultimate mechanical properties-strain rate curve of the material. Through curve translation, the test curves at different temperatures are overlapped into one curve to form a main limit mechanical properties at the reference temperature. curve. On the main curve of mechanical propert...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N3/18
Inventor 池旭辉庞爱民朱学珍常华封学华
Owner HUBEI INST OF AEROSPACE CHEMOTECHNOLOGY
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