Cationic electrodeposition coating composition
A cationic electrodeposition and composition technology, which is applied in electrophoretic coatings, epoxy resin coatings, polyurea/polyurethane coatings, etc., can solve the problems of difficult coating composition stability, throwing ability and corrosion resistance, and achieve excellent Stability, less blocking effect
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[0100] Preparation of Cationic Electrodeposition Coating Composition
[0101] The ratio of modified epoxy resin (A), amino group-containing epoxy resin (B) and blocked polyisocyanate curing agent (C) in the cationic electrodeposition coating composition of the present invention is: based on the components ( The total solid content of A), component (B) and component (C), the consumption of component (A) is 3 mass %-40 mass %, preferably 10 mass %-37 mass %, said component (B ) is used in an amount of 20% by mass to 60% by mass, preferably 28% by mass to 55% by mass, and component (C) is used in an amount of 10% by mass to 40% by mass, preferably 15% by mass to 35% by mass.
[0102] When the amount of the modified epoxy resin (A) is less than 3% by mass, corrosion resistance and exposure corrosion resistance may deteriorate. When the amount of the modified epoxy resin (A) is greater than 40% by mass, exposure corrosion resistance and composition stability may be deteriorated....
Embodiment
[0115] The present invention is explained in detail below with reference to Preparation Examples, Examples, and Comparative Examples; however, the present invention is not limited thereto. In the examples, "part" and "%" are based on mass.
[0116] Preparation of modified epoxy resin (A)
Synthetic example 1
[0118] Preparation of Modifier No. 1
[0119] 300 parts of ε-caprolactone was added to 400 parts of PP-400 (trade name of polypropylene glycol, molecular weight 400, manufactured by Sanyo Chemical Industry Co., Ltd.), and the mixture was heated to 130°C. Then, 0.01 part of tetrabutoxytitanium was added, and the mixture was heated to 170°C. While maintaining this temperature, samples were taken over time to monitor the amount of unreacted ε-caprolactone by infrared absorption spectroscopy. When the reaction rate reached above 98%, the resulting product was cooled to obtain No. 1 modifier.
PUM
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Abstract
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