A method for measuring optical constant and thickness of metal absorbing film layer
A technology for absorbing film layers and optical constants, which is applied in the direction of color/spectral characteristic measurement, measuring devices, optical devices, etc. Disconnection and other problems, to achieve the effect of simplifying the design and development and production control process, reducing equipment investment costs, and improving accuracy
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Embodiment 1
[0046] The embodiment provides a method for measuring the optical constant and thickness of a metal absorbing film layer, the flow of the measurement method is as follows figure 1 As shown, it specifically includes the following steps:
[0047] 1. Sample preparation
[0048] The coating sample in this step can be coated with a metal absorbing film layer on the substrate by magnetron sputtering or other coating methods. The plated metal absorbing film layer can be black metal (such as iron, chromium, manganese and their alloys) or heavy metal (such as titanium, nickel, niobium, tin, zinc, cobalt and their alloys).
[0049] Magnetron sputtering: Ar gas is used for magnetron sputtering. Under the same gas flow rate, the thickness of the metal absorbing film layer is proportional to the sputtering power (plating power described later), and proportional to the light transmittance. inverse relationship.
[0050] In order to improve the accuracy of the analysis, under the conditio...
Embodiment 2
[0073] Nickel-chromium alloy NiCr film is commonly used in off-line Low-E coated glass and solar control coated glass film system. The NiCr thin film plays a crucial role in adjusting the optical properties and environmental resistance of the product. The optical constant and thickness of the NiCr thin film are tested and analyzed in detail below using the optical constant and thickness measurement method of the metal absorbing film layer provided in Example 1 of the present invention.
[0074] 1, the present embodiment adopts off-line coating production line to carry out NiCr thin film coating sample production, according to the magnetron sputtering power source power range, selects the stable and reliable power value to test, the present invention is in same power 3kW, argon Ar gas flow rate 1400sccm (sccm: gas Flow rate unit, milliliter per minute under standard conditions), the glass substrate passes through the NiCr target at the speed of 1m / min and 0.5m / min respectively, ...
Embodiment 3
[0090] Analyze the optical constants of other ferrous metals, heavy metals and their alloys according to the same method and flow process as in Example 2, such as iron Fe, chromium Cr, manganese Mn, titanium Ti, nickel Ni, niobium Nb, tin Sn, zinc Zn, cobalt Co , stainless steel, etc., such as Image 6 is the optical constant of chromium Cr film in the wavelength range of 380-780nm, Figure 7 is the optical constant of the niobium Nb thin film in the visible light wavelength range of 380-780nm, Figure 8 is the optical constant of the stainless steel film in the visible light wavelength range of 380-780nm, and Table 3 is the polynomial model parameters of the optical constants of the chromium Cr, niobium Nb, and stainless steel film layers in the visible light wavelength range of 380-780nm.
[0091] Table 3 is the polynomial model parameters of optical constants in the visible light wavelength range of chromium Cr, niobium Nb, and stainless steel coatings
[0092]
[0093...
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Abstract
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